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GA/T 1633-2019 English PDF

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GA/T 1633-2019: Forensic sciences--Examination methods for ethyl glucuronide in blood and urine samples--GC-MS and LC-MS
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
GA/T 1633-2019329 Add to Cart 3 days Forensic sciences--Examination methods for ethyl glucuronide in blood and urine samples--GC-MS and LC-MS Valid

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Basic data

Standard ID: GA/T 1633-2019 (GA/T1633-2019)
Description (Translated English): Forensic sciences--Examination methods for ethyl glucuronide in blood and urine samples--GC-MS and LC-MS
Sector / Industry: Public Security (Police) Industry Standard (Recommended)
Classification of Chinese Standard: A92
Classification of International Standard: 13.310
Word Count Estimation: 14,161
Date of Issue: 2019
Date of Implementation: 2019-12-01
Issuing agency(ies): Ministry of Public Security

GA/T 1633-2019: Forensic sciences--Examination methods for ethyl glucuronide in blood and urine samples--GC-MS and LC-MS


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Forensic sciences--Examination methods for ethyl glucuronide in blood and urine samples--GC-MS and LC-MS ICS 13.310 A92 Public Safety Industry Standards of the People's Republic of China Forensic ethyl glucose in blood and urine Glycoside inspection gas chromatography-mass spectrometry and Liquid chromatography-mass spectrometry Published on October 14,.2019 2019-12-01 Implementation Issued by the Ministry of Public Security of the People's Republic of China

Foreword

This standard was drafted in accordance with the rules given in GB/T 1.1-2009. Please note that some content of this document may involve patents. The issuer of this document does not assume responsibility for identifying these patents. This standard was proposed by the National Toxic Analysis Subcommittee of Criminal Technical Standardization Technical Committee (SAC/TC179/SC1) and Be in charge. This standard was drafted by. Judicial Expertise Research Institute, Ministry of Public Security Material Evidence Appraisal Center. The main drafters of this standard. Yan Hui, Shen Baohua, Shen Min, Zhuo Xianyi, Liu Wei, Xiang Ping, Yu Zhongshan, He Yi, Wang Fanglin. Forensic ethyl glucose in blood and urine Glycoside inspection gas chromatography-mass spectrometry and Liquid chromatography-mass spectrometry

1 Scope

This standard specifies gas chromatography-tandem mass spectrometry (GC-MS/) for ethyl glucuronide (EtG) in forensic blood and urine MS), liquid chromatography-tandem mass spectrometry (LC-MS/MS) qualitative and quantitative testing method. This standard applies to qualitative and quantitative analysis of ethyl glucuronide in forensic blood and urine. Among other suspicious samples The qualitative analysis and quantitative analysis of ethyl glucuronide can be used by reference.

2 Normative references

The following documents are essential for the application of this document. For dated references, only the dated version applies to this article Pieces. For the cited documents without date, the latest version (including all amendments) applies to this document. GB/T 6682 Analysis laboratory water specifications and test methods GA/T 122 Nomenclature of poison analysis

3 Terms and definitions

The terms and definitions defined in GA/T 122 apply to this document.

4 Principle

Using blank samples and added samples as controls, extract blood and urine according to the requirements of parallel operation (gas chromatography-tandem mass spectrometry) Derivatization is required before analysis). After gas chromatography-tandem mass spectrometry and liquid chromatography-tandem mass spectrometry, the qualitative quantitative analysis is used to determine the retention time and quality. Spectral characteristic ions and relative abundance ratio were used as the basis for qualitative judgment; based on the peak area, the internal standard method was used for quantitative analysis.

5 Reagents and materials

5.1 Reagent The water for gas chromatography-mass spectrometry experiment should meet the third grade water specified in GB/T 6682, and the water for liquid chromatography-mass spectrometry experiment should meet Grade 1 water specified in GB/T 6682.Unless otherwise stated, the reagents used in the analysis are of analytical grade, and the reagents include. a) Methanol (chromatographically pure); b) Acetonitrile (chromatographically pure); c) BSTFA (bistrimethylsilane trifluoroacetamide)/T MCS (trimethylchlorosilane) mixed solution (volume ratio 99.1); d) anhydrous pyridine; e) 50% formic acid solution (chromatographically pure);
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