Home Cart Quotation About-Us
www.ChineseStandard.net
SEARCH

GB/T 4497.1-2010 English PDF

Q: How long will the true-PDF of English version of GB/T 4497.1-2010 be delivered?

Upon your order, we will start to translate GB/T 4497.1-2010_English as soon as possible, and keep you informed of the progress. The lead time is typically 1 ~ 3 working days. The lengthier the document the longer the lead time.

Q: Can I share the purchased PDF of GB/T 4497.1-2010_English with my colleagues?

Yes. The purchased PDF of GB/T 4497.1-2010_English will be deemed to be sold to your employer/organization who actually pays for it, including your colleagues and your employer's intranet.

Q: Does the price include tax/VAT?

Yes. Our tax invoice, downloaded/delivered in 9 seconds, includes all tax/VAT and complies with 100+ countries' tax regulations (tax exempted in 100+ countries). Avoidance of Double Taxation Agreements (DTAs) between Singapore and 100+ Countries: https://www.iras.gov.sg/taxes/international-tax

Q: Do you accept my currency other than USD?

Yes. If you need your currency to be printed on the invoice, please write an email to Sales@ChineseStandard.net. In 2 working-hours, we will create a special link for you to pay in any currencies. Otherwise, follow the normal steps: Add to Cart -- Checkout -- Select your currency to pay.

Q: Should I purchase the latest version GB/T 4497.1-2010?

Yes. Unless special scenarios such as technical constraints or academic study, you should always prioritize to purchase the latest version GB/T 4497.1-2010 even if the enforcement date is in future. Complying with the latest version means that, by default, it also complies with all the earlier versions, technically.

US$234.00 · In stock
Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email.
GB/T 4497.1-2010: Rubber -- Determination of total sulfur content -- Part 1: Oxygen combustion flask method
Status: Valid

GB/T 4497.1: Historical versions

Standard ID	USD	BUY PDF	Lead-Days	Standard Title (Description)	Status
GB/T 4497.1-2010	234	Add to Cart	3 days	Rubber -- Determination of total sulfur content -- Part 1: Oxygen combustion flask method	Valid
GB/T 4497-1984	279	Add to Cart	3 days	Vulcanized rubber--Determination of total sulphur content--Oxygen combustion flask method	Obsolete

Similar standards

GB/T 2941 GB/T 3511 GB/T 3512 GB/T 4498.1 GB/T 4498.2 GB/T 4499

Basic data

Standard ID: GB/T 4497.1-2010 (GB/T4497.1-2010)
Description (Translated English): Rubber -- Determination of total sulfur content -- Part 1: Oxygen combustion flask method
Sector / Industry: National Standard (Recommended)
Classification of Chinese Standard: G40
Classification of International Standard: 83.060
Word Count Estimation: 12,132
Date of Issue: 2011-01-14
Date of Implementation: 2011-12-01
Older Standard (superseded by this standard): GB/T 4497-1984
Adopted Standard: ISO 6528-1-1992, IDT
Regulation (derived from): National Standard Approval Announcement 2011 No.2 (Total No.167)
Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary: This standard specifies the method for the determination of total sulfur in rubber oxygen flask combustion method. This section applies to the determination of barium sulfate in addition to containing rubber and rubber products in the total sulfur content. The method specified in this section applies to the following kinds of rubber-Determination of total sulfur content: natural rubber, chloroprene rubber, SBR, butadiene rubber, isoprene rubber, butyl rubber, EPDM rubber, nitrile rubber, hard rubber and said rubber and rubber. This section provides a method for the presence of lead, antimony, zinc, specimens barium and calcium compounds, and the results are usually low. If the calcium to form calcium carbonate, can be obtained by changing the absorption liquid and reliable test results.

GB/T 4497.1-2010: Rubber -- Determination of total sulfur content -- Part 1: Oxygen combustion flask method

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Rubber.Determination of total sulfur content.Part 1. Oxygen combustion flask method ICS 83.060 G40 National Standards of People's Republic of China Replacing GB/T 4497-1984 Determination of total sulfur content in rubber Part 1. oxygen bottle combustion method Rubber ─Determinationoftotalsulfurcontent- Part 1. Oxygencombustionflaskmethod (ISO 6528-1..1992, IDT) 2011-01-14 release 2011-12-01 implementation General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China China National Standardization Management Committee released

Foreword

This standard is drafted in accordance with the rules given in GB/T 1.1-2009. GB/T 4497 "Determination of the total sulfur content of rubber" is divided into three parts. Part 1. Oxygen bottle combustion method; - Part 2. Sodium peroxide melting method; Part 3. Furnace combustion method. This part is part 1 of GB/T 4497. This part of the GB/T 4497-1984 "vulcanized rubber, the determination of total sulfur content of oxygen bottle combustion method." This section is the main change compared with GB/T 4497-1984 as follows. --- modified the standard number and standard name; --- Added foreword; --- added warning words; - the standard titration solution has been modified to barium chloride into barium perchlorate (see 3.4, 1984 version 2.3.5); --- the standard absorption solution was modified, the concentration of 1% hydrogen peroxide absorption solution used as a concentration of 2% hydrogen peroxide and peroxide Hydrogen - hydrochloric acid (see 3.1.1 and 3.1.2, 1984, 2.3.1); - modified alcohol was added to the alcohol before the titration, and the added ethanol was modified to 2-propanol (see 3.4, 2.2.3 in 1984); - increased sample preparation (see Chapter 5); --- Added the contents of the test report (see Chapter 9). ISO 6828-1..1992 "Determination of total sulfur content of rubber Part 1. Oxygen bottle combustion" (English version). This section is proposed by the China Petroleum and Chemical Industry Association. This part is under the jurisdiction of the National Committee for the Standardization of Test Methods (SAC/TC35/SC2). The main drafting unit of this part. Beijing Rubber Industry Research and Design Institute. The main drafters of this section. Cang Fei-fei, Ding Xiao-ying, 瓮zi Liang, Ji Bo. Determination of total sulfur content in rubber Part 1. oxygen bottle combustion method WARNING. Personnel using this national standard should have practical experience in formal laboratory work. This section does not indicate all possible safety questions. It is the responsibility of the user to adopt appropriate safety and health measures and to ensure compliance with the relevant laws and regulations of the State.

1 Scope

This part of GB/T 4497 specifies the method for the determination of total sulfur content in rubber by the oxygen bottle combustion method. This part is applicable to the determination of total sulfur content in rubber and rubber products containing barium sulfate. The methods specified in this section apply to the determination of total sulfur content in various rubbers. natural rubber, chloroprene rubber, styrene-butadiene rubber, Rubber, isoprene rubber, butyl rubber, EPDM rubber, nitrile rubber, hard rubber and rubber for the above-mentioned rubber. The methods specified in this section are generally low on the presence of lead, antimony, zinc, barium and calcium compounds. If calcium is stored as calcium carbonate In the case, a reliable test result can be obtained by changing the absorption liquid.

2 principle

In a flask containing hydrogen peroxide absorbing liquid and filled with oxygen, the sample is fired, in which the carbon and hydrogen of the organic matter are oxidized and the sulfur oxide Is absorbed by hydrogen peroxide solution into sulfuric acid, and sometimes the absorption liquid through the ion exchange column to remove the interference ions. Absorbent with thorium reagent or Thorium reagent and methine blue as indicator, titrated with standard solution of barium perchlorate.

3 reagents and materials

Unless otherwise specified, the reagents used are analytical reagents, the experimental water is distilled water or water of the same purity. Note. Two methods of preparing indicators (3.8) are described. Analysts can choose the most appropriate method based on their experience, experimental equipment, and experimental requirements. Preparation of indicators. 3.1 Absorbent liquid 3.1.1 Hydrogen peroxide, 2% (mass fraction) Absorbate. 1 volume of 30% hydrogen peroxide was diluted to 15 volumes with distilled water. Warning. 30% of the hydrogen peroxide solution is very corrosive to the skin, the operation should wear rubber or plastic gloves and goggles. 3.1.2 Hydrogen peroxide - hydrochloric acid mixed solution. 4 volumes of 30% hydrogen peroxide diluted with distilled water to 60 volumes plus 5 volumes of hydrochloric acid (ρ20 = 1.18 g/mL) were mixed evenly. 3.2 hydrochloric acid solution, c (HCl) = 0.5mol/L. 3.3 2-propanol. 3.4 barium perchlorate standard titration solution, c [Ba (ClO4) 2] = 0.01mol/L. 3.4.1 Preparation. Dissolve 3.363 g of anhydrous barium perchlorate with.200 mL of distilled water. The pH was adjusted to 3.5 with hydrochloric acid solution (3.2). With 2- Propanol was diluted to 1 L. 3.4.2 Calibration. ......

Image

Tips & Frequently Asked Questions:

Question 1: How long will the true-PDF of GB/T 4497.1-2010_English be delivered?

Answer: Upon your order, we will start to translate GB/T 4497.1-2010_English as soon as possible, and keep you informed of the progress. The lead time is typically 1 ~ 3 working days. The lengthier the document the longer the lead time.

Question 2: Can I share the purchased PDF of GB/T 4497.1-2010_English with my colleagues?

Answer: Yes. The purchased PDF of GB/T 4497.1-2010_English will be deemed to be sold to your employer/organization who actually pays for it, including your colleagues and your employer's intranet.

Question 3: Does the price include tax/VAT?

Answer: Yes. Our tax invoice, downloaded/delivered in 9 seconds, includes all tax/VAT and complies with 100+ countries' tax regulations (tax exempted in 100+ countries) -- See Avoidance of Double Taxation Agreements (DTAs): List of DTAs signed between Singapore and 100+ countries

Question 4: Do you accept my currency other than USD?

Answer: Yes. If you need your currency to be printed on the invoice, please write an email to Sales@ChineseStandard.net. In 2 working-hours, we will create a special link for you to pay in any currencies. Otherwise, follow the normal steps: Add to Cart -- Checkout -- Select your currency to pay.

Question 5: Should I purchase the latest version GB/T 4497.1-2010?

Answer: Yes. Unless special scenarios such as technical constraints or academic study, you should always prioritize to purchase the latest version GB/T 4497.1-2010 even if the enforcement date is in future. Complying with the latest version means that, by default, it also complies with all the earlier versions, technically.