GB/T 42954-2023 English PDFUS$189.00 · In stock  
  Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. GB/T 42954-2023: Determination of plant growth regulators in fertilizers - Gas chromatography-mass spectrometry Status: Valid 
 Basic dataStandard ID: GB/T 42954-2023 (GB/T42954-2023)Description (Translated English): Determination of plant growth regulators in fertilizers - Gas chromatography-mass spectrometry Sector / Industry: National Standard (Recommended) Classification of Chinese Standard: G20 Classification of International Standard: 65.080 Word Count Estimation: 10,19 Date of Issue: 2023-08-06 Date of Implementation: 2024-03-01 Issuing agency(ies): State Administration for Market Regulation, China National Standardization Administration GB/T 42954-2023: Determination of plant growth regulators in fertilizers - Gas chromatography-mass spectrometry---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order. ICS 65.080 CCSG20 National Standards of People's Republic of China Determination of plant growth regulators in fertilizers Gas Chromatography-Mass Spectrometry Published on 2023-08-06 2024-03-01 Implementation State Administration for Market Regulation Released by the National Standardization Administration Committee ForewordThis document complies with the regulations of GB/T 1.1-2020 "Standardization Work Guidelines Part 1.Structure and Drafting Rules of Standardization Documents" Custom drafting. Please note that some content in this document may be subject to patents. The publisher of this document assumes no responsibility for identifying patents. This document is proposed by China Petroleum and Chemical Industry Federation. This document is under the jurisdiction of the National Standardization Technical Committee on Fertilizers and Soil Conditioners (SAC/TC105). This document was drafted by. Shandong Product Quality Inspection Institute, Shanghai Institute of Chemical Industry Testing Co., Ltd., Sichuan Guoguang Agrichemical Co., Ltd. Company, Shandong Agricultural University Fertilizer Technology Co., Ltd., Shandong Hetai Testing Technology Service Co., Ltd. The main drafters of this document. Zhang Juan, Huang Heqing, Sun Shengmin, Liu Shuang, Lu Dongdong, Yang Xu, Wu Pandao, Zhu Hairong, He Jie, Zhang Jing, Meng Qingyu, Tian Yewei, Chen Panxin, Ding Yiman, Yang Yi. Determination of plant growth regulators in fertilizers Gas Chromatography-Mass Spectrometry1 ScopeThis document describes the use of gas chromatography-mass spectrometry for the determination of ethyl ethyl, chloraniline, thiozolin, sulfonate, flumetrazine, and polymethacrylate in fertilizers. Methods for seven plant growth regulators including clobutrazole and unconazole. This document is applicable to the determination of ethanol, chlorpheniramine, thiocyanin, butylin, flumetrazine, paclobutrazol and uniconazole in fertilizers.2 Normative reference documentsThis document has no normative references.3 Terms and definitionsThere are no terms or definitions to be defined in this document.4 PrinciplesIn the sample, the amine fresh fat, chloraniline, thiazolin, butylin, flumetrazine, paclobutrazol, and unconconnazole were extracted with acetone. The extract solution was fixed to volume and vortexed. Spin, ultrasonic, centrifuge, filter, and undergo gas chromatography separation and mass spectrometry detection. By comparing with the standard material mass spectrum, retention time, fragment ion mass-to-charge ratio Its abundance was compared for qualitative analysis and external standard method for quantification.5 reagents or materials5.1 Helium, purity ≥99.999%. 5.2 Acetone, chromatographically pure. 5.3 Acetate standard material (CAS number. 10369-83-2), 1000mg/L (acetone is the solvent). 5.4 Chloropropyl standard material (CAS number. 101-21-3), 1000mg/L. 5.5 Thioxin standard material (CAS number. 55290-64-7), 1000mg/L. 5.6 Zhongbuling standard material (CAS number. 33629-47-9), 1000mg/L. 5.7 Flumetrazine standard material (CAS number. 62924-70-3), 1000mg/L. 5.8 Paclobutrazol standard material (CAS number. 76738-62-0), 1000mg/L. 5.9 Uniconazole standard material (CAS number. 83657-22-1), 1000mg/L. 5.10 Standard stock solution. Pipette respectively the standard products of ethyl ethyl, chlorpropazol, thiocyanin, butylin, flumetrazine, paclobutrazol and uniconazole. 1.0 mL, dilute to volume with acetone in a 10 mL volumetric flask, and prepare a standard solution with a mass concentration of 100 mg/L. Keep sealed Store in -20℃ refrigerator until use. The validity period is 1 month. 5.11 Intermediate mixed standard solution. Pipette 1.0 mL of each 100 mg/L standard stock solution (5.10) into a 10 mL volumetric flask. Dilute acetone to volume and prepare a standard solution with a mass concentration of 10 mg/L. Prepare it now. ......Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of GB/T 42954-2023_English be delivered?Answer: Upon your order, we will start to translate GB/T 42954-2023_English as soon as possible, and keep you informed of the progress. The lead time is typically 1 ~ 3 working days. 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