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GB/T 32699-2016 English PDF

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GB/T 32699-2016: Test method for purity of multifunctional acrylates used for UV materials -- Capillary gas chromatography
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
GB/T 32699-2016119 Add to Cart 3 days Test method for purity of multifunctional acrylates used for UV materials -- Capillary gas chromatography Valid

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Basic data

Standard ID: GB/T 32699-2016 (GB/T32699-2016)
Description (Translated English): Test method for purity of multifunctional acrylates used for UV materials -- Capillary gas chromatography
Sector / Industry: National Standard (Recommended)
Classification of Chinese Standard: G15
Classification of International Standard: 37.040.20
Word Count Estimation: 6,652
Date of Issue: 2016-06-14
Date of Implementation: 2017-01-01
Regulation (derived from): National Standard Announcement No. 8 of 2016
Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary: This standard specifies a method for the determination of the purity (ester content) of polyfunctional acrylate monomers for use in light-sensitive materials by capillary gas chromatography. This standard applies to the determination of the purity (ester content) of polyfunctional acrylate monomers for photosensitive materials.

GB/T 32699-2016: Test method for purity of multifunctional acrylates used for UV materials -- Capillary gas chromatography


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Test method for purity of multifunctional acrylates used for UV materials.Capillary gas chromatography ICS 37.040.20 G15 National Standards of People's Republic of China Functional properties of polyfunctional acrylate monomers for photosensitive materials (Determination of ester content) - Capillary gas chromatography 2016-06-14 release 2017-01-01 Implementation General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China China National Standardization Management Committee released

Foreword

This standard is drafted in accordance with the rules given in GB/T 1.1-2009. This standard is proposed by the China Petroleum and Chemical Industry Association. This standard is nationalized by the National Standardization Technical Committee for Photographic Materials (SAC/TC102). The drafting unit of this standard. Jiangsu Miki Chemical Co., Ltd., Tianjin Tianjiao Radiation Curing Material Co., Ltd., Jiangsu Rita Technology Co., Ltd., China Lucky Group Co., Ltd. The main drafters of this standard. Xue Zhongqun, Hui Zhengquan, Luo Kan, Zou Jinyu, Wang Hongbao, Dong Rongjiang, Huang Fengqi, Ma Huaixiang, Wang Lili. Functional properties of polyfunctional acrylate monomers for photosensitive materials (Determination of ester content) - Capillary gas chromatography

1 Scope

This standard specifies the method for the determination of the purity (ester content) of the polyfunctional acrylate monomer for photosensitive materials by capillary gas chromatography. This standard is applicable to the determination of the purity (ester content) of polyfunctional acrylate monomers for photosensitive materials.

2 method summary

A small amount of the photosensitive material was weighed with a multifunctional acrylate sample and dissolved in an appropriate amount of acetone. The gas was injected into a gas chromatograph containing an inert gas The capillary column of the body, the multifunctional acrylate is separated from the impurities such as alcohols, other esters, ethers and unknown compounds; the separated components are measured by a detector And record the chromatogram. Using the area normalization method, the peak area of the acrylic ester was divided by the total peak area of each component. The relative concentration of the acid esters.

3 reagents and materials

3.1 Acetone. Analytical purity. 3.2 Hydrogen. Before use, use dehydration device, silica gel, molecular sieve or activated carbon for purification. 3.3 high purity nitrogen. purity ≥ 99.99%. 3.4 Air. should be non-corrosive impurities, need to use before the use of dehydration devices, silica gel, molecular sieve or activated carbon for purification.

4 instruments and conditions

4.1 Gas chromatograph (GC) and chromatographic workstations in Table 1. Table 1 Project conditions Capillary column OV-170.53mm × 15m; film thickness 0.5μm; wide-hole elastic quartz cross Column Carrier gas with high purity nitrogen Carrier gas flow rate 6mL/min (wire speed 15cm/s) Oven program temperature rise The starting temperature is 70 ° C The initial temperature hold time is 2min ~ 5min Heating rate of 10 ℃/min Final temperature 260 ℃ ~ 280 ℃ End temperature retention time 10min ~ 15min Hydrogen Flame Ionization Detector Hydrogen 30mL/min Air 350mL/min
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