GB/T 2441.3-2010 English PDFUS$149.00 · In stock
Delivery: <= 2 days. True-PDF full-copy in English will be manually translated and delivered via email. GB/T 2441.3-2010: Determination of urea -- Part 3: Water content -- Karl fischer method Status: Valid GB/T 2441.3: Historical versions
Basic dataStandard ID: GB/T 2441.3-2010 (GB/T2441.3-2010)Description (Translated English): Determination of urea -- Part 3: Water content -- Karl fischer method Sector / Industry: National Standard (Recommended) Classification of Chinese Standard: G20 Classification of International Standard: 65.080 Word Count Estimation: 5,523 Date of Issue: 2010-06-30 Date of Implementation: 2011-01-01 Older Standard (superseded by this standard): GB/T 2441.3-2001 Quoted Standard: GB/T 6283; HG/T 2843 Regulation (derived from): National Standard Approval Announcement 2010 No.2 (Total No.157) Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China Summary: This standard specifies the determination of urea in water by the Karl Fischer method. This section applies to the determination of ammonia and carbon dioxide obtained urea synthesis moisture. Arbitration, using pyridine -containing Karl Fischer reagents. GB/T 2441.3-2010: Determination of urea -- Part 3: Water content -- Karl fischer method---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.Determination of urea.Part 3. Water content.Karl fischer method ICS 65.080 G20 National Standards of People's Republic of China Replacing GB/T 2441.3-2001 Determination of urea Part 3. Moisture Fisher Fischer 2010-06-30 release 2011-01-01 implementation General Administration of Quality Supervision, Inspection and Quarantine of the People 's Republic of China China National Standardization Management Committee released ForewordGB/T 2441 "Determination of urea method" is divided into the following nine parts. - Part 1. total nitrogen content; - Part 2. Biuret content spectrophotometric method; - Part 3. Moisture Fisher Fischer; - Part 4. Iron content - phenanthroline spectrophotometric method; - Part 5. Alkalinity volumetric method; - Part 6. Water insoluble content weight method; - Part 7. Particle size sieving method; - Part 8. Sulfate content visual turbidimetric method; Part 9. Spectrophotometric method for methylenediourea content. This part is part 3 of GB/T 2441. This part of the replacement GB/T 2441.3-2001 "Determination of moisture determination of moisture Karl Fischer method." This section is the main change compared with GB/T 2441.3-2001 as follows. --- removed ISO preface. This section is proposed by the China Petroleum and Chemical Industry Association. This section is under the jurisdiction of the National Technical Committee on Standardization of Fertilizers and Soil Conditioners (SAC/TC105). This part of the drafting unit. National Fertilizer Quality Supervision and Inspection Center (Shanghai). This part of the main drafters. Zhang Qiuzhen, room friends. This part of the previous version of the standard to replace the release of the situation. GB/T 2444-1981, GB/T 2444-1991, GB/T 2441.3-2001. Determination of urea Part 3. Moisture Fisher Fischer1 ScopeThis part of GB/T 2441 specifies the use of Karl Fischer method for the determination of moisture in urea. This part applies to the determination of urea moisture from ammonia and carbon dioxide synthesis. At the time of arbitration, the use of pyridine-containing Karl Fischer reagent.2 normative reference documentsThe terms of this document are the terms of this part by reference to this part of GB/T 2441. Any reference to the date of the text , All subsequent amendments (excluding corrigenda) or revisions do not apply to this part, however, encouragement under this section The parties to the agreement study whether the latest version of these documents can be used. For undated references, the latest edition of this document applies section. GB/T 6283 Determination of moisture content in chemical products Karl Fischer method (general method) HG/T 2843 chemical analysis of chemical fertilizers commonly used standard titration solution, standard solution, reagent solution and indicator solution3 principleThe moisture present in the sample is quantitatively reacted with the Karl Fischer reagent with known water droplet degree. The reaction is as follows. H2O I2 SO2 3C5H5 → N 2C5H5N · HI C5H5N · SO3 C5H5N · SO3 CH3 → OH C5H5NH · OSO2OCH34 reagentThe following parts of the reagents and solutions flammable and toxic to humans, the operator should be careful such as splashing on the skin should be immediately washed with water Wash or fit the way to deal with, if not suited to immediate medical treatment. The reagents, solutions and water used in this section shall comply with the requirements of HG/T 2843 when not specified and formulated. 4.1 Karl Fischer reagent; 4.1.1 Karl Fischer reagent containing pyridine; 4.1.2 Karl Fischer reagent without pyridine; 4.2 Methanol (dehydration); 4.3 Sodium tartrate dihydrate.5 instrumentsKarl Fischer direct power titration equipment, the typical device according to GB/T 6283 configuration.6 Analysis stepsMake two samples in parallel. 6.1 Calibration of Karl Fischer Reagent According to GB/T 6283 specified steps, with water or sodium tartrate diamine calibration reagent on the water titer T. 6.2 Determination. ......Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of GB/T 2441.3-2010_English be delivered?Answer: Upon your order, we will start to translate GB/T 2441.3-2010_English as soon as possible, and keep you informed of the progress. The lead time is typically 1 ~ 2 working days. 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