YS/T 555.9-2009 English PDFUS$169.00 · In stock
Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. YS/T 555.9-2009: Methods for chemical analysis of molybdenum concentrate. Determination of potassium and sodium content. Flame atomic absorption spectrometry Status: Valid YS/T 555.9: Historical versions
Basic dataStandard ID: YS/T 555.9-2009 (YS/T555.9-2009)Description (Translated English): Methods for chemical analysis of molybdenum concentrate. Determination of potassium and sodium content. Flame atomic absorption spectrometry Sector / Industry: Nonferrous Metallurgy Industry Standard (Recommended) Classification of Chinese Standard: H14;D43 Classification of International Standard: 77.120.99 Word Count Estimation: 6,673 Date of Issue: 2009-12-04 Date of Implementation: 2010-06-01 Older Standard (superseded by this standard): YS/T 555.10-2006 Regulation (derived from): MIIT [2009] No. 66 Issuing agency(ies): Ministry of Industry and Information Technology Summary: This standard specifies the molybdenum content of potassium and sodium content determination. This standard applies to molybdenum potassium and sodium content. Measuring range: 0. 01% to 2. 00%. YS/T 555.9-2009: Methods for chemical analysis of molybdenum concentrate. Determination of potassium and sodium content. Flame atomic absorption spectrometry---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order. Methods for chemical analysis of molybdenum concentrate.Determination of potassium and sodium content.Flame atomic absorption spectrometry ICS 77.120.99 H14 People's Republic of China Nonferrous Metals Industry Standard Replacing YS/T 555.10-2006 Methods for chemical analysis of molybdenum concentrate Determination of the amount of potassium and sodium content Flame Atomic Absorption Spectrometry Posted 2009-12-04 2010-06-01 implementation Ministry of Industry and Information Technology of the People's Republic of China released ForewordYS/T 555 "Methods for chemical analysis of molybdenum concentrate" includes 11 parts. YS/T 555.1 Methods for chemical analysis of molybdenum concentrate molybdenum content of lead molybdate assay gravimetric method YS/T 555.2 Methods for chemical analysis of molybdenum concentrate - Determination of silicon dioxide content and weight of molybdenum blue spectrophotometric method YS/T 555.3 Methods for chemical analysis of molybdenum concentrate arsenic content - Atomic Fluorescence Spectrometry and DDTC-Ag spectrophotometry YS/T 555.4 Methods for chemical analysis of molybdenum concentrate tin content - Atomic Fluorescence Spectrometry YS/T 555.5 Methods for chemical analysis of molybdenum concentrate phosphorus content of molybdenum blue spectrophotometric determination of phosphorus YS/T 555.6 Methods for chemical analysis of molybdenum concentrate copper, lead, bismuth, zinc content - Flame Atomic Absorption Spectrometry YS/T 555.7 Methods for chemical analysis of molybdenum concentrate calcium oxide content by flame atomic absorption spectrometry YS/T 555.8 Methods for chemical analysis of molybdenum concentrate - Determination of tungsten content - Thiocyanate spectrophotometric method YS/T 555.9 Methods for chemical analysis of molybdenum concentrate the amount of potassium and sodium contents - Flame Atomic Absorption Spectrometry YS/T 555.10 Methods for chemical analysis of molybdenum concentrate rhenium contents - Thiocyanate spectrophotometric Determination of YS/T 555.11 Methods for chemical analysis of molybdenum concentrate oil and moisture content of the total weight of the law Part is divided into 9 parts. The partial replacement of YS/T 555.10-2006 "concentrates - Methods of determination of potassium and sodium content" (formerly GB/T 15079.10- 1994). This portion of YS/T 555.10-2006 compared to the main changes are as follows. --- Increasing the molybdenum substrate method to eliminate interference; --- Increasing the precision of the terms; --- Text format has been modified, supplemented with quality assurance and control provisions. The non-ferrous metal part by the National Standardization Technical Committee and centralized. This section is responsible for drafting unit. Jinduicheng Molybdenum Group Co., Ltd., China Nonferrous Metals Industry Institute of Standards and Metrology and Quality. Participated in the drafting of this section. JCC (Dexing) New Mining Technology Development Co., Ltd., Luoyang Luanchuan Molybdenum Group Co. Shares the company. The main drafters of this section. Guang Ji, Lu Qingxiang, Wang Zhongqi, Souchon, Zhangjiang Feng, Yu Huanrong. This part certifier. Bin strong beam, Li Hongjun, Tian Yonghong. This part of the standard replaces the previous editions are. --- GB/T 15079.10-1994; --- YS/T 555.10-2006. Methods for chemical analysis of molybdenum concentrate Determination of the amount of potassium and sodium content Flame Atomic Absorption Spectrometry1 ScopeThis section provides the determination of molybdenum concentrate in the amount of potassium and sodium content. This section applies to the determination of molybdenum concentrate in the amount of potassium and sodium content. Measuring range. 0.01% to 2.00%.2 Method summarySamples with nitric acid, hydrofluoric acid decomposition in dilute nitric acid medium, cesium chloride as deionization agent for potassium atomic absorption spectrometer wavelength 766.5nm, 589.0nm sodium at the air - acetylene flame measured absorbance.3 ReagentsUnless otherwise indicated in the analysis using only recognized as analytical reagents and secondary deionized water. 3.1 nitrate (ρ1.42g/mL), pure class distinctions. 3.2 Hydrofluoric acid (ρ1.15g/mL). 3.3 cesium chloride solution (10g/L). Weigh 1g of cesium chloride (spectroscopically pure), placed in 100mL beaker, it adds appropriate amount of water to dissolve completely shift Into 100mL volumetric flask, dilute with water to volume, and mix. Store in plastic bottle. 3.4 molybdenum substrate solution (5mg/mL). Weigh 1.000g ammonium molybdate (high-purity reagents, potassium and sodium content is minimal), dissolved in water and transferred to 100mL volumetric flask, dilute with water to volume, and mix. Store in plastic bottle. 3.5 Potassium standard stock solution. Weigh 0.0953g pre-ignition 1h and cooled to room temperature in a dryer at 550 ℃ potassium chloride (Spectra Pure), placed in 200mL beaker, add appropriate amount of water to dissolve it completely and transferred to 500mL volumetric flask, dilute with water to volume, and mix. Store in plastic bottle. This solution 1mL containing 100μg potassium. 3.6 Potassium standard solution. Pipette 10.00mL potassium standard stock solution (3.5), placed in 100mL volumetric flask, dilute to the mark, mix uniform. Store in plastic bottle. This solution 1mL containing 10μg potassium. 3.7 Sodium standard stock solution. Weigh 0.1271g, pre-burning 1h and cooled to room temperature in a dryer at 550 ℃ sodium chloride (light Pure spectrum), placed in 200mL beaker, it adds appropriate amount of water to dissolve it completely and transferred to 500mL volumetric flask, dilute to the mark with water, mix uniform. Store in plastic bottle. This solution 1mL containing 100μg sodium. 3.8 Sodium standard solution. Pipette 10.00mL sodium standard stock solution (3.7), placed in 100mL volumetric flask, dilute to the mark with water, mix uniform. Store in plastic bottle. This solution 1mL containing 10μg sodium.4 InstrumentAtomic absorption spectrometer, with potassium, sodium hollow cathode lamp. Under optimum working conditions for those who can reach the following indicators can be used. --- Precision minimum requirements. measuring the absorbance of the highest standard solution 10 times the standard deviation should not exceed the average absorbance 1.5%. Lowest measured standard solution (not a "zero" standard solution) absorbance of 10 times, and the standard deviation is not more than the highest standard solution 0.5% average absorbance. --- Characteristic concentration. In line with the determination of the solution matrix solution, characteristic concentration of potassium and sodium should not exceed 0.01μg/mL. --- Linear calibration curve. The curve is divided into five sections according to concentration, absorbance difference between the absorbance difference between the highest and the lowest segment segment ......Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of YS/T 555.9-2009_English be delivered?Answer: Upon your order, we will start to translate YS/T 555.9-2009_English as soon as possible, and keep you informed of the progress. The lead time is typically 1 ~ 3 working days. 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