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YS/T 535.8-2009 English PDF

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YS/T 535.8-2009: Chemical analysis methods of sodium fluoride. Part 8: Determination of water insoluble matter content. Gravimetric method

YS/T 535.8: Historical versions

Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
YS/T 535.8-2009179 Add to Cart 2 days Chemical analysis methods of sodium fluoride. Part 8: Determination of water insoluble matter content. Gravimetric method  
YS/T 535.8-2006199 Add to Cart 2 days Methods for chemical analysis of sodium fluoride The gravimetric method for the determination of water-insoluble matter Obsolete

Similar standards

YS/T 581.15   GB/T 1425   GB/T 351   YS/T 535.11   YS/T 535.2   YS/T 535.10   

Basic data

Standard ID: YS/T 535.8-2009 (YS/T535.8-2009)
Description (Translated English): Chemical analysis methods of sodium fluoride. Part 8: Determination of water insoluble matter content. Gravimetric method
Sector / Industry: Nonferrous Metallurgy Industry Standard (Recommended)
Classification of Chinese Standard: H21
Classification of International Standard: 71.060.50
Word Count Estimation: 5,585
Date of Issue: 2009-12-04
Date of Implementation: 2010-06-01
Older Standard (superseded by this standard): YS/T 535.8-2006
Quoted Standard: YS/T 535.10-2009
Regulation (derived from): MIIT [2009] No. 66
Issuing agency(ies): Ministry of Industry and Information Technology
Summary: This standard specifies the amount of fluoride in the water insoluble measurement method. This standard applies to sodium fluoride in water insoluble content. Measuring range (mass fraction): �� 15. 0%.

YS/T 535.8-2009: Chemical analysis methods of sodium fluoride. Part 8: Determination of water insoluble matter content. Gravimetric method


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Chemical analysis methods of sodium fluoride. Part 8. Determination of water insoluble matter content.Gravimetric method ICS 71.060.50 H21 People's Republic of China Nonferrous Metals Industry Standard Replacing YS/T 535.8-2006 Chemical analysis of sodium fluoride Part 8. determination of water insoluble content Weight method 2009-12-04 released 2010-06-01 Implementation Issued by the Ministry of Industry and Information Technology of the People's Republic of China

Foreword

YS/T 535 "sodium fluoride chemical analysis method" is divided into 10 parts. - Part 1. Determination of wet water content - Weight method; - Part 2. Determination of fluorine content - Distillation - thorium nitrate titration capacity method; - Part 3. Determination of silicon content - Molybdenum blue spectrophotometric method; - Part 4. Determination of iron content - o - phenanthroline spectrophotometric method; - Part 5. Determination of soluble sulfate content - Turbidimetric method; - Part 6. Determination of carbonate content - Gravimetric method; - Part 7. Determination of acidity and neutral method; - Part 8. Determination of water insoluble content - Gravimetric method; - Part 9. Determination of chlorine content - Turbidimetric method; - Part 10. Preparation and storage of specimens. This section is part 8. This part replaces YS/T 535.8-2006 (original GB/T 8158.8-1987). This part is the revision of YS/T 535.8-2006 "Determination of water insoluble content by gravimetric method for chemical analysis of sodium fluoride" YS/T 535.8-2006 compared to increase the precision and quality assurance and control and so on. This part of the National Nonferrous Metals Standardization Technical Committee proposed and centralized. This part is drafted by Fushun Aluminum Co., Ltd. and China Nonferrous Metals Industry Standard Measurement Quality Research Institute. This part is drafted by Fushun Aluminum Company Limited. This part of the main drafters. Feng Yingxin, the original Jianchang, Liu Shulan. This part of the previous version of the standard to replace the release of the situation. YS/T 535.8-2006 (original GB/T 8158.8-1987). Chemical analysis of sodium fluoride Part 8. determination of water insoluble content Weight method

1 Scope

This section specifies the determination of the amount of water insoluble in sodium fluoride. This part is applicable to the determination of the amount of water insoluble in sodium fluoride. Determination range (mass fraction). ≤15.0%.

2 normative reference documents

The terms of this document are incorporated by reference in this section and become part of this section. Whichever is the date of the reference file, which is followed by all (Excluding corrigenda) or revisions do not apply to this part, however, encourage parties to reach an agreement under this section Whether you can use the latest version of these files. For undated references, the latest edition applies to this section. Methods for chemical analysis of sodium fluoride - Part 10. Preparation and storage of samples YS/T 535.10-2009

3 method summary

Dissolve the sample with water, filter out insoluble matter, dry weighing.

4 instruments and equipment

4.1 General laboratory equipment. 4.2 glass filter crucible (G3). 4.3 blast oven. can control at 110 ℃ ± 8 ℃.

5 samples

The specimen shall comply with the requirements of 4.2 of YS/T 535.10-2009.

6 Analysis steps

6.1 samples 6.2 The number of measurements Independent of the two measurements, whichever is the average. 6.3 Determination 6.3.1 Place the sample (6.1) in a 400 mL beaker, add.200 mL of water, heat the solution to near boiling and hold for about 10 min, The solution was filtered through a glass filter crucible (4.2) by vacuum filtration (the crucible was previously dried at 110 ° C ± 5 ° C oven (4.3) for 2 h or more and dried After the equipment is cooled and weighed). The precipitate was washed four times with approximately 50 mL of water at approximately 80 ° C each. 6.3.2 The glass filter crucible was placed in an oven (4.3) and held at 110 ° C ± 5 ° C for 2 h. 6.3.3 Remove the crucible from the oven, place it in a drier, and cool it and weigh it. 6.3.4 Repeat heating, cooling and weighing until the difference between successive weighing is not more than 1mg. Note. The empty crucible and the crucible with the sample should have the same cooling time in the dryer.
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