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YS/T 36.3-2011 English PDF

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YS/T 36.3-2011: Methods for chemical analysis of high-purity Tin. Part 3: Determination of magnesium, aluminium, cadmium, iron, cobalt, nickle, copper, zinc, silver, indium, gold, lead and bismuth content. Inductively coupled plasma-mass spectrometry
Status: Valid

YS/T 36.3: Historical versions

Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
YS/T 36.3-2011259 Add to Cart 3 days Methods for chemical analysis of high-purity Tin. Part 3: Determination of magnesium, aluminium, cadmium, iron, cobalt, nickle, copper, zinc, silver, indium, gold, lead and bismuth content. Inductively coupled plasma-mass spectrometry Valid
YS/T 36.3-1992279 Add to Cart 3 days (Methods for chemical analysis of high purity tin Determination of cobalt, aluminum, zinc, silver, copper, indium, calcium, bismuth, nickel, gold, magnesium, lead, iron chemical spectroscopy) Obsolete

Similar standards

GB/T 3884.2   GB/T 3884.1   YS/T 252.1   YS/T 35   YS/T 36.2   YS/T 36.1   

Basic data

Standard ID: YS/T 36.3-2011 (YS/T36.3-2011)
Description (Translated English): Methods for chemical analysis of high-purity Tin. Part 3: Determination of magnesium, aluminium, cadmium, iron, cobalt, nickle, copper, zinc, silver, indium, gold, lead and bismuth content. Inductively coupled plasma-mass spectrometry
Sector / Industry: Nonferrous Metallurgy Industry Standard (Recommended)
Classification of Chinese Standard: H13
Classification of International Standard: 77.120.60
Word Count Estimation: 10,132
Date of Issue: 2011-12-20
Date of Implementation: 2012-07-01
Older Standard (superseded by this standard): YS/T 36.3-1992
Regulation (derived from): MIIT Announcement 2011 No.43
Issuing agency(ies): Ministry of Industry and Information Technology
Summary: This standard provides high-purity tin magnesium, aluminum, calcium, iron, cobalt, Nickel, copper, zinc, determination of bismuth content, silver, indium, gold, lead. This section applies to high-purity tin magnesium, aluminum, calcium, iron, cobalt, Nickel, copper, zinc, silver, indium, gold, Determination of bismuth content, lead. Measuring range of the elements listed in Table 1.

YS/T 36.3-2011: Methods for chemical analysis of high-purity Tin. Part 3: Determination of magnesium, aluminium, cadmium, iron, cobalt, nickle, copper, zinc, silver, indium, gold, lead and bismuth content. Inductively coupled plasma-mass spectrometry



---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Methods for chemical analysis of high-purity Tin.Part 3. Determination of magnesium, aluminium, cadmium, iron, cobalt, nickle, copper, zinc, silver, indium, gold, lead and bismuth content.Inductively coupled plasma- ICS 77.120.60 H13 People's Republic of China Nonferrous Metals Industry Standard Replacing YS/T 36.3-1992 Chemical analysis of high purity tin Part 3. magnesium, aluminum, calcium, iron, cobalt, nickel, copper, Determination of zinc, silver, indium, gold, lead and bismuth Inductively coupled plasma mass spectrometry Part 3. Determination of magnesium, aluminum, cadmium, iron, cobalt, nickle, copper, zinc, silver, indium, gold, leadandbismuthcontent- 2011-12-20 release.2012-07-01 implementation Issued by the Ministry of Industry and Information Technology of the People's Republic of China

Foreword

YS/T 36 "tin chemical analysis method" consists of three parts. - Part 1. Determination of arsenic - Arsenic method; - Part 2. Determination of antimony content - Malachite green spectrophotometric method; Part 3. Determination of magnesium, aluminum, calcium, iron, cobalt, nickel, copper, zinc, silver, indium, gold, lead and bismuth inductively coupled plasma mass spectrometry. This section is part 3 of YS/T 36. This part is drafted in accordance with the rules given in GB/T 1.1-2009. This part of the method of YS/T 36.3-1992 "high purity tin chemical analysis method of chemical spectroscopy determination of magnesium, aluminum, calcium, iron, cobalt, nickel, Zinc, silver, indium, gold, lead, bismuth ", and YS/T 36.3-1992 compared to the main changes are as follows. The method of determination is changed from chemical spectroscopy to inductively coupled plasma mass spectrometry. Extend the measurement range; - complements the precision, quality assurance and control terms; - Added the "test report" requirement. This part of the National Nonferrous Metals Standardization Technical Committee (SAC/TC243) proposed and centralized. This part is responsible for drafting unit. Zhuzhou Smelting Group Co., Ltd. This part involved in the drafting unit. Changsha Mining and Metallurgy Research Institute, Emei Semiconductor Materials Factory. This part of the drafters. Jin Zhihong, He Zongpu, Zhu Xiaofeng, statements, Gao Jing, Wen Ying, Liu Aihua. This part of the previous version of the standard to replace the release of the situation. --- YS/T 36.3-1992. Chemical analysis of high purity tin Part 3. magnesium, aluminum, calcium, iron, cobalt, nickel, copper, Determination of zinc, silver, indium, gold, lead and bismuth Inductively coupled plasma mass spectrometry WARNING - Personnel using this standard should have practical experience in formal laboratory work. This standard does not indicate all possible security questions question. It is the responsibility of the user to take appropriate safety and health measures and to ensure compliance with the conditions set forth in the relevant national regulations.

1 Scope

YS/T 36 This section specifies the determination of magnesium, aluminum, calcium, iron, cobalt, nickel, copper, zinc, silver, indium, gold, lead and bismuth in high purity tin. This part is suitable for the determination of magnesium, aluminum, calcium, iron, cobalt, nickel, copper, zinc, silver, indium, gold, lead and bismuth in high purity tin. The range of each element See Table 1. Table 1 Determination of each element Elemental determination range/× 10-4% Elemental determination range/× 10-4% Mg 0.001 to 1.0 Zn 0.002 to 1.0 Al 0.002 to 0.5 Ag 0.001 to 1.0 Ca 0.004 to 1.0 In 0.001 to 0.5 Fe 0.003 to 1.0 Au 0.001 to 0.3 Co 0.001 to 0.5 Pb 0.001 to 1.0 Ni 0.001 to 1.0 Bi 0.001 to 1.0 Cu 0.002 to 1.0

2 principle of the method

At about 100 ℃ temperature, tin and hydrogen chloride and chlorine mixed gas role, resulting in volatile tin tetrachloride and impurities separated. Residual The impurities were dissolved in wort, evaporated to dryness, dissolved in nitric acid and tested on ICP-MS.

3 reagent

Unless otherwise stated, reagents identified as superior grades and distilled water or deionized water or comparable purity are used in the analysis. Laboratory The utensils are thoroughly soaked in nitric acid solution (1 19) and thoroughly cleaned with water. 3.1 Potassium permanganate. 3.2 Hydrochloric acid (ρ = 1.19 g/mL). UP grade or equivalent purity. 3.3 nitric acid (ρ = 1.42g/mL). UP grade or equivalent purity.
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