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YS/T 281.20-2011 English PDF

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YS/T 281.20-2011: Mehtods for chemical analysis of cobalt. Part 20: Determination of oxide content. Impulse infrared absorption
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
YS/T 281.20-2011159 Add to Cart 3 days Mehtods for chemical analysis of cobalt. Part 20: Determination of oxide content. Impulse infrared absorption Valid

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YS/T 252.6   GB/T 3884.2   GB/T 3884.1   YS/T 281.12   YS/T 281.10   YS/T 281.11   

Basic data

Standard ID: YS/T 281.20-2011 (YS/T281.20-2011)
Description (Translated English): Mehtods for chemical analysis of cobalt. Part 20: Determination of oxide content. Impulse infrared absorption
Sector / Industry: Nonferrous Metallurgy Industry Standard (Recommended)
Classification of Chinese Standard: H13
Classification of International Standard: 77.120.70
Word Count Estimation: 6,691
Date of Issue: 2011-12-20
Date of Implementation: 2012-07-01
Regulation (derived from): ?MIIT Announcement 2011 No.43
Issuing agency(ies): Ministry of Industry and Information Technology
Summary: This standard specifies the method for measuring the oxygen content of cobalt. This section applies to the determination of oxygen content in the cobalt. Measuring range: 0. 2% to 1%.

YS/T 281.20-2011: Mehtods for chemical analysis of cobalt. Part 20: Determination of oxide content. Impulse infrared absorption


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Mehtods for chemical analysis of cobalt.Part 20. Determination of oxide content.Impulse infrared absorption ICS 77.120.70 H13 People's Republic of China Nonferrous Metals Industry Standard Cobalt chemical analysis method Part 20. determination of oxygen - pulse - infrared absorption method Part 20. Determination ofoxidecontent-Impulseinfraredabsorption 2011-12-20 release 2012-07-01 Implementation Issued by the Ministry of Industry and Information Technology of the People's Republic of China

Foreword

YS/T 281 "cobalt chemical analysis method" is divided into the following 20 parts. Part 1. Determination of iron content - Sulfosalicylic acid spectrophotometric method Part 2. Determination of aluminum content - Chromazu S spectrophotometric method Part 3. Determination of silicon content - Molybdenum blue spectrophotometric method Part 4. Determination of arsenic content - Molybdenum blue spectrophotometric method - Part 5. Determination of phosphorus content - Molybdenum blue spectrophotometric method Part 6. Determination of magnesium content - Flame atomic absorption spectrometric method - Part 7. Determination of zinc content - Flame atomic absorption spectrometric method Part 8. Determination of cadmium content - Flame atomic absorption spectrometric method Part 9. Determination of lead content - Flame atomic absorption spectrometric method Part 10. Determination of nickel content - Flame atomic absorption spectrometric method - Part 11. Determination of copper and manganese - Flame atomic absorption spectrometric method - Part 12. Determination of arsenic, antimony, bismuth, tin and lead - Electrothermal atomic absorption spectrometry - Part 13. Determination of sulfur content - High frequency induction furnace combustion infrared absorption method - Part 14. Determination of carbon content - High frequency induction furnace combustion infrared absorption method - Part 15. Determination of arsenic, antimony and bismuth - Hydride generation - atomic fluorescence spectrometry - Part 16. Determination of the amount of arsenic, cadmium, copper, zinc, lead, bismuth, tin, antimony, silicon, manganese, iron, nickel, aluminum and magnesium. Spectrum method - Part 17. Determination of aluminum, manganese, nickel, copper, zinc, cadmium, tin, antimony, lead and bismuth inductively coupled plasma mass spectrometry - Part 18. Determination of sodium content - Flame atomic absorption spectrometric method - Part 19. Determination of calcium, magnesium, manganese, iron, cadmium and zinc - Inductively coupled plasma emission spectrometric method - Part 20. Determination of the amount of oxygen - Infrared absorption method This part is part 20 of YS/T 281. This part is drafted in accordance with the rules given in GB/T 1.1-2009. This part of the National Nonferrous Metals Standardization Technical Committee (SAC/TC243) proposed and centralized. This standard is responsible for drafting units. Jinchuan Group Co., Ltd., Beijing Mining and Metallurgy Research Institute. This part is responsible for the drafting of the unit. Shenzhen Green US High-tech Co., Ltd. This part participates in the drafting unit. Jinchuan Group Co., Ltd., Beijing Nonferrous Metals Research Institute. This part of the main drafters. Liu Cong, Lv Qingcheng, Yan pear, Xu Kaihua, He Yunxiang, Zhou Haisheng, Song Xiaoli, Cao Zhenhua. Cobalt chemical analysis method Part 20. determination of oxygen - pulse - infrared absorption method WARNING. Personnel using this standard should have experience working in a regular laboratory. This standard does not indicate all possible security issues. Make It is the responsibility of the user to take appropriate safety and health measures and to ensure compliance with the conditions set forth in the relevant national regulations.

1 Scope

This part of YS/T 281 specifies the determination of oxygen content in cobalt. This part applies to the determination of oxygen in cobalt. Measuring range. 0.2% ~ 1%.

2 principle of the method

The preformed sample was put into a high temperature degassed graphite crucible, heated in an argon (or helium) gas stream, and the oxygen in the sample The CO is oxidized to CO2 by the precipitation of CO or with argon (or helium) through a rare earth oxidized copper furnace at 400 ° C and introduced into an infrared detector Determination, the computer automatically gives oxygen content.

3 reagents and materials

3.1 argon (or helium). (wAr/He ≥ 99.99%). 3.2 dynamic gas (nitrogen or compressed air). purity of about 99.8%. 3.3 Carbon tetrachloride. 3.4 Rare earth copper oxide. 3.5 anhydrous magnesium perchlorate. 3.6 Asbestos. 3.7 glass wool. 3.8 Vacuum grease. 3.9 graphite crucible. the crucible before use into the oven at 110 ℃ ± 5 ℃ baking 1h, then transferred to the dryer to cool to room temperature. 3.10 Nickel Foil. (wO < 0.0020%), scrub the surface of the nickel foil with a clean dyed carbon tetrachloride, cut into small pieces and put it into carbon tetrachloride Soak for about 15min; use, with a hair dryer to dry, so that attached to the nickel foil surface of carbon tetrachloride completely volatile. 3.11 Oxygen Standard Samples. Use standard samples similar to the oxygen content of the substance to be measured. It is best to use a standard sample of cobalt in cobalt.

4 instruments

Pulse heating infrared absorber. with electronic AC voltage regulator. The instrument should meet the following criteria, the use of working conditions to ensure that the oxygen in the sample completely released. --- Instrument sensitivity ≤ 0.0010%; --- pulse heating power of not less than 6.5kW (furnace temperature of not less than 2400 ℃); --- system blank ≤ 0.0010%.
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