YS/T 1158.1-2016 English PDFUS$139.00 · In stock
Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. YS/T 1158.1-2016: Methods for chemical analysis of copper-indium-gallium-selenide target—Part 1: Determination of gallium, indium contents—Inductively coupled plasma atomic emission spectrometry Status: Valid
Basic dataStandard ID: YS/T 1158.1-2016 (YS/T1158.1-2016)Description (Translated English): Methods for chemical analysis of copper-indium-gallium-selenide target��Part 1: Determination of gallium, indium contents��Inductively coupled plasma atomic emission spectrometry Sector / Industry: Nonferrous Metallurgy Industry Standard (Recommended) Classification of Chinese Standard: H13 Classification of International Standard: 77.120.30 Word Count Estimation: 6,657 Date of Issue: 2016-07-11 Date of Implementation: 2017-01-01 Regulation (derived from): Notice of the Ministry of Industry and Information Technology (2016 No. 37) Issuing agency(ies): Ministry of Industry and Information Technology Summary: This standard specifies the method for determining the amount of gallium and indium in a copper indium gallium selenide target. All weighing results in this standard are in g and accurate to 0.0001g. YS/T 1158.1-2016: Methods for chemical analysis of copper-indium-gallium-selenide target—Part 1: Determination of gallium, indium contents—Inductively coupled plasma atomic emission spectrometry---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order. Methods for chemical analysis of copper-indium-gallium-selenide target-Part 1. Determination of gallium, indium contents-Inductively coupled plasma atomic emission spectrometry ICS 77.120.30 H13 People's Republic of China non-ferrous metal industry standards CIGS target chemical analysis method Part 1. Determination of gallium content and indium content Inductively coupled plasma atomic emission spectrometry Methods for chemical analysis of copper-indium-galium-selenide target Part 1.Determinationofgalium, indiumcontents 2016-07-11 released 2017-01-01 implementation Ministry of Industry and Information Technology of the People's Republic of China ForewordYS/T 1158 "CIGS target chemical analysis method" is divided into the following three parts. --- Part 1. Determination of gallium content and indium content Inductively coupled plasma atomic emission spectrometry; --- Part 2. Determination of selenium content by weight method; --- Part 3. Determination of aluminum, iron, nickel, chromium, manganese, lead, zinc, cadmium, cobalt, molybdenum, barium, magnesium content Inductively coupled plasma mass spectrometry. This part of YS/T 1158 Part 1. This section drafted in accordance with GB/T 1.1-2009 given rules. This part of the National Non-ferrous Metals Standardization Technical Committee (SAC/TC243) and focal point. The main drafting unit of this section. Guangxi Zhuang Autonomous Region Metallurgical Product Quality Supervision and Inspection Station, Guangxi Zhuang Autonomous Region, Analysis and Testing Research center. Participated in the drafting of this section. Liuzhou Centenary Advanced Materials Co., Ltd., Qingyuan Pilot Materials Co., Ltd., Guilin University of Technology, Guangzhou Nonferrous Metal Research Institute. The main drafters of this section. Liu Shuting, Chen Jinzhong, Wei Li, Jiang Tiancheng, Huang Zhaomin, Zhou Su Lian, Xiong Xiaoyan, Deng Yuning, Li Feng, Nie Xiaoming, Huang Mengchuan, Wu Xiangwu, Liu Zebin, Zhuang Ai-chun, Wei Shenglin. CIGS target chemical analysis method Part 1. Determination of gallium content and indium content Inductively coupled plasma atomic emission spectrometry1 ScopeYS/T 1158 provisions of this part of the CIGS target gallium content and amount of indium determination. This section applies to the determination of copper and indium gallium selenide target gallium content and indium content. The measurement range is 1.00% ~ 13.00% of gallium, 10.00% of indium ~ 30.00%. All weighing results in this section are in grams (g) and accurate to 0.0001g.2 method summaryAfter the sample was nitric acid, hydrochloric acid dissolved, with yttrium as the internal standard solution, using inductively coupled plasma atomic emission spectrometry Determination of the sample solution The intensity of the characteristic spectrum of the element to be measured, the amount of gallium in the sample and the amount of indium were calculated by the internal standard curve method.3 reagentUnless otherwise stated, only reagents that are identified as analytically pure and secondary water are used in the analysis. 3.1 Hydrochloric acid (p = 1.19 g/mL). 3.2 Nitric acid (p = 1.42 g/mL). 3.3 Hydrochloric acid (2 1). 3.4 Nitric acid (2 1). 3.5 gallium standard stock solution Weigh 0.30g metal gallium (wGa ≥ 99.99%, W1) in 150mL beaker, add 10mL nitric acid (3.4), 5mL hydrochloric acid (3.3), covered with a watch glass, low temperature heating until completely dissolved, removed, cooled to room temperature, transferred to pre-weighed 100mL dry volumetric flask, the water diluted to the mark, weighing, the volume of the solution after the volume of W2, shake. This solution 1g contains (W1/W2) g gallium. 3.6 indium standard storage solution Weigh 1.0g of indium metal (wIn ≥ 99.99%, W3) in a 150mL beaker, add 10mL of nitric acid (3.4), 5mL hydrochloric acid (3.1), covered with a watch glass, low temperature heating until completely dissolved, removed, cooled to room temperature, transferred to the pre-weighed 100mL dry volumetric flask, diluted with water to the mark, weighing, the volume of the solution after the volume of W4, shake. This solution 1g contains (W3/W4) g indium. 3.7 gallium standard solution Weigh the gallium standard stock solution (3.5) 10.0g (W5) Weigh into a pre-weighed 100mL dry volumetric flask, add 5mL nitric acid (3.4), 2mL hydrochloric acid (3.3), diluted with water to the mark, weighing, the volume of the solution after the volume of W6, shake. This solution contains 1g (W5 · W1)/(W6 · W2) g gallium. 3.8 Indium standard solution Weigh in indium standard stock solution (3.6) 10.0g (W7) to the weighed 100mL dry volumetric flask, add 5mL nitric acid (3.4), 2mL hydrochloric acid (3.3), diluted with water to the mark, weighing, the volume of the solution after the volume of W8, shake. This solution contains 1g (W7 · W3)/(W8 · W4) g indium. 3.9 yttrium internal standard solution Weigh 1.2699g yttrium oxide (wY2O3 ≥ 99.99%, after pre-burning at 1000 ℃ 1h, placed in a dry Cooled to room temperature), placed in 300mL beaker, added 30mL hydrochloric acid (3.3), heated to dissolve, removed to cool to room temperature, into 1000mL volumetric flask, diluted with water to the mark, shake. 1 mL of this solution contains 1 mg of yttrium. ......Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of YS/T 1158.1-2016_English be delivered?Answer: Upon your order, we will start to translate YS/T 1158.1-2016_English as soon as possible, and keep you informed of the progress. The lead time is typically 1 ~ 3 working days. The lengthier the document the longer the lead time.Question 2: Can I share the purchased PDF of YS/T 1158.1-2016_English with my colleagues?Answer: Yes. 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