YS/T 1046.5-2015 English PDFUS$139.00 · In stock
Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. YS/T 1046.5-2015: Methods for chemical analysis of copper slag concentrates. Part 5: Determination of silicon dioxide content. Potassium fluosilicate titration method Status: Valid
Basic dataStandard ID: YS/T 1046.5-2015 (YS/T1046.5-2015)Description (Translated English): Methods for chemical analysis of copper slag concentrates. Part 5: Determination of silicon dioxide content. Potassium fluosilicate titration method Sector / Industry: Nonferrous Metallurgy Industry Standard (Recommended) Classification of Chinese Standard: H13 Classification of International Standard: 77.120.60 Word Count Estimation: 6,678 Date of Issue: 2015-04-30 Date of Implementation: 2015-10-01 Regulation (derived from): Ministry of Industry and Information Technology Announcement (2015 No. 28) Issuing agency(ies): Ministry of Industry and Information Technology Summary: This standard specifies the determination of silica content in copper slag concentrates. This standard is applicable to the determination of binary silicon content in the concentrate. The determination range is 8.00% ~ 25.00%. YS/T 1046.5-2015: Methods for chemical analysis of copper slag concentrates. Part 5: Determination of silicon dioxide content. Potassium fluosilicate titration method---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order. Methods for chemical analysis of copper slag concentrates - Part 5. Determination of silicon dioxide content-Potassium fluosilicate titration method ICS 77.120.60 H13 People's Republic of China Nonferrous Metals Industry Standard Methods for chemical analysis of copper concentrates Slag Part 5. Determination of the amount of silica Silicon potassium fluoride titration Part 5. Determinationofsilicondioxidecontent- Issued on. 2015-04-30 2015-10-01 implementation Ministry of Industry and Information Technology of the People's Republic of China released ForewordYS/T 1046-2015 "copper slag concentrates chemical analysis method" is divided into seven sections. --- Part 1. Determination of copper content iodometry; --- Part 2. Determination of gold and silver atomic absorption spectroscopy and fire assay gravimetric method; --- Part 3. Determination of sulfur content of combustion titration method; --- Part 4. Determination of iron content dichromate method; --- Part 5. Determination of the amount of silica silicon potassium fluoride titration; --- Part 6. aluminum oxide content - Inductively coupled plasma atomic emission spectrometry; --- Part 7. arsenic, antimony, bismuth, lead, zinc, magnesium oxide content - Inductively coupled plasma atomic emission spectrometry. This is Part 5. This section drafted in accordance with GB/T 1.1-2009 given rules. The non-ferrous metal part by the National Standardization Technical Committee (SAC/TC243) centralized. This section is responsible for drafting unit. Daye Nonferrous Metals Group Holdings Limited, Zhongtiaoshan Nonferrous Metals Group Co., Ltd. This section is drafted. Zhongtiaoshan Nonferrous Metals Group Co., Ltd. It participated in the drafting of this section. Tongling Nonferrous Metals Group Holdings Limited, Daye Nonferrous Metals Group Holdings Co., Ltd., Beijing Mine Metallurgical Research Institute, Shandong constant state Smelting Company. The main drafters of this section. Dong Xiaolin, Zhang Guanghua, Ma Lijun, Li Hongying, Wang Jinping, Ye Xin, Hujun Kai, Chen Lan, Wang Yongbin, Su spring, Li Ting, Hang Zhou, Magofuku red, Zhang Yanfeng. Methods for chemical analysis of copper concentrates Slag Part 5. Determination of the amount of silica Silicon potassium fluoride titration1 ScopeThis section YS/T 1046 specifies the method for determination of copper slag concentrate silica content. This section applies to the determination of copper slag concentrate silica content. Measurement range of 8.00% - 25.00%.2 Method summarySample with a base melted with hot water extraction, after acidification, in strongly acidic solution was added potassium chloride and potassium fluoride and silicate ions formed fluorosilicone The precipitate potassium fluoride potassium silicate material amount of hydrolysis, precipitation of hydrofluoric acid in hot water with phenolphthalein as an indicator, sodium hydroxide standard titration solution Titration, calculate the mass fraction of silica based on the volume of sodium hydroxide standard titration solution consumed.3 ReagentsUnless otherwise indicated in the analysis using only recognized as analytical grade reagents and distilled or deionized water or equivalent purity. 3.1 sodium hydroxide. 3.2 sodium peroxide. 3.3 potassium hydroxide. 3.4 potassium chloride. Before potassium hydrogen phthalate 3.5, the benchmark reagents, used in 105 ℃ ~ 110 ℃ drying to constant weight. 3.6 hydrochloric acid (ρ = 1.19g/mL). 3.7 hydrochloride (11). 3.8 nitric acid (ρ = 1.42g/mL). 3.9 potassium fluoride solution (200g/L). Weigh 100g of potassium fluoride were dissolved in 300mL of water, 100mL added nitric acid (3.8), potassium chloride (3.4) to saturation, diluted with water to 500mL, mix, 30min dry filter in a plastic bottle aside. 3.10 Potassium chloride - ethanol washing solution. Weigh 250g of potassium chloride (3.4) was dissolved in 3000mL of water, was added 1000mL of ethanol, diluted with water To 5000mL, and mix, adding 1mL phenolphthalein ethanol solution (3.14), with sodium hydroxide solution (3.13.2) and to the solution was slightly red. 3.11 potassium chloride - ethanol solution. Weigh 5g of potassium chloride (3.4) was dissolved in 50mL of water was added 50mL of ethanol, and mix. 3.12 potassium sodium tartrate solution (10g/L). Weigh 10g of potassium sodium tartrate was dissolved in 1L of water, add 5 drops of phenolphthalein ethanol solution after boiling (3.14), sodium hydroxide solution (3.13.2) and to the solution was slightly red. 3.13 sodium hydroxide solution. 3.13.1 Storage standard sodium hydroxide solution. Weigh 110g of sodium hydroxide (3.1) dissolved in 100mL of carbon dioxide-free water, mix, into poly Ethylene container, sealed place until the solution clear. 3.13.2 sodium hydroxide solution [c (NaOH) ≈0.2mol/L]. plastic measuring cylinder 11mL sodium hydroxide standard stock solution (3.13.1) The supernatant was diluted to 1L with carbon dioxide-free water, and mix. ......Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of YS/T 1046.5-2015_English be delivered?Answer: Upon your order, we will start to translate YS/T 1046.5-2015_English as soon as possible, and keep you informed of the progress. The lead time is typically 1 ~ 3 working days. 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