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YS/T 1014.1-2014 English PDF

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YS/T 1014.1-2014: Methods for chemical analysis of bismuth trioxide. Part 1: Determination of bismuth trioxide content. Na2 EDTA titrimetric method
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
YS/T 1014.1-2014159 Add to Cart 3 days Methods for chemical analysis of bismuth trioxide. Part 1: Determination of bismuth trioxide content. Na2 EDTA titrimetric method Valid

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Basic data

Standard ID: YS/T 1014.1-2014 (YS/T1014.1-2014)
Description (Translated English): Methods for chemical analysis of bismuth trioxide. Part 1: Determination of bismuth trioxide content. Na2 EDTA titrimetric method
Sector / Industry: Nonferrous Metallurgy Industry Standard (Recommended)
Classification of Chinese Standard: H13
Classification of International Standard: 77.120.99
Word Count Estimation: 6,623
Date of Issue: 10/14/2014
Date of Implementation: 4/1/2015
Regulation (derived from): People's Republic of China Ministry of Industry and Information Technology Notice 2014 No. 63; Industry Standard Filing Notice 2014 No. 12 (Overall No. 180)
Issuing agency(ies): Ministry of Industry and Information Technology
Summary: This Standard specifies the method for determination of bismuth trioxide bismuth oxide content. This section applies to the determination of bismuth trioxide bismuth trioxide amount measuring range: �� 98.0%.

YS/T 1014.1-2014: Methods for chemical analysis of bismuth trioxide. Part 1: Determination of bismuth trioxide content. Na2 EDTA titrimetric method


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Methods for chemical analysis of bismuth trioxide Part 1. Determination of bismuth trioxide content Na2 EDTA titrimetric method ICS 77.120.99 H13 People's Republic of China Nonferrous Metals Industry Standard Bismuth oxide chemical analysis Part 1. bismuth trioxide contents - Na2EDTA titration Part 1. Determinationofbismuthtrioxidecontent- Issued on. 2014-10-14 2015-04-01 implementation Ministry of Industry and Information Technology of the People's Republic of China released

Foreword

YS/T 1014 "Methods for chemical analysis of bismuth trioxide" is divided into five sections. --- Part 1. bismuth trioxide contents - Na2EDTA titration; --- Part 2. silver, copper, magnesium, nickel, cobalt, manganese, calcium, iron, cadmium, lead, zinc, antimony, aluminum, sodium, sulfur content - Inductively coupled plasma Atomic emission spectrometry; --- Part 3. Determination of chlorine content of silver chloride turbidimetry; --- Part 4. loss on ignition - Gravimetric method; --- Part 5. moisture content - Gravimetric method. This section YS/T 1014 Part 1. This section drafted in accordance with GB/T 1.1-2009 given rules. The non-ferrous metal part by the National Standardization Technical Committee (SAC/TC243) centralized. This section is responsible for drafting unit. Zhuzhou Smelter Group Co., Ltd. Guangdong pilot dilute material. Participated in the drafting of this section. Guangzhou Nonferrous Metal Research Institute, Henan Yuguang Gold & Lead Co., Ltd., Hunan Nonferrous Metal Research Institute. The main drafters of this section. Jiang Qing, to De Lei, Dai Fengying, Xie Hui, Kong Jianmin, Zhou Junling, Zhu Chan Fang, Wang Kaikai, Juan, Pang Wenlin. Bismuth oxide chemical analysis Part 1. bismuth trioxide contents - Na2EDTA titration

1 Scope

YS/T 1014 This section specifies the method for determination of bismuth trioxide in the amount of bismuth trioxide. This section applies to the determination of bismuth trioxide bismuth trioxide amount measurement range. ≥98.0%.

2 Method summary

Sample dissolved in nitric acid, sodium acetate to adjust the pH value between 1.5 to 1.7, with xylenol orange as indicator, with standard Na2EDTA Titration titration solution, measured the amount of bismuth trioxide.

3 Reagents

Unless otherwise indicated in the analysis using only recognized as analytical grade reagents and distilled or deionized water or equivalent purity. 3.1 ascorbic acid. 3.2 nitric acid (ρ = 1.42g/mL). 3.3 nitric acid (595). 3.4 thiourea saturated solution. 3.5 tartaric acid solution (200g/L). 3.6 Anhydrous sodium acetate (200g/L). 3.7 Na2EDTA Standard Solution (about 0.020mol/L). 3.7.1 preparation. Weigh 7.60g disodium edetate in 300mL beaker, add water, heat gently to dissolve, cooled to room temperature and transferred to 1000mL volumetric flask, dilute to the mark, mix, place three days after calibration. 3.7.2 Calibration. Weigh 0.197g bismuth (wBi≥99.99%) (accurate to 0.0001g) 5 parts were placed in 500mL beaker triangle , The tartaric acid solution is added 5.0mL (3.5), was added 10mL of nitric acid (3.2), a low temperature around completely dissolved by heating, and evaporated to 5mL, taking Under rinsed with water and dish table Beibi, ascorbic acid was added 0.5g (3.1), 5.0mL saturated solution of thiourea (3.4), 100mL water and shake. With The same below 6.4.2. Along with the calibration blank test. According to equation (1) to calculate the actual concentration Na2EDTA standard titration solution. c = 1000 × m0 (V1-V0) × 208.98 (1) Where. The actual concentration c --- Na2EDTA standard titration solution, expressed in moles per liter (mol/L); m0 --- saying that the quality of the calibration to take bismuth, in grams (g); --- Bismuth molar mass of 208.98 units of grams per mole (g/mol); When V1 --- calibration volume Na2EDTA standard titration titration solution consumed bismuth solution in milliliters (mL); V0 --- the calibration, volume Na2EDTA standard titration solution consumed in the blank titration solution in milliliters (mL).
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