SN/T 3856-2014 English PDFUS$629.00 · In stock
Delivery: <= 5 days. True-PDF full-copy in English will be manually translated and delivered via email. SN/T 3856-2014: Determination of ethoxyquin residue in food for export Status: Valid
Basic dataStandard ID: SN/T 3856-2014 (SN/T3856-2014)Description (Translated English): Determination of ethoxyquin residue in food for export Sector / Industry: Commodity Inspection Standard (Recommended) Classification of Chinese Standard: X04 Classification of International Standard: 67.050 Word Count Estimation: 24,277 Quoted Standard: GB/T 6682 Regulation (derived from): AQSIQ notification issued in 2014 on the first batch of 230 industry-standard entry-exit inspection and quarantine Issuing agency(ies): General Administration of Customs Summary: This Standard specifies the liquid chromatography and gas chromatography foods ethoxyquin residues - mass spectrometry methods. This Standard applies to pork, shrimp, eggs, liver, pears, cabbage, tomatoes, chili powder in food ethoxy quinoline residues me SN/T 3856-2014: Determination of ethoxyquin residue in food for export---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.Determination of ethoxyquin residue in food for export People's Republic of China Entry-Exit Inspection and Quarantine Standards Determination of Ethoxyquin residues in food exports Issued on. 2014-01-13 2014-08-01 implementation People's Republic of China The State Administration of Quality Supervision, Inspection and Quarantine released ForewordThis standard was drafted in accordance with GB/T 1.1-2009 given rules. Please note that some of the content of this document may involve patents. Distribution of this document Institutions do not assume the responsibility to identify these patents. This standard is proposed and managed by the National Certification and Accreditation Administration Committee. This standard was drafted. Chongqing, People's Republic of China Exit Inspection and Quarantine, Chongqing Import and Export Food Safety Engineering Technology center. The main drafters of this standard. Zhengguo Can, Peng Guangyu, Lixian Liang, Cao Shurui, Tang Bobin, Wang Jing, Liu Yi, Wang Guomin. Determination of Ethoxyquin residues in food exports1 ScopeThis standard specifies the liquid chromatography and gas chromatography in food ethoxyquin residues - mass spectrometry methods. This standard applies to quinoline ethoxy residues in pork, shrimp, eggs, liver, pears, cabbage, tomatoes, chili powder in food Determination And confirmation.2 Normative referencesThe following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein Member. For undated references, the latest edition (including any amendments) applies to this document. Laboratory use specifications and test methods GB/T 6682 Analysis The first gas chromatography - mass spectrometry3 Method summarySample of ethoxyquin residue extracted with hexane, the pH adjusted liquid-liquid extraction purification and nitrogen blow was concentrated to dryness, normal hexane, with Gas chromatography mass spectrometer (GC-MS) was measured, quantified by external standard peak area.4 Reagents and materialsUnless otherwise specified, the reagents were of analytical grade water as a water GB/T 6682 regulations. 4.1 hexane. chromatographically pure. 4.2 Methanol. chromatographically pure. 4.3 sodium carbonate. 4.4 anhydrous sodium. 650 ℃ burning 4h, cooled in a desiccator to room temperature and stored in a sealed bottle aside. 4.5 hydrochloric acid. 4.6 sodium hydroxide. 4.7 0.5mol/L hydrochloric acid solution. take about 42mL hydrochloric acid (4.5) diluted with water to 1000mL. 4.8 5mol/L sodium hydroxide solution. Take 20g sodium hydroxide (4.6) dissolved in water and dilute to 100mL. 4.9 Ethoxyquin standard substance. C14H19NO, purity ≥98%, CAS. 91-53-2. 4.10 standard stock solution. accurately weighed 0.01g (accurate to 0.1mg) Ethoxyquin standard in 100mL flask with n-hexane Dissolve and dilute to the mark, formulated at a concentration of 100mg/L standard stock solution, and this solution was stored at -18 ℃ under dark. 4.11 intermediate standard solution. precise amount of 10mL standard stock solution (4.10) in 100mL flask, dissolve and dilute with n-hexane To the mark, formulated at a concentration of 10ms/L standard stock solution, and this solution was stored at -18 ℃ under dark. 4.12 standard solution. take the right amount of all kinds of stock solution, with n-hexane formulated into an appropriate concentration of the standard working solution, standard working solution It was stored at -18 ℃ under dark. ......Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of SN/T 3856-2014_English be delivered?Answer: Upon your order, we will start to translate SN/T 3856-2014_English as soon as possible, and keep you informed of the progress. 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