SN/T 3147-2017 English PDF

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SN/T 3147-2017: Determination of phthalate esters(PAEs) in foodstuffs for export
Status: Valid

SN/T 3147: Historical versions

Standard ID	USD	BUY PDF	Lead-Days	Standard Title (Description)	Status
SN/T 3147-2017	859	Add to Cart	6 days	Determination of phthalate esters(PAEs) in foodstuffs for export	Valid
SN/T 3147-2012	RFQ	ASK	7 days	Determination of phthalate esters (PAEs) in food for export	Obsolete

Similar standards

GB 5009.22   NY/T 2334   SN/T 2641   SN/T 3142   SN/T 3146   SN/T 3137   

Basic data

Standard ID: SN/T 3147-2017 (SN/T3147-2017)
Description (Translated English): Determination of phthalate esters(PAEs) in foodstuffs for export
Sector / Industry: Commodity Inspection Standard (Recommended)
Classification of Chinese Standard: X04
Classification of International Standard: 67.050
Word Count Estimation: 37,393
Date of Issue: 2017-05-12
Date of Implementation: 2017-12-01
Older Standard (superseded by this standard): SN/T 3147-2012
Quoted Standard: GB/T 6682
Regulation (derived from): State-Quality-Inspection-Accreditation (2017) 228
Issuing agency(ies): General Administration of Customs
Summary: This standard specifies dimethyl phthalate, diethyl phthalate, diisopropyl phthalate, diallyl phthalate, dipropyl phthalate, ortho-benzene. Diisobutyl phthalate, dibutyl phthalate, di(2-methoxy)ethyl phthalate, diisoamyl phthalate, di(4-methyl-phthalate) 2-pentyl)ester, di(2-ethoxy)ethyl phthalate, diamyl phthalate, dihexyl phthalate, butyl benzyl phthalate, ortho-benzene Di(2-butoxy)ethyl dicarboxylate, dicyclohexyl phthalate, di(2-ethyl)hexyl phthalate, diheptyl phthalate, diphenyl phthalate Ester, di-n-octyl phthalate, diisononyl phthalate, diisononyl phthalate, adjacent

SN/T 3147-2017: Determination of phthalate esters(PAEs) in foodstuffs for export

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of phthalate esters (PAEs) in foodstuffs for export People's Republic of China entry and exit inspection and quarantine industry standards Replace SN/T 3147-2012 Method for determination of phthalates in foods for export Released on.2017-05-12 2017-12-01 implementation People's Republic The General Administration of Quality Supervision, Inspection and Quarantine issued

Foreword

This standard was drafted in accordance with the rules given in GB/T 1.1-2009. This standard replaces SN/T 3147-2012 "Determination of Phthalates in Exported Foods". The main technical changes of this standard compared with SN/T 3147-2012 are as follows. --- The applicable matrix for the detection range is extended to alcohol, liquid beverages, solid beverages, jams, jellies, condiments, flavors, oils and fats. Food, dairy products, starch products, olive oil and pastries; --- The detection range increases diisooctyl phthalate; --- Increased pretreatment methods for alcohol samples; --- Revised the pretreatment method for some samples; --- The quantitative limit and recovery of 24 phthalates in alcoholic matrices and diisooctyl phthalate in other matrices are given. Please note that some of the contents of this document may involve patents. The issuing organization of this document is not responsible for identifying these patents. This standard is proposed and managed by the National Certification and Accreditation Administration. This standard was drafted. Xiamen Entry-Exit Inspection and Quarantine Bureau of the People's Republic of China, Hunan Provincial Institute of Inspection and Quarantine, Chinese People Shanghai Entry-Exit Inspection and Quarantine Bureau of the Republic, Shenzhen Entry-Exit Inspection and Quarantine Bureau of the People's Republic of China, Fujian Provincial Product Quality Inspection Institute, Fujian Entry-Exit Inspection and Quarantine Bureau of the People's Republic of China. The main drafters of this standard. Wu Min, Zheng Xianghua, Lin Liyi, Chen Luxing, Fang Enhua, Wang Danhong, Chen Yan, Huang Zhiqiang, Yue Zhenfeng, Deng Xiaojun, Huang Yonghui. The previous versions of the standards replaced by this standard are. ---SN/T 3147-2012. Method for determination of phthalates in foods for export

1 Scope

This standard specifies dimethyl phthalate, diethyl phthalate, diisopropyl phthalate, phthalic acid Allyl ester, dipropyl phthalate, diisobutyl phthalate, dibutyl phthalate, di(2-methoxy)ethyl phthalate, Diisoamyl phthalate, bis(4-methyl-2-pentyl) phthalate, di(2-ethoxy)ethyl phthalate, phthalic acid Dipentyl ester, dihexyl phthalate, butyl benzyl phthalate, di(2-butoxy)ethyl phthalate, biphenyl phthalate Hexyl ester, di(2-ethyl)hexyl phthalate, diheptyl phthalate, diphenyl phthalate, di-n-octyl phthalate, ortho-benzene Determination of diisononyl dicarboxylate, diisononyl phthalate, dinonyl phthalate and diisooctyl phthalate by gas chromatography-mass spectrometry Method and liquid chromatography-mass spectrometry/mass spectrometry detection method. This standard applies to alcohol, liquid beverages, solid beverages, jams, jellies, condiments, flavors and fragrances, dairy products, starch products, olives Determination and confirmation of 24 phthalate esters such as dimethyl phthalate in oils and cakes.

2 Normative references

The following documents are indispensable for the application of this document. For dated references, only the dated version applies to this article. Pieces. For undated references, the latest edition (including all amendments) applies to this document. GB/T 6682 Analytical laboratory water specifications and test methods First gas chromatography-mass spectrometry

3 method summary

The phthalate compound in food is purified by n-hexane or acetonitrile, liquid-liquid extraction or solid phase extraction, and then subjected to gas chromatography. The spectrometer was used for the measurement. The characteristic selection ion monitoring scanning mode (SIM) was used, and the external standard method was used for quantification.

4 reagents and materials

All reagents are of analytical grade unless otherwise specified. Water is a first grade water in accordance with GB/T 6682 (stored in glass bottles to avoid Contact plastic) 4.1 n-hexane. chromatographically pure. 4.2 Acetonitrile. Chromatographically pure. 4.3 Methanol. Chromatographically pure. 4.4 Acetone. chromatographically pure. 4.5 Sodium chloride. 4.6 Magnesium Sulfate. Chromatographically pure. 4.7 Sodium acetate. chromatographically pure. 4.8 5% methanol solution. Measure 5 mL of methanol, mix with water and make up 100 mL, and set aside. 4.9 Standards. See Table A.1 in Appendix A for details. 4.10 Standard stock solution. Weigh the appropriate amount of the above various standards (accurate to 0.1mg) and prepare 1000mg/L of storage with n-hexane. ......

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