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SN/T 1572-2005 English PDF

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SN/T 1572-2005: Inspection of fumonisins in cereals and feedstuffs for import and export. Liquid chromatographic method
Status: Obsolete
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
SN/T 1572-2005679 Add to Cart 3 days Inspection of fumonisins in cereals and feedstuffs for import and export. Liquid chromatographic method Obsolete

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Basic data

Standard ID: SN/T 1572-2005 (SN/T1572-2005)
Description (Translated English): Inspection of fumonisins in cereals and feedstuffs for import and export. Liquid chromatographic method
Sector / Industry: Commodity Inspection Standard (Recommended)
Classification of Chinese Standard: B22;B46
Classification of International Standard: 67.060; 65.120
Word Count Estimation: 17,115
Date of Issue: 2005-05-20
Date of Implementation: 2005-12-01
Quoted Standard: SN/T 0800.1-1999
Regulation (derived from): 2005 Bulletin No. 8 industry standard
Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of the People Republic of China
Summary: This standard specifies the import and export of cereals, fodder fumonisins B1, B2 inspection sampling, sample preparation and liquid chromatography detection methods. This standard applies to import corn and corn fodder fumonisins B1, B2 test.

SN/T 1572-2005: Inspection of fumonisins in cereals and feedstuffs for import and export. Liquid chromatographic method


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Inspection of fumonisins in cereals and feedstuffs for import and export.Liquid chromatographic method Book of the People's Republic of China Entry and Exit Inspection and Quarantine Method for testing fumonisin in import and export grain and feed Liquid chromatography Released on.2005-05-20 Implementation of.2005-12-01 People's Republic The General Administration of Quality Supervision, Inspection and Quarantine issued

Foreword

Appendix A of this standard is an informative annex. This standard is proposed and managed by the National Certification and Accreditation Administration. This standard was drafted. Liaoning Entry-Exit Inspection and Quarantine Bureau of the People's Republic of China, Jilin Province Entry and Exit Inspection Epidemic situation. The main drafters of this standard. Lin Weixuan, Tian Miao, Yan Jun, Zhao Wei, Guo Lan, Shang Minglei, Cao Dongmei. This standard is the first industry standard for entry-exit inspection and quarantine. Method for testing fumonisin in import and export grain and feed Liquid chromatography

1 Scope

This standard specifies the sampling, sample preparation and liquid chromatographic detection methods for the detection of fumonisin B1 and B2 in grain, grain and feed. This standard applies to the testing of fumonisins B1 and B2 in import and export corn and corn feed.

2 Normative references

The terms in the following documents become the terms of this standard by reference in this standard. Any dated reference document, followed by Some amendments (not including errata content) or revisions do not apply to this standard. Parties using this standard should study the following standards. The possibility of the latest version. For undated references, the latest edition applies to this standard. SN/T 0800.1-1999 Import and export grain and oil, feed inspection sampling and sample preparation methods

3 sampling and sample preparation

Execute according to SN/T 0800.1. Samples must be protected from contamination or fumonisin levels during sampling and sample preparation. Variety.

4 Determination method

4.1 Method summary The sample is extracted with methanol + water, purified by FumoniTest immunoaffinity column or SAX strong anion solid phase extraction column, derivatized, used Reversed-phase liquid chromatography column separation, fluorescence detector detection, external standard method for quantification. 4.2 Reagents and materials 4.2.1 Water. Ultrapure water. 4.2.2 Methanol. Chromatographically pure. 4.2.3 Acetonitrile. chromatographically pure. 4.2.4 Acetic acid. excellent grade pure. 4.2.5 Phosphoric acid. excellent grade pure. 4.2.6 Hydrochloric acid. excellent grade pure. 4.2.7 Sodium dihydrogen phosphate. analytically pure. 4.2.8 Disodium hydrogen phosphate. analytically pure. 4.2.9 Potassium dihydrogen phosphate. analytically pure. 4.2.10 Sodium chloride. analytically pure. 4.2.11 Potassium chloride. analytically pure. 4.2.12 Sodium hydroxide. analytically pure. 4.2.13 Sodium tetraborate. excellent grade pure. 4.2.14 Mercaptoethanol. excellent grade pure. 4.2.15 O-phthalaldehyde. excellent grade pure. 4.2.16 Methanol + water (1+1). 4.2.17 Methanol + water (3+1).
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