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SB/T 10405-2006 English PDF

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SB/T 10405-2006: Methods for wet ashing procedures for preparing wood for chemical analysis
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
SB/T 10405-2006229 Add to Cart 3 days Methods for wet ashing procedures for preparing wood for chemical analysis Valid

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Basic data

Standard ID: SB/T 10405-2006 (SB/T10405-2006)
Description (Translated English): Methods for wet ashing procedures for preparing wood for chemical analysis
Sector / Industry: Domestic Trade Industry Standard (Recommended)
Classification of Chinese Standard: B71
Classification of International Standard: 71.100.50
Word Count Estimation: 7,786
Date of Issue: 2006-05-12
Date of Implementation: 2006-12-01
Quoted Standard: GB/T 1933
Regulation (derived from): ?Industry Standard Announcement 2006 No.8 (Total No.80)
Issuing agency(ies): Ministry of Commerce of the People's Republic of China
Summary: This standard specifies the technical material preservative wet ashing of the two methods. This standard applies to the analysis of arsenic in wood preservative surgery, pre-treatment levels of phosphates and other ingredients, Ming, copper.

SB/T 10405-2006: Methods for wet ashing procedures for preparing wood for chemical analysis

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Methods for wet ashing procedures for preparing wood for chemical analysis ICS 71.100.50 B71 Record number. 17960-2006 People's Republic of China domestic trade industry standard Wet ashing method before chemical analysis of preservative wood Released on.2006-05-12 Implementation of.2006-12-01 Published by the Ministry of Commerce

Content

Foreword I 1 Scope 1 2 Normative references 1 3 Sample preparation 1 4 General safety precautions 1 5 Hydrogen peroxide-nitric acid digestion method 1 6 Perchloric acid digestion method 2

Foreword

This standard is proposed and managed by the Ministry of Commerce of the People's Republic of China. This standard is drafted by. Wood Conservation Development Center. Participated in the drafting of this standard. Wood Conservation Development Center, Guangdong Forestry Research Institute, Dongguan Tianbao Wood Protection Technology Co., Ltd. the company. The main drafters of this standard. Yu Qiu, Su Haitao, Zhang Yanjun, Chen Lifang, Jin Zhongwei, Tao Yiming, Ma Shouhua. This standard is the first release. Wet ashing method before chemical analysis of preservative wood

1 Scope

This standard specifies two methods for wet ashing of preservative wood. This standard is applicable to the analysis of pretreatment of arsenic, chromium, copper, phosphate and other components in preservative wood.

2 Normative references

The terms in the following documents become the terms of this standard by reference to this standard. All dated references, followed by all Modifications (not including errata content) or revisions do not apply to this standard, however, parties to agreements based on this standard are encouraged to study Is it possible to use the latest version of these files? For undated references, the latest edition applies to this standard. GB/T 1933 Wood Density Determination Method

3 sample preparation

3.1 Sampling method Take a representative sample, the sampling site should avoid thrift, cracking and stress wood, and should be more than 30cm from the end. Hollow Drill sampling, when sampling with a hollow drill, the volume of the sample to be tested should be calculated. 3.2 Determination of density The density of the sample was measured in accordance with GB/T 1933 wood density measurement method, expressed in kilograms per cubic meter (kg/m3). 3.3 Sample preparation method The wood sample is comminuted to pass through a No. 30 standard sieve.

4 General safety precautions

4.1 Special safety precautions for the use of perchloric acid digestion methods are described in Section 6.3. 4.2 The acid used in this standard produces toxic fumes and should be operated in a fume hood with good venting throughout the operation. Operators should wear protective safety equipment such as protective glasses. 4.3 Do not allow the digestion solution to be dried to prevent explosion. 5 Hydrogen peroxide-nitric acid digestion 5.1 Principle After the sample is decomposed by hydrogen peroxide-nitric acid, the element to be tested becomes soluble and then quantitatively determined. 5.2 Reagents a) concentrated nitric acid (70%, AR); b) Hydrogen peroxide (50%, AR). 5.3 Operation process The wood powder sample is dried in an oven at 125 ° C for about 2.5 h to constant weight, and the analytical balance with a sensitivity of 0.1 mg is accurately weighed out about 5 g. The sample was placed in a 500 mL flask, and 75 mL of concentrated nitric acid was slowly added along the wall of the bottle to completely wet the wood powder (equivalent to a test per gram of wood powder). Add 15 mL of concentrated nitric acid). Add three glass beads and heat slowly on the hot plate; After the initial reaction to form brown smoke, heating is continued until the solution becomes clear and transparent. Cool down, add 5mL peroxygen drop by drop
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