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JJF 1563-2016 English PDF

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JJF 1563-2016: Calibration Specification for Workstation of Chromatographic Data
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
JJF 1563-2016419 Add to Cart 4 days Calibration Specification for Workstation of Chromatographic Data Valid

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Basic data

Standard ID: JJF 1563-2016 (JJF1563-2016)
Description (Translated English): Calibration Specification for Workstation of Chromatographic Data
Sector / Industry: Metrology & Measurement Industry Standard
Classification of Chinese Standard: A61
Classification of International Standard: 17.020
Word Count Estimation: 18,162
Date of Issue: 2016-06-27
Date of Implementation: 2016-09-27
Quoted Standard: GB/T 25478-2010; ASTM E1657-1998
Adopted Standard: ASTM E1657-1998(2011), NEQ
Regulation (derived from): Notice of the General Administration of Quality Supervision, Inspection and Quarantine of the People Republic of China 2016 No.16
Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine
Summary: This standard applies to liquid chromatography, gas chromatography, ion chromatograph used in the analog interface of the calibration of the chromatographic data workstation. Other types of chromatographic data The calibration of the workstation can be done with reference to this standard.

JJF 1563-2016: Calibration Specification for Workstation of Chromatographic Data

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Calibration Specification for Workstation of Chromatographic Data National Metrological Technical Code of the People's Republic of China Standard for Calibration of Chromatographic Data Workstations 2016-06-27 released 2016-09-27 implementation State Administration of Quality Supervision, Inspection and Quarantine issued Standard for Calibration of Chromatographic Data Workstations Responsible unit. National Physical and Chemical Metrology Technical Committee The main drafting unit. China Institute of Metrology Institute of Metrology and Measurement, Guangxi Zhuang Autonomous Region Participated in the drafting unit. Xinjiang Uygur Autonomous Region Measurement and Testing Research Institute Dalian Yili Te Analysis Instrument Co., Ltd. This specification entrusts the National Physical Chemistry Metrology Technical Committee to explain The main drafters of this specification. Tao Hong (China Institute of Metrology) Feng Keli (Institute of Metrology and Measurement, Guangxi Zhuang Autonomous Region) Zhang qinghe (China Institute of Metrology) Participate in the drafters. Bai Xu (Xinjiang Uygur Autonomous Region Measurement and Testing Institute) Yu Dexiu (Dalian Li Lite Analytical Instruments Co., Ltd.)

table of Contents

Introduction (II) 1 Scope (1) 2 References (1) 3 Overview (1) 4 Metering characteristics (1) 5 Calibration conditions (2) 5.1 Environmental conditions (2) 5.2 Measuring equipment (2) 6 Calibration items and calibration methods (2) 6.1 Sampling frequency (2) 6.2 Baseline noise and baseline drift (2) 6.3 Interval error and repeatability (3) 6.4 Voltage indication error and repeatability (3) 6.5 Dynamic Linearity (4) 6.6 Qualitative Repeatability and Quantitative Repeatability (4) 6.7 Quantitative error (4) 7 Calibration results (4) 8 Recurrence time interval (5) Appendix A Chromatographic Signal Generators (6) Appendix B Calibration records (for reference) (7) Appendix C Calibration Certificate Inside Page Format (9) Appendix D Examples of Measurement Uncertainty Evaluation (11)

Introduction

This specification is based on JJF 1001-2011 "General measurement terms and definitions", JJF 1071-2010 "National measurement Calibration rules for the preparation of rules ", JJF 1059.1-2012" measurement uncertainty assessment and representation "as the basis and basis, Reference GB/T 25478-2010 "Chromatographic Data Workstation", ASTME1657-98 (2011) "Liquid Chromatography Quot; StandardPractice for Test & lt; RTI ID = 0.0 & gt; & lt;/RTI & gt; PhotometricDetectorsUsedinLiquidChromatography). This specification is the first release. Standard for Calibration of Chromatographic Data Workstations

1 Scope

This specification applies to the chromatographic data of the analog interface used in liquid chromatography, gas chromatograph, ion chromatograph Station calibration. Other types of chromatographic data The calibration of the workstation can be done with reference to this specification.

2 reference file

This specification refers to the following documents. Chromatographic Data Workstation Standard Test Method for Variable Wavelength Photometric Detectors for Liquid Chromatography (Standard PracticeforTestingVariable-WavelengthPhotometricDetectorsUsedinLiquidChroma- tography For dated references, only the dated edition applies to this specification; references that are not dated , The latest version (including all modifications) applies to this specification.

3 Overview

The chromatographic data workstation consists of a computer, one or more data collectors and colors that convert analog signals into digital Spectrum data processing software, is able to complete the chromatograph signal conversion, data acquisition, analysis, storage and other functions Complete system.

4 measurement characteristics

Chromatographic data station measurement of the technical indicators in Table 1. Table 1 Chromatographic data workstation main technical indicators Terms and Conditions Technical Specifications 4.1 sampling frequency ≥ 20Hz 4.2 Baseline noise ≤ 6μV 4.3 Baseline drift ≤50μV/h 4.4 Maximum permissible error of time interval ± 0.6s 4.5 time interval repeatability ≤ 1s 4.6 Voltage indication maximum allowable error ± 1% 4.7 voltage indication repeatability ≤ 0.01% 4.8 Dynamic linear linear correlation coefficient r≥0.9998 4.9 Qualitative Repetitive RSD Retention Time ≤0.3% 4.10 Quantitative repeatability RSD peak height ≤ 0.3%, RSD peak area ≤ 0.3% 4.11 Quantitative maximum allowable error ± 0.5% Note. The technical indicators are not used for qualified judgment, for reference only.
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