HYT147.1-2013 English PDF
Basic dataStandard ID: HY/T 147.1-2013 (HY/T147.1-2013)Description (Translated English): Code of practice for marine monitoring technology. Part 1: Seawater Sector / Industry: Marine Industry Standard (Recommended) Classification of Chinese Standard: A45 Classification of International Standard: 07.060 Word Count Estimation: 110,193 Quoted Standard: GB/T 6379.2-2004; GB 17378.1; GB 17378.2; GB 17378.3; GB 17378.4; GB 17378.7-2007; Regulation (derived from): Industry standard filing Notice 2013 No. 8 (No. 164 overall) Issuing agency(ies): State Oceanic Administration Summary: This standard specifies: sea monitoring project analysis. This standard applies to: far from the sea and inshore marine areas monitoring, also applies to the estuary, into the sea outfall and adjacent waters water monitored. HYT147.1-2013: Code of practice for marine monitoring technology. Part 1: Seawater---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.Code of practice for marine monitoring technology.Part 1.Seawater ICS 07.060 A45 People's Republic of China Marine Industry Standard Marine monitoring technical regulations Part 1.sea water Part 1.seawater Released on.2013-04-25 2013-05-01 Implementation Issued by the State Oceanic Administration Table of contentsPreface Ⅴ 1 Scope 1 2 Normative references 1 3 Terms and definitions 1 4 General provisions 1 5 Simultaneous determination of copper, lead, zinc, cadmium, chromium, beryllium, manganese, cobalt, nickel, arsenic, and thallium---inductively coupled plasma mass spectrometry 3 6 Determination of hexavalent chromium-portable spectrometer method 6 7 Nitrite 8 8 Nitrate 11 9 Ammonium salt 15 10 Phosphate 18 11 Determination of silicate---flow analysis method 21 12 Determination of total nitrogen---flow analysis method 23 13 Determination of total phosphorus---flow analysis method 25 14 Determination of carbon/nitrogen elements-element analyzer method 26 15 Determination of Chemical Oxygen Demand (CODCr)---Portable Spectrometer Method 28 16 Determination of Cyanide-Portable Spectrometer Method 30 17 Determination of chlorophyll a and pheochrome---fluorescence method 33 18 Determination of Organochlorine Pesticides---Gas Chromatography 35 19 Determination of polychlorinated biphenyls---gas chromatography 40 20 Phthalates 43 21 Determination of Organophosphorus Pesticides---Gas Chromatography 50 22 Determination of phenolic compounds---gas chromatography/mass spectrometry combined method 53 23 Determination of Chloramphenicol---High Performance Liquid Chromatography/Tandem Mass Spectrometry 57 24 Determination of sulfonamide antibiotics---High performance liquid chromatography/tandem mass spectrometry 60 25 Determination of Volatile Organic Compounds-Gas Chromatography/Mass Spectrometry 65 26 Determination of Aromatic Amines --- Gas Chromatography/Mass Spectrometry Combined Method 70 27 Determination of organotin---gas chromatography 74 28 Determination of triazine and amide herbicides---gas chromatography/mass spectrometry 78 Appendix A (informative appendix) Method detection limit 83 Appendix B (Normative Appendix) Record Form 86 Figure 1 Gas chromatogram of 19 standard solutions of organochlorine pesticides 38 Figure 2 Gas chromatogram of 8 standard solutions of polychlorinated biphenyls 42 Figure 3 Gas chromatogram of 6 standard solutions of phthalate ester 45 Figure 4 Gas chromatography/mass spectrometry of 6 standard solutions of phthalate esters 49 Figure 5 Gas chromatogram of 14 standard solutions of organophosphorus pesticides 52 Figure 6 4 phenolic compounds, alternative standards and internal standard standard solution gas chromatography/mass spectrogram 56 Figure 7 Chloramphenicol standard solution liquid chromatography/tandem mass spectrum 59 Figure 8 15 kinds of sulfonamide antibiotics standard solution liquid chromatography/tandem mass spectrum Figure 63 Figure 9 52 kinds of VOCs standard solution gas chromatography/mass spectrum 68 Figure 10 22 kinds of aromatic amine standard solutions gas chromatography/mass spectrum 72 Figure 11 Gas chromatogram of organotin compound standard solution 77 Figure 12 The gas chromatography/mass spectra of standard solutions of triazine and amide herbicides 80 Table 1 Repeatability and reproducibility of each element determined by ICP-MS 5 Table 2 The repeatability, reproducibility and recovery rate of OCPs measured by GC-ECD 39 Table 3 The repeatability, reproducibility and recovery rate of PCBs determined by GC-ECD 42 Table 4 The repeatability, reproducibility and recovery rate of phthalate ester determined by GC-ECD 46 Table 5 GC-MS determination of the quantitative ion and reference ion of phthalate 49 Table 6 The repeatability, reproducibility and recovery rate of phthalate ester determined by GC-MS 50 Table 7 Repeatability, reproducibility and recovery rate of organophosphorus pesticides determined by GC-FPD 53 Table 8 Retention time, quasi-molecular ion and quantitative ion of phenolic compounds 56 Table 9 Repeatability, reproducibility and recovery rate of phenolic compounds determined by GC-MS 57 Table 10 Mobile phase gradient program 59 Table 11 Ion fragments and relative abundance ratio of chloramphenicol 60 Table 12 HPLC mobile phase gradient program 62 Table 13 Qualitative and quantitative ion pairs and collision energy of 15 sulfonamides 64 Table 14 The repeatability, reproducibility and recovery rate of sulfonamides determined by HPLC-MS-MS 65 Table 15 GC-MS determination of 52 volatile organic compounds quantitative ions, repeatability, reproducibility and recovery rate 68 Table 16 Retention time and characteristic ion of aromatic amine 73 Table 17 The repeatability, reproducibility and recovery rate of aromatic amines determined by GC-MS 74 Table 18 The repeatability, reproducibility and recovery rate of organotin compounds determined by GC-FPD 78 Table 19 Retention time and characteristic ions of triazine and amide herbicides 81 Table 20 The repeatability, reproducibility and recovery rate of triazine and amide herbicides determined by GC-MS 81 Table A.1 Detection limit of determination method 83 Table B.1 Analysis record sheet in seawater samples (ICP-MS method) 86 Table B.2 Analysis record table in water sample (method) 87 Table B.3 Chlorophyll a Analysis Record Sheet (Fluorometer Method) 88 Table B.4 Standard curve record sheet for organochlorine pesticides (gas chromatography) 89 Table B.5 Organochlorine pesticide analysis record form (gas chromatography) 90 Table B.6 Polychlorinated biphenyl standard curve record sheet (gas chromatography) 91 Table B.7 Polychlorinated biphenyl analysis record sheet (gas chromatography) 92 Table B.8 Standard curve record table of phthalate ester (gas chromatography) 93 Table B.9 Phthalic acid ester analysis record sheet (gas chromatography) 94 Table B.10 Phthalic acid ester analysis record sheet (gas chromatography/mass spectrometry combined use) 95 Table B.11 Standard Curve Recording Sheet for Organophosphorus Pesticides (Gas Chromatography) 96 Table B.12 Organophosphorus pesticide analysis record form (gas chromatography) 97 Table B.13 Phenolic compound analysis record form (gas chromatography/mass spectrometry combined use) 98 Table B.14 Chloramphenicol Standard Curve Recording Sheet (High Performance Liquid Chromatography-Tandem Mass Spectrometry) 99 Table B.15 Chloramphenicol Analysis Record Sheet (High Performance Liquid Chromatography-Tandem Mass Spectrometry) 100 Table B.16 Analysis record of sulfa antibiotics (high performance liquid chromatography-tandem mass spectrometry) 101 Table B.17 Volatile Organic Compound Analysis Record Sheet (Gas Chromatography/Mass Spectrometry Combined Use) 102 Table B.18 Aromatic amine analysis record form (gas chromatography/mass spectrometry combined use) 104 Table B.19 Organotin Compound Analysis Record Sheet (Gas Chromatography) 105 Table B.20 Triazine and amide herbicide analysis record sheet (gas chromatography/mass spectrometry combined use) 106ForewordHY/T 147 "Marine Monitoring Technical Regulations" is divided into seven parts. ---Part 1.Sea water; ---Part 2.Sediment; ---Part 3.Organisms; ---Part 4.Ocean atmosphere; ---Part 5.Marine ecology; ---Part 6.Marine Hydrology, Meteorology and Sea Ice; ---Part 7.Satellite remote sensing technology methods. This part is part 1 of HY/T 147. This section was drafted in accordance with the rules given in GB/T 1.1-2009. This part was proposed by the National Marine Environmental Monitoring Center. This part is under the jurisdiction of the National Marine Standardization Technical Committee (SAC/TC283). This section is responsible for the drafting unit. National Marine Environmental Monitoring Center. Participating in the drafting of this section. South China Sea Environmental Monitoring Center of State Oceanic Administration, East China Sea Environmental Monitoring Center of State Oceanic Administration, State Oceanic Administration Beihai Environmental Monitoring Center. The main drafters of this section. Han Gengchen, Yao Ziwei, Zhang Zhifeng, Wang Juying, Ma Yongan, Jiang Wenbo, Zhao Shilan, Ma Xindong, Wang Lijun, Hu Yingying, Fu Yunna, Na Guangshui, Liu Guangyuan, Chen Shumei, Lin Zhongsheng, Wang Yanjie, Xu Xueren, Xu Hengzhen, Liu Liang, Zhao Huade, Huang Chuguang, Chen Changshu, Zhou Peiyu, Lu Chuqian, Lu Dapeng, Li Dongmei, Guo Juan, Yu Hansheng, Li Xiaomin, Zhu Aijia, Ni Zhixin, Cheng Xiangsheng, Qin Banghui, Liu Fuping, Kong Dingjiang, Yang Qing, Qin Yutao, Liu Caicai, Ren Min, Xu Guofeng, Zhang Yong, Qiu Jinkun, Zhang Shugang, Cui Wenlin, Zhao Yuhui, Xia Youlin, Wang Xinping, Wu Shengqing, Cao Lixin, Xie Li, Yang Xiaofei, Sun Xiaodong, Li Guangmei, Li Fujuan, Wang Youliang, Wang Mei, Zhang Qi, Zhang Qingbo. Marine monitoring technical regulations Part 1.sea water1 ScopeThis part of HY/T 147 specifies the analysis method for seawater monitoring items. This section applies to the monitoring of sea water in the far sea and inshore waters, as well as the monitoring of estuaries, sewage outfalls into the sea and water bodies in adjacent sea areas. Note. There are differences in the scope of application of specific monitoring methods.2 Normative referencesThe following documents are indispensable for the application of this document. For dated reference documents, only the dated version applies to this article Pieces. For undated references, the latest version (including all amendments) applies to this document. GB/T 6379.2-2004 Measurement methods and accuracy of results (accuracy and precision) Part 2.Determine standard measurement methods Basic method of method repeatability and reproducibility GB 17378.1 Marine Monitoring Specification Part 1.General GB 17378.2 Marine Monitoring Specification Part 2.Data Processing and Analysis Quality Control GB 17378.3 Marine Monitoring Specification Part 3.Sample Collection, Storage and Transportation GB 17378.4 Marine Monitoring Specification Part 4.Seawater Analysis GB 17378.7-2007 Marine Monitoring Specification Part 7.Offshore Pollution Ecological Investigation and Biological Monitoring3 Terms and definitionsThe following terms and definitions defined in GB 17378.2 apply to this document. 3.1 Continuousflow analysis Use a peristaltic pump to press the sample into a carrier flow that flows at a certain flow rate and is separated by air bubbles or nitrogen bubbles, and the sample and reagents are connected. After fully mixing and fully reacting in the continuous flow carrier to reach a steady state, the reaction product is detected by a detector. 3.2 Fieldspikedsamples Take a set of parallel samples at the sampling site, and add the standard solution of the tested substance of known concentration prepared in the laboratory to one of the samples. Among the water samples of known volume, the standard sample is added on site, and the other sample is not added.4 General rules4.1 Sample collection 4.1.1 Sampling equipment The sampling equipment required for this section includes. a) Water collector made of polyvinyl chloride or polytetrafluoroethylene; ......Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of HYT147.1-2013_English be delivered?Answer: Upon your order, we will start to translate HYT147.1-2013_English as soon as possible, and keep you informed of the progress. The lead time is typically 1 ~ 3 working days. 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