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GB/T 9869.2-2025 English PDF

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GB/T 9869.2-2025: Rubber - Measurement of vulcanization characteristics using curemeters - Part 2: Oscillating disc curemeter
Status: Valid
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GB/T 9869.2-2025344 Add to Cart 4 days Rubber - Measurement of vulcanization characteristics using curemeters - Part 2: Oscillating disc curemeter Valid

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GB/T 7762   GB/T 7759.2   GB/T 10707   GB/T 9869.1   GB/T 9869   GB/T 9870.2   

Basic data

Standard ID: GB/T 9869.2-2025 (GB/T9869.2-2025)
Description (Translated English): Rubber - Measurement of vulcanization characteristics using curemeters - Part 2: Oscillating disc curemeter
Sector / Industry: National Standard (Recommended)
Classification of Chinese Standard: G40
Classification of International Standard: 83.060
Word Count Estimation: 17,11
Date of Issue: 2025-06-30
Date of Implementation: 2026-01-01
Older Standard (superseded by this standard): GB/T 9869-2014
Issuing agency(ies): State Administration for Market Regulation, China National Standardization Administration

GB/T 9869.2-2025: Rubber - Measurement of vulcanization characteristics using curemeters - Part 2: Oscillating disc curemeter


---This is an excerpt. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.), auto-downloaded/delivered in 9 seconds, can be purchased online: https://www.ChineseStandard.net/PDF.aspx/GBT9869.2-2025
ICS 83.060 CCSG40 National Standard of the People's Republic of China Replaces GB/T 9869-2014 Determination of vulcanization characteristics of rubber using a vulcanizer Part 2.Disc oscillating rheometer (ISO 6502-2.2018, IDT) Released on June 30, 2025 Implementation on January 1, 2026 State Administration for Market Regulation The National Standardization Administration issued

Table of Contents

Preface III Introduction IV 1 Scope 1 2 Normative references 1 3 Terms and Definitions 1 4 Principle 1 5 Device 2 6 Calibration 7 7 Sample 7 8 Vulcanization 7 9 Sample Conditioning 7 10 Test Step 7 11 Test results 8 12 Test Report 9 Appendix A (Normative) Calibration Specifications 10 Reference 12 Preface This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for standardization work Part 1.Structure and drafting rules for standardization documents" Drafting. This document is Part 2 of GB/T 9869 “Rubber - Determination of vulcanization characteristics using a vulcanizer”. GB/T 9869 has been published as follows part. --- Part 1.Introduction; --- Part 2.Disc oscillating rheometer. This document replaces GB/T 9869-2014 "Rubber compounds - Determination of vulcanization characteristics - Disc oscillation vulcanometer method" and is in line with GB/T Compared with 9869-2014, in addition to structural adjustments and editorial changes, the main technical changes are as follows. a) The descriptions of torque and compound stiffness have been deleted (see 4.1 of GB/T 9869-2014); b) The vulcanization curve type diagram (see 4.2 of GB/T 9869-2014) has been deleted; c) Deleted the detailed description of the parameters obtained from the relationship between torque and time of the vulcanization curve (see GB/T 9869-2014 4.3); d) Added inspection of mold cavity shape (see 5.2); e) The recording accuracy of torque has been changed (see 5.6.2, 5.6.2 of GB/T 9869-2014); f) The calibration content for torque sensors and recorders has been changed (see Chapter 6, Chapter 6 of GB/T 9869-2014); g) Added requirements for sample conditioning (see Chapter 9); h) Added calibration specifications (see Appendix A). This document is equivalent to ISO 6502-2.2018 "Rubber - Determination of vulcanization characteristics by vulcanizer - Part 2.Oscillating disk vulcanizer". Please note that some of the contents of this document may involve patents. The issuing organization of this document does not assume the responsibility for identifying patents. This document was proposed by the China Petroleum and Chemical Industry Federation. This document is under the jurisdiction of the National Technical Committee on Rubber and Rubber Products of Standardization (SAC/TC35). This document was drafted by. Sailun Group Co., Ltd., Xuzhou Xulun Rubber Co., Ltd., Shandong Linglong Tire Co., Ltd. Shandong Yanggu Huatai Chemical Co., Ltd., Qingdao Doublestar Tire Industry Co., Ltd., Jiangsu Mingzhu Testing Machinery Co., Ltd., Bayi Rubber Rubber Co., Ltd., Guangzhou Liangheng Testing Technology Service Co., Ltd., Xuzhou Industrial Vocational and Technical College, Shaanxi Yanchang Petroleum Group Rubber Co., Ltd. Co., Ltd., Hubei Linglong Tire Co., Ltd., Shandong Huasheng Rubber Co., Ltd., and Beijing Rubber Industry Research and Design Institute Co., Ltd. The main drafters of this document are. Zhang Xiaojun, Zhang Yu, Wei Bangfeng, Liu Lian, Zhang Lijie, Lu Guanshan, Huang Cunying, Zhu Xiaohua, Guo Fei, Huang Quanze, Bao Dafei, Zhu Muzhi, Liu Jun, Yao Ming, Yuan Shuang, Liu Qianfang, Xu Yunhui, Wang Zaixue, Gong Rui, Shen Chunhe, Wang Feng, Zhang Zhengliang, Xu Kai, Zhu Xinjing, Xie Junfang and Sun Siwen. The previous versions of this document and the documents it replaces are as follows. ---First issued as GB/T 9869-1998 in.1998, first revised in.1997, second revised in.2014; --- This is the third revision, and the standard number is adjusted to GB/T 9869.2.

introduction

There are many types of existing vulcanizers, and their appearance and structure are different. With the continuous improvement of the level of vulcanization testing technology, the current standards have been At the same time, in order to be consistent with the ISO 6502 series of standards, it is necessary to revise the current standards and update the technical content. GB/T 9869 “Determination of vulcanization characteristics of rubber using vulcanizer” aims to provide guidance for the selection and use of vulcanizers. The test method for determining the vulcanization characteristics of rubber using a vulcanizer is intended to consist of three parts. --- Part 1.Introduction. The purpose is to provide a general introduction and guidance for the design and use of vulcanizers. --- Part 2.Disc oscillating rheometer. The purpose is to clarify the technical requirements that the disc oscillating rheometer must meet and specify the use of disc Method for determining the vulcanization characteristics of rubber using an oscillating vulcanizer. --- Part 3.Rotorless Rheometer. The purpose is to clarify the technical requirements that rotorless rheometer must meet, and to specify the use of rotorless rheometer. Method for determining the vulcanization characteristics of rubber compounds using a chemical analyzer. The correspondence between this series of files and the previous version of the files is as follows. ---GB/T 9869.1.GB/T 25268-2010; ---GB/T 9869.2.GB/T 9869-2014; ---GB/T 9869.3.GB/T 16584-1996. Determination of vulcanization characteristics of rubber using a vulcanizer Part 2.Disc oscillating rheometer Warning 1---People who use this document should have practical experience in regular laboratory work. This document does not indicate all possible safety The user is responsible for taking appropriate safety and health measures and ensuring that the conditions stipulated by relevant national laws and regulations are met. Warning 2 - Some of the steps specified in this document may involve the use or generation of certain wastes, which may cause harm to the local environment. Appropriate safe operation and waste disposal terms after use should be specified in the relevant documents. 1 Scope This document describes the method for determining the vulcanization characteristics of rubber compounds using a disk oscillating vulcanimeter. ISO 6502-1. 2 Normative references The contents of the following documents constitute the essential clauses of this document through normative references in this document. For referenced documents without a date, only the latest version (including all amendments) applies to this document. This document. GB/T 9869.1-2025 Rubber vulcanizate for the determination of vulcanization characteristics Part 1.Introduction (GB/T 9869.1-2025, ISO 6502-1.2018, IDT) Note. GB/T 25269-2010 Guide to calibration of rubber testing equipment (ISO 18899.2004, IDT) 3 Terms and Definitions The terms and definitions defined in GB/T 9869.1-2025 apply to this document. 4 Principles 4.1 Place the rubber sample in a closed mold cavity with a specified initial pressure and maintained at the vulcanization temperature. The disk oscillates with a small oscillating amplitude. The disk oscillation causes shear strain on the sample. The torque of the disk oscillation depends on the stiffness of the rubber compound (shear Modulus). The torque is automatically recorded graphically as a function of time. 4.2 As the vulcanization progresses, the stiffness of the rubber specimen gradually increases. When the recorded torque rises to a stable value or a maximum value, the vulcanization is obtained. Curve (see GB/T 9869.1-2025). If the torque continues to rise, it is considered that vulcanization is not completed within the given time. The time values obtained depend on the test temperature and the properties of the rubber compound. 4.3 The parameter M = f(t) can be obtained from the recorded torque versus time vulcanization curve. Given in.
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