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GB/T 7739.13-2019 English PDF

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GB/T 7739.13-2019: Methods for chemical analysis of gold concentrates -- Part 13: Determination of lead, zinc, bismuth, cadmium, chromium, arsenic and mercury contents -- Inductively coupled plasma atomic emission spectrometry
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
GB/T 7739.13-2019199 Add to Cart 3 days Methods for chemical analysis of gold concentrates -- Part 13: Determination of lead, zinc, bismuth, cadmium, chromium, arsenic and mercury contents -- Inductively coupled plasma atomic emission spectrometry Valid

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Basic data

Standard ID: GB/T 7739.13-2019 (GB/T7739.13-2019)
Description (Translated English): Methods for chemical analysis of gold concentrates -- Part 13: Determination of lead, zinc, bismuth, cadmium, chromium, arsenic and mercury contents -- Inductively coupled plasma atomic emission spectrometry
Sector / Industry: National Standard (Recommended)
Classification of Chinese Standard: D46
Classification of International Standard: 77.150.01
Word Count Estimation: 10,128
Date of Issue: 2019-06-04
Date of Implementation: 2020-05-01
Issuing agency(ies): State Administration for Market Regulation, China National Standardization Administration

GB/T 7739.13-2019: Methods for chemical analysis of gold concentrates -- Part 13: Determination of lead, zinc, bismuth, cadmium, chromium, arsenic and mercury contents -- Inductively coupled plasma atomic emission spectrometry



---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Methods for chemical analysis of gold concentrates--Part 13. Determination of lead, zinc, bismuth, cadmium, chromium, arsenic and mercury contents--Inductively coupled plasma atomic emission spectrometry ICS 77.150.01 D46 National Standards of People's Republic of China Gold concentrate chemical analysis method Part 13. Lead, zinc, antimony, cadmium, chromium, Determination of the amount of arsenic and mercury Inductively coupled plasma atomic emission spectrometry Part 13.Determinationoflead,zinc,bismuth,cadmium, 2019-06-04 released 2020-05-01 implementation State market supervision and administration China National Standardization Administration issued

Content

Foreword I 1 Scope 1 2 Principle of the method 1 3 reagent 1 4 instruments 2 5 sample 2 6 Test step 2 7 test data processing 4 8 precision 5 Appendix A (informative) Recommended analytical lines and instruments for the determination of multiple elements by inductively coupled plasma atomic emission spectrometry Working condition parameter 7

Foreword

GB/T 7739 "Chemical Analysis Method for Gold Concentrate" is divided into 14 parts. --- Part 1. Determination of the amount of gold and silver; --- Part 2. Determination of the amount of silver; --- Part 3. Determination of the amount of arsenic; --- Part 4. Determination of copper content; --- Part 5. Determination of lead content; ---Part 6. Determination of the amount of zinc; --- Part 7. Determination of iron content; --- Part 8. Determination of sulfur content; --- Part 9. Determination of carbon content; --- Part 10. Determination of the amount of sputum; --- Part 11. Determination of the amount of arsenic and strontium; --- Part 12. Determination of arsenic, mercury, cadmium, lead -- Part 13. Determination of lead, zinc, bismuth, cadmium, cadmium, arsenic and mercury - Inductively coupled plasma atomic emission spectrometry; --- Part 14. Determination of enthalpy measurements by inductively coupled plasma atomic emission spectrometry and inductively coupled plasma mass spectrometry. This part is the 13th part of GB/T 7739. This part is drafted in accordance with the rules given in GB/T 1.1-2009. This part is proposed and managed by the National Gold Standardization Technical Committee (SAC/TC379). This section drafted by. Fujian Zijin Mining and Metallurgical Testing Technology Co., Ltd., Daye Nonferrous Design Institute Co., Ltd., Changchun Gold Research Institute Co., Ltd., North Mine Testing Technology Co., Ltd., Jiangxi Jinyuan Nonferrous Metals Geological Testing Co., Ltd., Zhongtiaoshan Nonferrous Metal Group Co., Ltd. Shandong Hengbang Smelting Co., Ltd., Huajin Guozheng (Shenzhen) Gold and Silver Jewelry Inspection Center Co., Ltd. The main drafters of this section. Xiazhu, Liu Chunhua, Wu Yinlai, Bao Weidong, Chen Zhuhai, Zeng Jing, Pan Xiaoling, Hong Bo, Wang Ju, Han Xiao, Fang Di, Cao Yu, Dai Xuding, Li Jing, Yang Dingxian, Dong Naijun, Zhang Junfeng, Qi Haiguang, Zhang Weitao, Lin Shuxuan. Gold concentrate chemical analysis method Part 13. Lead, zinc, antimony, cadmium, chromium, Determination of the amount of arsenic and mercury Inductively coupled plasma atomic emission spectrometry Caution - Lead, cadmium, chromium, arsenic and mercury are toxic substances. Personnel using this section should have practical experience in formal laboratory work. Headquarters The points do not indicate all possible security issues. It is the responsibility of the user to take appropriate safety and health measures and to ensure compliance with national regulations. Prescribed conditions.

1 Scope

This part of GB/T 7739 specifies the determination of lead, zinc, antimony and cadmium in gold concentrate by inductively coupled plasma atomic emission spectrometry. A method of the amount of chromium, arsenic and mercury. This section applies to the determination of lead, zinc, antimony, cadmium, chromium, arsenic and mercury in gold concentrates. The measurement range of each element is shown in Table 1. Table 1 Measurement range Element measurement range /% Element measurement range /% Lead 0.0050~5.00 Cadmium 0.0050~2.00 Zinc 0.0050~5.00 Chromium 0.010~2.00 Arsenic 0.0050~5.00 Mercury 0.0050~2.00 铋0.0050~2.00

2 Method summary

The sample is dissolved in hydrochloric acid or nitric acid (measurement of lead, zinc, antimony, cadmium, arsenic and mercury) or dissolved in sulfur-phosphorus mixed acid (determination of chromium) in dilute nitric acid medium In the selected condition of the inductively coupled plasma atomic emission spectrometer, the spectral intensity of each element in the test solution is determined, and the standard solution is used. As an internal standard, the amount of lead, zinc, antimony, cadmium, chromium, arsenic and mercury is calculated according to the standard curve internal standard method.

3 reagents

Analytically pure reagents and secondary deionized water were used in the analysis unless otherwise stated. 3.1 Nitric acid (ρ = 1.42 g/mL). 3.2 Hydrochloric acid (ρ=1.19g/mL). 3.3 Perchloric acid (ρ = 1.76 g/mL). 3.4 Sulfuric acid (ρ=1.84g/mL). 3.5 Phosphoric acid (ρ = 1.87 g/mL). 3.6 Hydrofluoric acid (ρ=1.14g/mL). 3.7 Tartaric acid solution (200g/L).
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