GB/T 7598-2008 English PDFUS$259.00 · In stock
Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. GB/T 7598-2008: Determination of water-soluble acid in transformer oils in service Status: Valid GB/T 7598: Historical versions
Basic dataStandard ID: GB/T 7598-2008 (GB/T7598-2008)Description (Translated English): Determination of water-soluble acid in transformer oils in service Sector / Industry: National Standard (Recommended) Classification of Chinese Standard: E38 Classification of International Standard: 75.100 Word Count Estimation: 11,125 Date of Issue: 2008-09-24 Date of Implementation: 2009-08-01 Older Standard (superseded by this standard): GB/T 7598-1987 Quoted Standard: GB/T 601 Regulation (derived from): National Standard Approval Announcement 2008 No.16 (Total No.129) Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China Summary: This standard specifies the method for the determination of transformer oil in the water-soluble acid. This method is suitable for the operation of transformer oil, other mineral oils measured water soluble acids may refer to. GB/T 7598-2008: Determination of water-soluble acid in transformer oils in service---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.Determination of water-soluble acid in transformer oils in service ICS 75.100 E38 National Standards of People's Republic of China Replacing GB/T 7598-1987 In transformer oils in water-soluble acid assay Posted 2008-09-24 2009-08-01 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released Table of ContentsPreface Ⅰ 1 Scope 1 2 Normative references 1 3 Summary of Method 1 4 Reagents and materials 1 5 Preparation 2 6 Test Step 3 Precision 3 7 Appendix A (informative) Determination of water-soluble acid (pH meter method) 4 Annex B (informative) Determination of water-soluble acid (Highly odd colorimeter method) 6ForewordThis standard replaces GB/T 7598-1987 "in transformer oil, turbine oil water-soluble acid assay (colorimetry)." This standard GB/T 7598-1987 and the main technical differences are as follows. --- The name of the revision of this standard as "water-soluble acid in transformer oils Determination." --- Modify the scope of this standard. --- The original standard pH standard buffer solution, pH standard colorimetric solution and increase the effective use of indicators. --- The original standard indicator was revised. --- Original standard increased the pH standard colorimetric solution preparation step. --- The original standard colorimetric steps do revision. --- Of colorimetric accuracy has been revised. --- The original contents of the appropriate standard of rescheduling. --- Increased precision pH meter method and the method in the appendix. The Standard Appendix A, Appendix B is an informative annex. This standard is proposed and managed by the China Electricity Council. This standard was drafted. Xi'an Thermal Power Research Institute Co., Ltd. The main drafters of this standard. Feng Liping, Xiaoxiu Yuan, Meng Yuchan. This standard supersedes the previous editions are. --- GB/T 7598-1987. In transformer oils in water-soluble acid assay1 ScopeThis standard specifies the determination method in transformer oils in a water-soluble acid. This method is suitable for the operation of transformer oil, other mineral oils Determination of water-soluble acid may be implemented by reference.2 Normative referencesThe following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard. Preparation of GB/T 601 chemical reagent standard titration solution3 Method SummaryUnder test conditions, test oil samples mixed with an equal volume of distilled water, whichever is the liquid part of the water out through colorimetric determination of water-soluble oil acid. Results are expressed as pH. Similarly, the method can be used pH meter, refer to Appendix A; Haili Qi colorimetric, see Appendix B.4 Reagents and materials4.1 double distilled water or demineralized water, after boiling, pH 6.0 to 7.0, a conductivity of less than 3μs/cm (25 ℃). Potassium hydrogen phthalate 4.2. reference reagents. 4.3 potassium dihydrogen phosphate. reference reagents. 4.4 Sodium hydroxide. AR. 4.5 hydrochloric acid. AR, relative density of 1.19. 4.6 sodium phosphate dibasic anhydrous. pure class distinctions. 4.7 pH indicator. bromocresol green, bromocresol purple. Its preparation method and the color range are shown in Table 1. Table 1 formulated indicator Name indicator color range method of preparation Bromocresol Green 3.8 to 5.4 Yellow - Blue 0.1g of bromocresol green and 7.5mL0.02mol/L sodium hydroxide together research absorbed, diluted with demineralized water to 250mL, then 0.1mol/L sodium hydroxide or hydrochloric acid to a pH of 4.5 to 5.4 Bromocresol purple 5.2 to 6.8 Yellow - purple 0.1g of bromocresol purple was dissolved 9.25mL0.02mol/L sodium hydroxide, diluted with demineralized water to 250mL. Then 0.1mol/L sodium hydroxide or hydrochloric acid to a pH of 6.0 Than 4.8 Color tube. a plug, a diameter of 15mm, capacity 10mL. 4.9 conical flask. 250mL. 4.10 separatory funnel. 250mL. 4.11 cylinders. 50mL. 4.12 thermometer. 0 ℃ ~ 100 ℃. 4.13 water bath. 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