GB/T 5059.5-2014 English PDFUS$169.00 · In stock
Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. GB/T 5059.5-2014: Ferromolybdenum -- Determination of silicon content -- Sulphuric acid dehydration gravimetric method and molybdenum blue spectrophotometric method Status: Valid GB/T 5059.5: Historical versions
Basic dataStandard ID: GB/T 5059.5-2014 (GB/T5059.5-2014)Description (Translated English): Ferromolybdenum -- Determination of silicon content -- Sulphuric acid dehydration gravimetric method and molybdenum blue spectrophotometric method Sector / Industry: National Standard (Recommended) Classification of Chinese Standard: H11 Classification of International Standard: 77.100 Word Count Estimation: 7,777 Date of Issue: 6/9/2014 Date of Implementation: 1/1/2015 Older Standard (superseded by this standard): GB/T 5059.5-1986 Quoted Standard: GB/T 4010 Regulation (derived from): National Standards Bulletin No. 11 of 2014 Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China Summary: This Standard specifies the sulfuric acid dehydration gravimetric method and silicon molybdenum blue spectrophotometric determination of molybdenum iron in silicon. This Standard applies to the determination of molybdenum iron silicon content. Measuring r GB/T 5059.5-2014: Ferromolybdenum -- Determination of silicon content -- Sulphuric acid dehydration gravimetric method and molybdenum blue spectrophotometric method---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order. Ferromolybdenum. Determination of silicon content. Sulphuric acid dehydration gravimetric method and molybdenum blue spectrophotometric method ICS 77.100 H11 National Standards of People's Republic of China Replacing GB/T 5059.5-1986 Determination of silicon content in ferromolybdenum Sulfuric acid dehydration gravimetric method and silicon molybdenum blue spectrophotometry Issued on. 2014-06-09 2015-01-01 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released ForewordGB/T 5059 "ferro molybdenum" is divided into the following sections. --- Part 1. Determination of molybdenum iron molybdenum content of lead molybdate gravimetric method, ammonium metavanadate titration and 8-hydroxyquinoline gravimetric method; --- Part 2. Determination of antimony content ferromolybdenum malachite green spectrophotometry; --- Part 3. Determination of Fe, Cu, Mo Flame atomic absorption spectrometric method; --- Part 5. Determination of silicon content ferromolybdenum sulfuric acid dehydration gravimetric method and silicon molybdenum blue spectrophotometric method; --- Part 6. Determination of phosphorus content of iron molybdenum bismuth phosphomolybdate blue spectrophotometric method and the molybdenum blue spectrophotometric method; --- Part 7. Determination of carbon content ferromolybdenum The infrared absorption method; --- Part 9. molybdenum iron sulfur content Infrared absorption method and combustion iodometric method. This section GB/T 5059 Part 5. This section drafted in accordance with GB/T 1.1-2009 given rules. This Part replaces GB /"ferromolybdenum chemical determination of silicon content - Gravimetric method" T 5059.5-1986. This portion of the GB/T 5059.5- Compared to 1986, in addition to editorial changes, the major technical changes are as follows. --- This section adds two. silicon molybdenum blue spectrophotometric method. --- This section has been revised to a method to increase the content of Chapter 2 and Chapter 9. --- A method for determining the scope of the original standard "is less than 2.50%" to "0.50% to 2.50%." This part is proposed by the China Iron and Steel Association. This part of pig iron and ferroalloy by the National Standardization Technical Committee (SAC/TC318) centralized. This section is drafted. Sinosteel Jilin Ferroalloy Co., Ltd., Liaoning Shen Hong Group Co., Ltd., China Molybdenum Group Co., Ltd. The main drafters of this section. Yuan Ping, Zhang Yingjie, high Yumin, Wang Ping ON TRADITIONAL Li Haibo, Tian Yonghong. This part of the standard replaces the previous editions are. --- GB/T 5059.5-1986. Determination of silicon content in ferromolybdenum Sulfuric acid dehydration gravimetric method and silicon molybdenum blue spectrophotometry Warning. Use of this section shall be a person experiences regular laboratory work. This section does not indicate that all possible security issues. Users have the responsibility to take appropriate safety and health practices and to ensure compliance with the conditions relevant national regulations.1 ScopeGB/T 5059 This section specifies the spectrophotometric determination of molybdenum iron content of sulfuric acid dehydration gravimetric method for silicon and silicon molybdenum blue spectrophotometric. This section applies to the determination of silicon content in ferromolybdenum. Measurement range (mass fraction). a method of sulfuric acid dehydration gravimetric method ~ 0.50% 2.50%, method two silicon molybdenum blue spectrophotometry 0.01% to 1.00%.2 Normative referencesThe following documents for the application of this document is essential, dated references, only the dated version suitable for use herein Member. For undated references, the latest edition (including any amendments) applies to this document. GB/T 4010 alloy chemical analysis and preparation of samples3 a method of sulfuric acid dehydration gravimetric method3.1 Principle Sample of nitric acid, hydrochloric acid decomposition, sulfuric smoke, the silicon to form insoluble silicates, filtered, washed with burning to constant weight. Join hydrofluoric acid Li, silicon tetrafluoride silicon was removed by volatilization, and then calcined to constant, by differential weighing before and after treatment of hydrofluoric acid measured silicon content. 3.2 Reagents Unless otherwise indicated in the analysis using only recognized as analytical grade reagents and distilled water or its equivalent purity water. 3.2.1 hydrofluoric acid, ρ = 1.15g/mL. 3.2.2 hydrochloride, ρ = 1.19g/mL. 3.2.3 nitrate, 11. 3.2.4 hydrochloric acid, 14. 3.2.5 hydrochloric acid, 110. 3.2.6 sulfuric acid, 11. 3.3 Sampling and Preparation In accordance with the provisions of GB/T 4010 will be sampling and sample preparation, the sample should be adopted 0.125mm sieve. 3.4 Analysis Steps 3.4.1 Sample volume Weigh 1.00g sample, accurate to 0.0001g. ......Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of GB/T 5059.5-2014_English be delivered?Answer: Upon your order, we will start to translate GB/T 5059.5-2014_English as soon as possible, and keep you informed of the progress. 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