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GB/T 43220-2023 English PDF

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GB/T 43220-2023: Determination of arsenic in solid biofuels
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
GB/T 43220-2023269 Add to Cart 3 days Determination of arsenic in solid biofuels Valid

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Basic data

Standard ID: GB/T 43220-2023 (GB/T43220-2023)
Description (Translated English): Determination of arsenic in solid biofuels
Sector / Industry: National Standard (Recommended)
Classification of Chinese Standard: D21
Classification of International Standard: 73.040
Word Count Estimation: 14,196
Date of Issue: 2023-09-07
Date of Implementation: 2024-04-01
Issuing agency(ies): State Administration for Market Regulation, China National Standardization Administration

GB/T 43220-2023: Determination of arsenic in solid biofuels

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
ICS 73.040 CCSD21 National Standards of People's Republic of China Method for determination of arsenic in solid biomass fuels Published on 2023-09-07 2024-04-01 Implementation State Administration for Market Regulation Released by the National Standardization Administration Committee

Table of contents

Preface III 1 Scope 1 2 Normative reference documents 1 3 Terms and Definitions 1 4 Hydride generation-atomic fluorescence spectrometry 1 5 Hydrogen generation-atomic absorption method 4 6 Calculation and presentation of results 6 7 Method Precision 6 8 Test report 7 Appendix A (informative) Instrument reference working conditions 8

Foreword

This document complies with the provisions of GB/T 1.1-2020 "Standardization Work Guidelines Part 1.Structure and Drafting Rules of Standardization Documents" Drafting. Please note that some content in this document may be subject to patents. The publisher of this document assumes no responsibility for identifying patents. This document is proposed by the China Coal Industry Association. This document is under the jurisdiction of the National Coal Standardization Technical Committee (SAC/TC42). This document was drafted by. Coal Testing Center of Coal Science and Technology Research Institute Co., Ltd. The main drafters of this document. Chen Huizhu, Fu Kun, and Chen Sihan. Method for determination of arsenic in solid biomass fuels

1 Scope

This document describes the hydride generation-atomic fluorescence spectrometry and hydride generation-atomic absorption methods for the determination of arsenic in solid biomass fuels. Method summary, reagents and materials, instruments and equipment, samples, test procedures, result calculation and presentation, method precision and test report. This document applies to the determination of arsenic in solid biomass fuels.

2 Normative reference documents

The contents of the following documents constitute essential provisions of this document through normative references in the text. Among them, the dated quotations For undated referenced documents, only the version corresponding to that date applies to this document; for undated referenced documents, the latest version (including all amendments) applies to this document. GB/T 622 Chemical reagent hydrochloric acid GB/T 623 Chemical reagent perchloric acid GB/T 625 Chemical Reagent Sulfuric Acid GB/T 626 Chemical reagent nitric acid GB/T 6682 Specifications and test methods for water used in analytical laboratories GB/T 6684 Chemical reagent 30% hydrogen peroxide GB/T 15337 General principles of atomic absorption spectrometry GB/T 21191 Atomic Fluorescence Spectrometer GB/T 21923 General rules for inspection of solid biomass fuel GB/T 26814 Microwave digestion device GB/T 28730 Solid biomass fuel sample preparation method

3 Terms and definitions

The terms and definitions defined in GB/T 21923 apply to this document. 4 Hydride generation-atomic fluorescence spectrometry 4.1 Summary of methods After the solid biomass fuel is digested by microwave digestion, wet digestion or Ashka mixed burning method, a pre-reducing agent is added to reduce the pentavalent arsenic. into trivalent arsenic, and use sodium borohydride to reduce the trivalent arsenic to gaseous hydride. Argon is used as a carrier gas to introduce the gaseous hydride obtained by reduction into atoms. In a certain concentration range, the fluorescence intensity is directly proportional to the arsenic content. The arsenic content in the solution can be measured by comparing with the standard series. 4.2 Reagents and materials Warning. The strong acid used in the test is highly corrosive and oxidizing. Protective equipment must be worn during operation and avoid contact with skin and clothing. All The sample pretreatment process needs to be carried out in a fume hood. Unless otherwise stated, chemical reagents of analytical grade and above that comply with national standards are used in the analysis, and the water used is in compliance with GB/T 6682 regulations.
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