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GB/T 36065-2018 English PDF

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GB/T 36065-2018: Nanotechnologies -- Analysis of amorphous carbon, ash and volatile of carbon nanotubes -- Thermogravimetry
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GB/T 36065-2018359 Add to Cart 4 days Nanotechnologies -- Analysis of amorphous carbon, ash and volatile of carbon nanotubes -- Thermogravimetry Valid

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Basic data

Standard ID: GB/T 36065-2018 (GB/T36065-2018)
Description (Translated English): Nanotechnologies -- Analysis of amorphous carbon, ash and volatile of carbon nanotubes -- Thermogravimetry
Sector / Industry: National Standard (Recommended)
Classification of Chinese Standard: G04
Classification of International Standard: 71.040.50
Word Count Estimation: 18,144
Date of Issue: 2018-03-15
Date of Implementation: 2018-10-01
Issuing agency(ies): State Administration for Market Regulation, China National Standardization Administration

GB/T 36065-2018: Nanotechnologies -- Analysis of amorphous carbon, ash and volatile of carbon nanotubes -- Thermogravimetry


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Nanotechnologies--Analysis of amorphous carbon, ash and volatile of carbon nanotubes--Thermogravimetry ICS 71.040.50 G04 National Standards of People's Republic of China Nanotechnology Carbon Nanotubes Amorphous Carbon, Ash, and Analytical thermogravimetry of volatiles Published by.2018-03-15 2018-10-01 implementation General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China China National Standardization Administration released Directory Preface III Introduction IV 1 Scope 1 2 Normative references 1 3 Terms and Definitions 1 4 Abbreviations and symbols 2 5 Reaction principle under different experimental atmospheres 2 6 Instruments and Accessories 3 7 Reagents and Materials 3 8 Test Method 3 9 Data Analysis 4 10 Test Report 7 Appendix A (Normative Appendix) Relationship between Tox' and Te and Oxygen Content in Oxygen and Syngas Mixtures Appendix B (Informative) Examples of Thermogravimetric Data Processing in Different Atmospheres 9 Reference 13

Foreword

This standard was drafted in accordance with the rules given in GB/T 1.1-2009. This standard was proposed by the Chinese Academy of Sciences. This standard is under the jurisdiction of the National Nanotechnology Standardization Technical Committee (SAC/TC279). This standard was drafted by. National Nanoscience Center, Shenzhen German Nanotechnology Co., Ltd., Nanotechnology, and National Applications Cheng Research Center. The main drafters of this standard. Zhang Donghui, Ge Guanglu, Kong Lingyong, Wang Yuanhang, Shang Weili, Yan Xiaoying, Zhu Jun, Zhang Ying.

Introduction

Carbon nanotubes are nanotubes composed of carbon atoms. Carbon nanotubes have many excellent mechanical, electrical and chemical properties in many fields It has a wide range of application prospects and is a nanomaterial that has been industrially produced [1]. Amorphous carbon, ash, and volatiles in carbon nanotubes The content and its main oxidation temperature and thermal stability have a great influence on its performance and application [2, 3]. Therefore, the components of the carbon nanotube sample are accurate. Accurate measurement and evaluation of its oxidative and thermal stability are key control parameters for the quality of carbon nanotube samples. Thermogravimetry (referred to as TG) is to evaluate the content of different components in carbon nanotubes samples and their main oxidation temperature and heat The effective method of stability, the use of different experimental atmospheres can obtain different information [4~8]. This standard gives carbon in different experimental atmospheres Thermogravimetric analysis (TGA) techniques and specifications for nanotube samples, including different experimental atmospheres Under the TG principle and data processing process and so on. The experimental atmosphere specifically includes a carbon dioxide atmosphere, a mixed gas atmosphere of oxygen and synthetic air And nitrogen atmosphere. The formulation of this standard will provide for the production of carbon nanotube samples, testing organizations, research institutes and related supervision and management departments. The use of TG to analyze the contents of amorphous carbon, ash, volatiles and other components and oxidation temperature in carbon nanotubes under the same experimental atmosphere reference. Nanotechnology Carbon Nanotubes Amorphous Carbon, Ash, and Analytical thermogravimetry of volatiles

1 Scope

This standard specifies the use of thermogravimetric analysis of amorphous carbon, ash, and volatiles in carbon nanotube samples under different experimental atmospheres. The method for measuring the main oxidation temperature and thermal stability of the carbon nanotubes and the carbon nanotubes includes an atmosphere of carbon dioxide, a mixture of oxygen and synthetic air. Gas atmosphere and nitrogen atmosphere. This standard applies to single-wall and multi-wall carbon nanotube samples obtained by chemical vapor deposition. Carbon nanotube test obtained by other preparation methods You can refer to the implementation.

2 Normative references

The following documents are indispensable for the application of this document. For dated references, only dated versions apply to this article Pieces. For undated references, the latest version (including all amendments) applies to this document. GB/T 5314 powder metallurgy powder sampling method GB/T 6425 thermal analysis terminology Thermal analysis method for thermal stability of GB/T 13464 GB/T 19619 nanomaterials Thermogravimetric analysis of oxidation temperature and ash of GB/T 29189 carbon nanotubes GB/T 30544.3 Nanotechnology terminology part 3. Carbon nano-objects Thermal weight characterization of GB/T 32868 nanotechnology single-walled carbon nanotubes ISO /T R10929 Nanotechnology Multi-Wall Carbon Nanotube Characterization [Nanotechnologies-Characterizationofmultiwal Carbon(MWCNT)samples]

3 Terms and definitions

GB/T 6425, GB/T 13464, GB/T 19619, GB/T 29189, GB/T 30544.3, GB/T 32868, ISO /T R10929 The defined and the following terms and definitions apply to this document. 3.1 Amorphous Carbon Amorphous Carbon Amorphous carbon and disordered carbon formed by the accumulation of molecular fragments of graphite layered structure. Note. Modified GB/T 34916-2017, Definition 3.1. 3.2 Amorphous carbon content Wam The mass fraction of amorphous carbon in the carbon nanotube sample. 3.3 Volatile content volatilecontent Wv The carbon nanotube sample was heated from room temperature to a set temperature under a nitrogen atmosphere and maintained at this temperature until the volatiles were completely released. The sample did not
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