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GB/T 35446-2017 English PDF

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GB/T 35446-2017: Textiles -- Determination of some organic solvents
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
GB/T 35446-2017199 Add to Cart 3 days Textiles -- Determination of some organic solvents Valid

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Basic data

Standard ID: GB/T 35446-2017 (GB/T35446-2017)
Description (Translated English): Textiles -- Determination of some organic solvents
Sector / Industry: National Standard (Recommended)
Classification of Chinese Standard: W04
Classification of International Standard: 59.080.01
Word Count Estimation: 10,177
Date of Issue: 2017-12-29
Date of Implementation: 2018-07-01
Regulation (derived from): National Standards Bulletin 2017 No. 32
Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China

GB/T 35446-2017: Textiles -- Determination of some organic solvents

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Textiles - Determination of some organic solvents ICS 59.080.01 W04 National Standards of People's Republic of China Textiles - Determination of certain organic solvents 2017-12-29 Posted 2018-07-01 implementation General Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China China National Standardization Administration released

Foreword

This standard was drafted in accordance with the rules given in GB/T 1.1-2009. This standard proposed by the China Textile Industry Federation. This standard by the National Textile Standardization Technical Committee (SAC/TC209) centralized. This standard was drafted by the People's Republic of China Jiangsu Entry-Exit Inspection and Quarantine Bureau, China Textile Standard (Beijing) Inspection and Certification Center Co., Ltd., Exit Inspection and Quarantine of the People's Republic of China. The main drafters of this standard. Ding You Chao, Si Ying, Wu Gang, Gao Ying, Zheng Kai, Cao Xizhong, Zhang Hui, Qian Kai, Qi Yan, Tang Juan. Textiles - Determination of certain organic solvents Warning --- personnel using this standard should have formal laboratory work experience. This standard does not indicate all possible safety issues question. It is the user's responsibility to take appropriate safety and health measures and to ensure compliance with the requirements of the relevant state laws and regulations.

1 Scope

This standard specifies the use of gas chromatography - mass spectrometry (GC/MSD) or gas chromatography - flame ionization detector (GC/FID) determination Textiles in 9 kinds of organic solvents (see Appendix A) residual amount of the method. This standard applies to all kinds of textile products.

2 principle

Methanol in the ultrasonic bath to extract residual organic solvents in the sample, after concentration by volume gas chromatography - mass spectrometry or gas chromatography - hydrogen Flame ionization detector for detection, qualitative analysis based on retention time and/or mass spectrometry selected ions, external standard quantitative.

3 Reagents and materials

Unless otherwise indicated, all reagents used in the analysis are analytical grade or above purity reagents. 3.1 Methanol, after the test detected no organic solvent or other interfering substances exist. 3.2 methanol. Chromatographic purity. 3.3 organic solvent reference material. 3.4 Standard stock solution (1000mg/L). Weigh the appropriate amount of organic solvent reference material, respectively, with methanol (3.2) or other suitable solvents Prepared into a concentration of about 1000mg/L standard stock solution. Note. The standard stock solution is stored in a refrigerator at 0 ° C to 4 ° C for a period of 6 months. 3.5 mixed standard working solution (1mg/L) were respectively draw the standard solution of organic solvent solution (3.4) placed in the same volumetric flask with methanol (3.2) diluted to 1mg/L step by step. Now with the current use. Note.According to the needs can be formulated into other suitable concentrations.

4 instruments and equipment

4.1 Gas Chromatograph with mass selective detector (GC/MSD). 4.2 Gas Chromatograph with Hydrogen Flame Ionization Detector (GC/FID). 4.3 Balance. Sense of 0.01mg and 0.01g respectively. 4.4 ultrasonic generator. Operating frequency is 40kHz. 4.5 Extractor .50 mL, made of hard glass with screw cap seal. 4.6 Concentrate the bottle. 4.7 Rotary evaporator. 4.8 organic microporous membrane 0.45μm, nylon membrane.
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