GB/T 3260.11-2023 English PDFUS$269.00 · In stock
Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. GB/T 3260.11-2023: Methods for chemical analysis of tin - Part 11: Determination of copper, iron, bismuth, lead, antimony, arsenic, aluminum, zinc, cadmium, silver, nickel and cobalt contents - Inductively coupled plasma atomic emission spectrometry Status: Valid GB/T 3260.11: Historical versions
Basic dataStandard ID: GB/T 3260.11-2023 (GB/T3260.11-2023)Description (Translated English): Methods for chemical analysis of tin - Part 11: Determination of copper, iron, bismuth, lead, antimony, arsenic, aluminum, zinc, cadmium, silver, nickel and cobalt contents - Inductively coupled plasma atomic emission spectrometry Sector / Industry: National Standard (Recommended) Classification of Chinese Standard: H13 Classification of International Standard: 77.120.60 Word Count Estimation: 13,136 Date of Issue: 2023-11-27 Date of Implementation: 2024-06-01 Issuing agency(ies): State Administration for Market Regulation, China National Standardization Administration GB/T 3260.11-2023: Methods for chemical analysis of tin - Part 11: Determination of copper, iron, bismuth, lead, antimony, arsenic, aluminum, zinc, cadmium, silver, nickel and cobalt contents - Inductively coupled plasma atomic emission spectrometry---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order. ICS 77:120:60 CCSH13 National Standards of People's Republic of China Tin chemical analysis methods Part 11: Copper, iron, bismuth, lead, antimony, arsenic, Determination of aluminum, zinc, cadmium, silver, nickel and cobalt content Inductively coupled plasma atomic emission spectrometry Published on 2023-11-27 and implemented on 2024-06-01 State Administration for Market Regulation Released by the National Standardization Administration Committee ForewordThis document complies with the provisions of GB/T 1:1-2020 "Standardization Work Guidelines Part 1: Structure and Drafting Rules of Standardization Documents" Drafting: This document is Part 11 of GB/T 3260 "Chemical Analysis Methods for Tin": GB/T 3260 has released the following parts: ---Part 1: Determination of copper content by flame atomic absorption spectrometry; ---Part 2: Determination of iron content 1,10-phenanthroline spectrophotometric method; ---Part 3: Determination of bismuth content by potassium iodide spectrophotometry and flame atomic absorption spectrometry; ---Part 4: Determination of lead content by flame atomic absorption spectrometry; ---Part 5: Determination of antimony content by malachite green spectrophotometry; ---Part 6: Determination of arsenic content Malachite green-arsenic molybdenum heteropoly acid spectrophotometry; ---Part 7: Determination of aluminum content by electrothermal atomic absorption spectrometry; ---Part 8: Determination of zinc content by flame atomic absorption spectrometry; ---Part 9: Determination of sulfur content by high-frequency induction furnace combustion infrared absorption method; ---Part 10: Determination of cadmium amount by flame atomic absorption spectrometry; ---Part 11: Determination of copper, iron, bismuth, lead, antimony, arsenic, aluminum, zinc, cadmium, silver, nickel and cobalt content by inductively coupled plasma atomic emission radioactive spectroscopy: Please note that some content in this document may be subject to patents: The publisher of this document assumes no responsibility for identifying patents: This document is proposed by the China Nonferrous Metals Industry Association: This document is under the jurisdiction of the National Nonferrous Metals Standardization Technical Committee (SAC/TC243): This document was drafted by: National Standard (Beijing) Inspection and Certification Co:, Ltd:, Yunnan Tin Industry Co:, Ltd: Tin Industry Branch, Liuzhou Huaxi Co:, Ltd: Color Design Research Institute Co:, Ltd:, Shenzhen Zhongjin Lingnan Nonferrous Metals Co:, Ltd:, Fuyang Product Quality Supervision and Inspection Institute, National Hetong (Qingdao) Testing and Evaluation Co:, Ltd:, China Inspection and Certification Group Guangxi Co:, Ltd:, Kunming Metallurgical Research Institute Co:, Ltd:, China National Guilin Institute of Mineral Geology Co:, Ltd:, Beikang Detection Technology Co:, Ltd:, Zijin Copper Co:, Ltd:, Daye Nonferrous Design Research Institute Co:, Ltd:, Chenzhou Commodity Quality Supervision and Inspection Institute, Tongling Nonferrous Metals Group Holdings Co:, Ltd:, Yunnan Tin Industry Mining and Metallurgy Testing Center Co:, Ltd:, Shaoguan City Quality Supervision and Inspection Institute of Guangdong Province, Heilongjiang Zijin Copper Co:, Ltd:, Anhui National Copper, Lead, Zinc and Products Quality Supervision and Inspection Center: The main drafters of this document: Mo Shumin, Zhang Xin, Li Aichang, Zheng Jiale, Chen Xiongfei, Tan Feng, Liang Shanzuo, Liu Yingbo, Yang Min, Gan Xiongsheng, Yuan Lili, Wang Xingjun, Zhang Lu, Wang Jinrong, Xing Huabing, Gu Xingqian, Su Chunfeng, Gan Cong, Chen Lan, Xie Lei, Wang Yang, Chai Xubin, Yuan Qi, Chen Yu, Zang Zhenjuan, Chen Si, Meng Xueren, Hu Yanzhi, Liu Hanxiao, Jiang Jing, Shi Yu, Lu Shimei, Cheng Zihui, Hu Meihua, Pan Xiaoling, Yang Huadong, Hu Hongdan, Lin Binyu, Shen Xianli, Li Changchun, Sun Guojuan, Gu Feifei, Wu Sijing:IntroductionTin has excellent properties such as soft texture, low melting point, and strong malleability: It is mainly used in the manufacture of solder, tin-plated sheets, alloys, chemical products, etc: The GB/T 3260 "Tin Chemical Analysis Methods" series of standards aims to establish a complete set of tin chemical analysis methods, combined with the optimization of the standard system The requirements are planned to be composed of 8 parts after integration: ---Part 1: Determination of copper, lead, zinc, cadmium, silver, nickel and cobalt content by flame atomic absorption spectrometry; ---Part 2: Determination of iron content 1,10-phenanthroline spectrophotometric method; ---Part 3: Determination of bismuth content by potassium iodide spectrophotometry and flame atomic absorption spectrometry; ---Part 5: Determination of antimony content by malachite green spectrophotometry; ---Part 6: Determination of arsenic content Malachite green-arsenic molybdenum heteropoly acid spectrophotometry; ---Part 7: Determination of aluminum content by electrothermal atomic absorption spectrometry; ---Part 9: Determination of sulfur content by high-frequency induction furnace combustion infrared absorption method; ---Part 11: Determination of copper, iron, bismuth, lead, antimony, arsenic, aluminum, zinc, cadmium, silver, nickel and cobalt content by inductively coupled plasma atomic emission radioactive spectroscopy: Inductively coupled plasma atomic emission spectroscopy has the advantages of simultaneous determination of multiple elements and low detection limit, and has been widely used in non-ferrous metals and their Determination of impurity elements in compounds: The method described in this document can achieve the simultaneous determination of 12 impurity elements in tin products: The method is fast and Accurate, it is of great significance to promote the production and trade of tin products: Tin chemical analysis methods Part 11: Copper, iron, bismuth, lead, antimony, arsenic, Determination of aluminum, zinc, cadmium, silver, nickel and cobalt content Inductively coupled plasma atomic emission spectrometry Warning---Personnel using this document should have practical experience in regular laboratory work: This document does not address all possible security issues question: Users are responsible for taking appropriate safety and health measures and ensuring compliance with the conditions stipulated in relevant national regulations:1 ScopeThis document describes the use of inductively coupled plasma atomic emission spectrometry for the determination of copper, iron, bismuth, lead, antimony, arsenic, aluminum, zinc, cadmium, silver, Test methods for nickel and cobalt content: This document is applicable to the determination of copper, iron, bismuth, lead, antimony, arsenic, aluminum, zinc, cadmium, silver, nickel and cobalt in tin, among which the determination of bismuth, lead, antimony and arsenic The range (mass fraction) is 0:0020%~0:050%: The measurement range (mass fraction) of copper, iron, aluminum, zinc, cadmium, silver, nickel and cobalt is 0:0003%~0:050%:2 Normative reference documentsThe contents of the following documents constitute essential provisions of this document through normative references in the text: Among them, the dated quotations For undated referenced documents, only the version corresponding to that date applies to this document; for undated referenced documents, the latest version (including all amendments) applies to this document: GB/T 6682 Specifications and test methods for water used in analytical laboratories3 Terms and definitionsThere are no terms or definitions to be defined in this document:4 PrinciplesThe sample is dissolved in a mixed acid of hydrofluoric acid (or hydrochloric acid) and nitric acid, and measured on an inductively coupled plasma atomic emission spectrometer in an acid medium: The emission intensity of each element is calculated according to the working curve method:5 reagents or materialsUnless otherwise stated, only reagents confirmed to be of superior grade purity or above are used in the analysis: 5:1 Water: Class II water or Class I water in compliance with GB/T 6682: 5:2 High purity tin: wSn≥99:999%: 5:3 Tartaric acid: 5:4 Hydrofluoric acid: ρ=1:13g/mL: 5:5 Nitric acid: ρ=1:42g/mL: ......Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of GB/T 3260.11-2023_English be delivered?Answer: Upon your order, we will start to translate GB/T 3260.11-2023_English as soon as possible, and keep you informed of the progress. 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