GB/T 29676-2013 English PDFUS$169.00 · In stock
Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. GB/T 29676-2013: Determination of chlorobutanol in cosmetics -- Gas chromatography-mass spectrometry Status: Valid
Basic dataStandard ID: GB/T 29676-2013 (GB/T29676-2013)Description (Translated English): Determination of chlorobutanol in cosmetics -- Gas chromatography-mass spectrometry Sector / Industry: National Standard (Recommended) Classification of Chinese Standard: Y42 Classification of International Standard: 71.100.70 Word Count Estimation: 7,735 Regulation (derived from): National Standards Bulletin 2013 No. 17 Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China Summary: This standard specifies: cosmetics chlorobutanol gas chromatography mass spectrometry. This standard applies to: cream, liquid, loose powder, shampoo, lipstick cosmetics in chlorobutanol determination. The standard for chlorobutanol detection limit of 0. GB/T 29676-2013: Determination of chlorobutanol in cosmetics -- Gas chromatography-mass spectrometry---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order. Determination of chlorobutanol in cosmetics.Gas chromatography-mass spectrometry ICS 71.100.70 Y42 National Standards of People's Republic of China Determination of chlorobutanol in cosmetics Gas chromatography - mass spectrometry Issued on. 2013-09-06 2014-02-15 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released ForewordThis standard was drafted in accordance with GB/T 1.1-2009 given rules. Please note that some of the content of this document may involve patents. Release mechanism of the present document does not assume responsibility for the identification of these patents. The standard proposed by China National Light Industry Council. This standard by the National Standardization Technical Committee of Fragrance Flavor and Cosmetic (SAC/TC257) centralized. This standard was drafted. China Inspection and Quarantine Science Research Institute, Shanghai Institute of Daily Chemical Industry. The main drafters of this standard. Ma Qiang, birch, Wang Chao, Xiao Haiqing, Yan Yan, Liu Qian, Ding Lan, exercise Wei, Shen Min, Kang Wei. Determination of chlorobutanol in cosmetics Gas chromatography - mass spectrometry1 ScopeThis standard specifies chlorobutanol in cosmetics by gas chromatography - mass spectrometry. This standard applies to creams, liquid, loose powder, shampoo, lipstick Cosmetics Determination chlorobutanol. The standard for chlorobutanol detection limit of 0.15mg/kg, the limit of quantification of 0.4mg/kg. Principle 2 By solvent extraction of the sample, after centrifugation, by gas chromatography - mass spectrometry, external standard.3 Reagents and materialsUnless otherwise specified, the reagents were of analytical grade. 3.1 Methanol. chromatographically pure. 3.2 ethanol. chromatography. 3.3 chlorobutanol standard substance. Formula C4H7Cl3O, CAS No. 57-15-8, purity of not less than 99%, the formula in Appendix A Figure A.1. 3.4 anhydrous sodium sulfate. ignited by 650 ℃ 4h placed in the dryer. 3.5 chlorobutanol standard stock solution. accurately weighed amount of chlorobutanol standard substance (accurate to 0.0001g), anhydrous ethanol (3.2) formulated at a concentration of 1000μg/mL standard stock solution, and stored in the dark at 4 ℃, can be used for three months. 3.6 50% methanol - ethanol solution. accurately weighed 50mL of methanol and 50mL of anhydrous ethanol, mix and reserve.4 instruments and equipment4.1 Gas chromatography - mass spectrometry (GC-MS) instrument. with electron impact ionization (EI). 4.2 Analysis of balance. a sense of the amount of 0.0001g and 0.001g. 4.3 centrifuge. speed of not less than 5000r/min. 4.4 ultrasonic bath. 4.5 plug cuvette. 10mL. 4.6 stoppered conical flask. 50mL. 4.7 plug teflon plastic centrifuge tube. 50mL. 4.8 microporous membrane. 0.45μm, organic phase. Step 5 Analysis 5.1 Sample Preparation 5.1.1 cream, liquid, loose powder, shampoo sample class Weigh 0.5g (accurate to 0.001g) sample in 50mL stoppered Erlenmeyer flask (4.6) was added 20mL50% methanol - ethanol solution ......Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of GB/T 29676-2013_English be delivered?Answer: Upon your order, we will start to translate GB/T 29676-2013_English as soon as possible, and keep you informed of the progress. The lead time is typically 1 ~ 3 working days. The lengthier the document the longer the lead time.Question 2: Can I share the purchased PDF of GB/T 29676-2013_English with my colleagues?Answer: Yes. The purchased PDF of GB/T 29676-2013_English will be deemed to be sold to your employer/organization who actually pays for it, including your colleagues and your employer's intranet.Question 3: Does the price include tax/VAT?Answer: Yes. 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