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GB/T 23834.2-2009 English PDF

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GB/T 23834.2-2009: Chemical analysis method for stannous sulfate -- Part 2: Determination of insoluble substance in hydrochloric acid -- Gravimetric method
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
GB/T 23834.2-2009189 Add to Cart 3 days Chemical analysis method for stannous sulfate -- Part 2: Determination of insoluble substance in hydrochloric acid -- Gravimetric method Valid

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Basic data

Standard ID: GB/T 23834.2-2009 (GB/T23834.2-2009)
Description (Translated English): Chemical analysis method for stannous sulfate -- Part 2: Determination of insoluble substance in hydrochloric acid -- Gravimetric method
Sector / Industry: National Standard (Recommended)
Classification of Chinese Standard: G10
Classification of International Standard: 71.060.01
Word Count Estimation: 8,858
Date of Issue: 2009-05-18
Date of Implementation: 2010-02-01
Regulation (derived from): PRC National Standard Approval Announcement 2009 No.6 (Total No.146)
Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary: This standard specifies the method for determination of tin in hydrochloric acid sulfate principle insoluble content, safety tips, general provisions, reagents, instrument, analysis steps and calculations. This section applies to the determination of stannous sulfate, hydrochloric acid insoluble content. Measuring range: 0. 001 to 0. 05%.

GB/T 23834.2-2009: Chemical analysis method for stannous sulfate -- Part 2: Determination of insoluble substance in hydrochloric acid -- Gravimetric method


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Chemical analysis method for stannous sulfate Part 2. Determination of insoluble substance in hydrochloric acid Gravimetric method. ICS 71.060.01 G10 National Standards of People's Republic of China Sulfite chemical analysis of tin Part 2. The hydrochloric acid insoluble matter - Gravimetric method Posted 2009-05-18 2010-02-01 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released

Foreword

GB/T 23834-2009 "sulfite chemical analysis of tin" is divided into six parts. --- Part 1. Determination of tin sulfate dichromate method --- Part 2. hydrochloric acid insoluble matter - Gravimetric method --- Part 3. the total amount of alkali and alkaline earth metal sulfates Gravimetric method --- Part 4. Determination of Lead and Copper by Flame Atomic Absorption Spectrometry --- Part 5. Determination of arsenic content diethyl dithiocarbamate spectrophotometry silver --- Part 6. Determination of iron content  phenanthroline spectrophotometry method This section GB/T 23834 Part 2. This part is proposed by the China Petroleum and Chemical Industry Association. This part of the National Standardization Technical Committee chemical inorganic chemicals Club (SAC/TC63/SC1) centralized. This section is responsible for drafting units. Fine Chemicals Group Co., Ltd., Yunnan Tin Group Co., Ltd., CNOOC Tianjin Chemical Research Design Institute. The main drafters of this section. Wang Hui Zhou, He Yingying, Highland, Guofeng Xin, Liu Ruo. This section first release. Sulfite chemical analysis of tin Part 2. The hydrochloric acid insoluble matter - Gravimetric method

1 Scope

This section specifies the method for determination of the principles of stannous sulfate in hydrochloric acid insoluble content, safety tips, general provisions, reagents, instruments, Analysis procedures and results of calculations. This section applies to the determination of stannous hydrochloric acid insoluble content of sulfuric acid. Measurement range. 0.001% to 0.05%.

2 Normative references

The following documents contain provisions which, through reference GB/T 23834 in this section constitute provisions of this section. For dated reference documents Member, all subsequent amendments (not including errata content) or revisions do not apply to this section, however, encouraged to reach under this section Research into whether the parties to the agreement to use the latest versions of these documents. For undated reference documents, the latest versions apply to this section. GB/T 603 chemical reagent test methods in the formulation and preparation of products (GB/T 603-2002, ISO 6353-1 with. 1982, NEQ) GB/T 6682-2008 analytical laboratory use specifications and test methods (ISO 3696. 1987, MOD) Preparations of HG/T 3696.3 inorganic chemical products, chemical analysis

3 PRINCIPLE OF THE METHOD

Soluble salt is stannous sulfate, stannous ion but easily hydrolyzed stannous hydroxide [Sn (OH) 2Ksp = 1.4 × 10-28], because The dissolution with hydrochloric acid, filtered, washed and dried to obtain the content of hydrochloric acid insolubles.

4 Safety Tips

Reagents used in this test method is corrosive, be careful when operating! As water immediately splashed on the skin or eyes Flushing, severe cases should be treated immediately.

5 General Provisions

This standard reagents and water, did not indicate when the other requirements, refer to analytically pure reagents and GB/T 6682-2008 stipulated three Grade water. Used in the test preparation and products, did not indicate when the other requirements, according to GB/T 603 or HG/T 3696.3 of preparation.

6 Reagents

6.1 hydrochloric acid; 6.2 hydrochloric acid solution. 2 + 1; 6.3 Silver nitrate solution. 10g/L.

7 instruments and equipment

7.1 sintered glass crucible. sand core pore size of 5μm ~ 15μm. Glass sand crucible should always use 1 + 1 hydrochloric acid boiling 15min ~ 30min, and then tap water rinse, washed three times with three water, After then dip in boiling water three 15min, hot filtration at 105 ℃ ± 2 ℃ under dried to constant weight.
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