GA/T 1008.12-2013 English PDF

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GA/T 1008.12-2013	439	Add to Cart	3 days	GC and GC-MS examination methods for drugs-Part 12: Chlordiazepoxide	Obsolete

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Basic data

Standard ID: GA/T 1008.12-2013 (GA/T1008.12-2013)
Description (Translated English): GC and GC-MS examination methods for drugs-Part 12: Chlordiazepoxide
Sector / Industry: Public Security (Police) Industry Standard (Recommended)
Classification of Chinese Standard: A92
Classification of International Standard: 13.130
Word Count Estimation: 11,167
Quoted Standard: GA/T 122; JJF 1059-1999
Regulation (derived from): Industry standard filing notice 2015 No. 4 (total 184)
Issuing agency(ies): Ministry of Public Security
Summary: This standard specifies the GC-MS qualitative analysis and gas chromatography (GC) quantitative analysis of clozapine. This standard is applicable to qualitative and quantitative examination and identification of clozapine in solid samples of drug cases.

GA/T 1008.12-2013: GC and GC-MS examination methods for drugs-Part 12: Chlordiazepoxide

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GC and GC-MS examination methods for drugs-Part 12. Chlordiazepoxide ICS 13.130 A92 People's Republic of China Public Security Industry Standards Common drugs by gas chromatography, gas chromatography - mass spectrometry Testing method Part 12. chlordiazepoxide Part 12. Chlordiazepoxide Issued on. 2013-01-16 2013-03-01 implementation People's Republic of China Ministry of Public Security

Table of Contents

Introduction Ⅲ 1 Scope 1 2 Normative references 1 3 Terms and definitions 4 Principle 1 5 Reagents and reference materials, instruments and apparatus volume 1 Qualitative analysis of 6

7 Quantitative Analysis

8 results of the evaluation 5 Appendix A (informative) external standard quantitation sample extraction operation parameters in Table 7 Annex B (informative) chlordiazepoxide related spectrum 8

Foreword

This section drafted in accordance with GB/T 1.1-2009 given rules. Please note that some content of this document may involve patents, the issuing authority of this document does not assume responsibility for the identification of these patents. GA/T 1008 "Common drugs by gas chromatography, gas chromatography - mass spectrometry test method" is divided into 12 parts. --- Part 1. opium, five-component; --- Part 2. morphine; --- Part 3. Cannabis three components; --- Part 4. cocaine; --- Part 5. Two-methylenedioxymethamphetamine amphetamine; --- Part 6. methadone; --- Part 7. methaqualone; --- Part 8. triazolam; --- Part 9. estazolam; --- Part 10. diazepam; --- Part 11. bromazepam; --- Part 12. chlordiazepoxide. This section GA/T 1008 Part 12. This part of the National Standardization Technical Committee for Standardization of Poison Analyses for Criminal Technology Technical Committee (SAC/TC179/SC1) mention And the focal point. This section drafted by. Ministry of Public Security Evidence Identification Center. The main drafters of this section. Gregory students, Chang Chun, Zheng Hui, Qian Zhenhua, Xu Peng, Huang Xing, Wang, Wang Wei Xin, Chang Ying, Liu Kelin. Common drugs by gas chromatography, gas chromatography - mass spectrometry Testing method Part 12. chlordiazepoxide

1 Scope

GA/T 1008 provisions of this part of the chlordiazepoxide gas chromatography - mass spectrometry (GC-MS) and qualitative analysis by gas chromatography (GC) quantitative analysis. This section applies to the qualitative and quantitative examination and identification of drug cases in solid samples of chlordiazepoxide.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein Member. For undated references, the latest edition (including any amendments) applies to this document. GA/T 122 toxicological analysis Terminology JJF1059-1999 Measurement Uncertainty and representation

3 Terms and Definitions

Terms and definitions GA/T 122 defined apply to this document. Principle 4 This method uses the internal standard method or external standard method for quality control of solid samples of suspected drug chlordiazepoxide organic solvent extraction using Gas chromatography - mass spectrometry (GC-MS) qualitative analysis by gas chromatography - flame ionization detector (GC-FID) to be given chlordiazepoxide Quantitative analysis. 5 Reagents and reference materials, instruments and appliances volume 5.1 Reagents and Standards The reagents used were of analytical grade. a) methanol. b) traceable standard substance. chlordiazepoxide. c) external standard quantitation using 1.0mg/mL chlordiazepoxide standard stock solution. Weigh chlordiazepoxide standard substance (based on the converted reference material purity Equal to 50.0mg of chlordiazepoxide), placed in a 50mL volumetric flask, add 20mL of methanol was dissolved by shaking, diluted with methanol to Scale, formulated as 1.0mg/mL standard stock solution chlordiazepoxide, home refrigerator freezer to save, save for 6 months. d) external standard quantitation using 0.1mg/mL chlordiazepoxide working standard solution. Pipette 1.0mg/mL chlordiazepoxide standard solution 5mL added To 50mL volumetric flask, diluted with methanol to the mark, formulated as 0.1mg/mL working standard solution chlordiazepoxide, home refrigerator cold Tibetan save, save time of 3 months. ......

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