GA/T 1008.10-2013 English PDF

Standard ID	USD	BUY PDF	Lead-Days	Standard Title (Description)	Status
GA/T 1008.10-2013	439	Add to Cart	3 days	GC and GC-MS examination methods for drugs-Part 10: Diazepam	Obsolete

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Basic data

Standard ID: GA/T 1008.10-2013 (GA/T1008.10-2013)
Description (Translated English): GC and GC-MS examination methods for drugs-Part 10: Diazepam
Sector / Industry: Public Security (Police) Industry Standard (Recommended)
Classification of Chinese Standard: A92
Classification of International Standard: 13.130
Word Count Estimation: 11,197
Quoted Standard: GA/T 122; JJF 1059-1999
Regulation (derived from): Industry standard filing notice 2015 No. 4 (total 184)
Issuing agency(ies): Ministry of Public Security
Summary: This standard specifies the qualitative analysis of diazepam by gas chromatography-mass spectrometry (GC-MS) and quantitative analysis by gas chromatography (GC). This standard is applicable to qualitative and quantitative examination of diazepam in solid

GA/T 1008.10-2013: GC and GC-MS examination methods for drugs-Part 10: Diazepam

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GC and GC-MS examination methods for drugs-Part 10. Diazepam ICS 13.130 A92 People 's Republic of China Public Security Industry Standard Gas Chromatography, Gas Chromatography - Mass Spectrometry of Common Drugs Testing method Part 10. Diazepam Part 10. Diazepam 2013-01-16 release 2013-03-01 implementation Issued by the Ministry of Public Security of the People 's Republic of China Directory Preface III 1 Scope 1 2 normative reference document 1 3 Terms and definitions 1 Principle 1 5 reagents and reference materials, instruments and measuring instruments 1 Qualitative analysis Quantitative analysis 8 Results 5 Appendix A (informative) External standard quantitative method Sample extraction operation parameter selection Table 7 Appendix B (informative) Diazepam Related Spectrum

Foreword

This part is drafted in accordance with the rules given in GB/T 1.1-2009. Please note that some of the contents of this document may relate to patents and that the issuer of this document does not assume responsibility for the identification of these patents. GA/T 1008 "common drug gas chromatography, gas chromatography - mass spectrometry test method" is divided into 12 parts. - Part 1. Five elements in opium; - Part 2. morphine; - Part 3. Three ingredients in cannabis; - Part 4. Cocaine; - Part 5. Dimethylenediamine Amphetamine; - Part 6. methadone; - Part 7. Ammonone; - Part 8. Triazolam; - Part 9. estazolam; - Part 10. Diazepam; - Part 11. Bromepam; - Part 12. Chlorotiazole. This section is part 10 of GA/T 1008. This part of the National Criminal Technology Standardization Technical Committee of the Standardization Subcommittee on Poisons Analysis (SAC/TC179/SC1) Out of charge. This part of the drafting unit. the Ministry of Public Security evidence identification center. The main drafters of this part. Gao Lisheng, Zhang Chunshui, Zheng Hui, Qian Zhenhua, Xu Peng, Huang Xing, Wang Yi, Wang Weixin, Chang Ying, Liu Keling. Gas Chromatography, Gas Chromatography - Mass Spectrometry of Common Drugs Testing method Part 10. Diazepam

1 Scope

This part of GA/T 1008 specifies the GC-MS qualitative analysis and gas chromatography (GC) quantification of diazepam analysis. This part is applicable to the qualitative and quantitative identification of diazepam in solid samples of drug cases.

2 normative reference documents

The following documents are indispensable for the application of this document. For dated references, only the dated edition applies to this article Pieces. For undated references, the latest edition (including all modifications) applies to this document. Glossary of Terminology for Poison Analysis Evaluation and Representation of Measurement Uncertainty JJF1059-1999

3 terms and definitions

The terms and definitions defined in GA/T 122 apply to this document.

4 principle

This method uses internal standard or external standard method for quality control, the suspected drug samples of solid diazepam organic solvent extraction, with Gas chromatography-mass spectrometry (GC-MS), and gas chromatography-hydrogen flame ionization detector (GC-FID) was used to determine diazepam Quantitative analysis. 5 reagents and reference materials, instruments and measuring instruments 5.1 Reagents and standard substances The reagents used were of analytical grade. a) Methanol. b) traceable standard substance. diazepam. c) External standard with 1.0mg/mL diazepam standard stock solution. Weigh diazepam standard substance (according to the standard material purity after conversion Equal to 50.0 mg of diazepam) was placed in a 50 mL volumetric flask, dissolved in 20 mL of methanol and dissolved in methanol Scale, prepared into 1.0mg/mL diazepam standard stock solution, set the refrigerator frozen storage, save time of 6 months. d) external standard quantitative 0.1mg/mL diazepam standard working solution. remove 1.0mg/mL diazepam standard stock solution 5mL added To 50mL volumetric flask, diluted with methanol to the mark, prepared into 0.1mg/mL diazepam standard working fluid, set the refrigerator in the cold Save, save time for 3 months. ......

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