GA/T 1008.1-2013 English PDF

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GA/T 1008.1-2013	479	Add to Cart	3 days	GC and GC-MS examination methods for drugs-Part 1: Five components in opium	Obsolete

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Basic data

Standard ID: GA/T 1008.1-2013 (GA/T1008.1-2013)
Description (Translated English): GC and GC-MS examination methods for drugs-Part 1: Five components in opium
Sector / Industry: Public Security (Police) Industry Standard (Recommended)
Classification of Chinese Standard: A92
Classification of International Standard: 13.130
Word Count Estimation: 12,116
Quoted Standard: GA/T 122; JJF 1059-1999
Regulation (derived from): Industry standard filing notice 2014 No. 4 (total 172)
Issuing agency(ies): Ministry of Public Security
Summary: This standard specifies the qualitative analysis of morphine, codeine, phenobarbital, papaverine, naloxerine by gas chromatography-mass spectrometry (GC-MS) and gas chromatography (GC) quantitative analysis of morphine. This standard applies to morphine,

GA/T 1008.1-2013: GC and GC-MS examination methods for drugs-Part 1: Five components in opium

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GC and GC-MS examination methods for drugs-Part 1. Five components in opium ICS 13.130 A92 People 's Republic of China Public Security Industry Standard Gas Chromatography, Gas Chromatography - Mass Spectrometry of Common Drugs Testing method Part 1. Five Ingredients in Opium Part 1. Fivecomponentsinopium 2013-01-16 release 2013-03-01 implementation Issued by the Ministry of Public Security of the People 's Republic of China Directory Preface III 1 Scope 1 2 normative reference document 1 3 Terms and definitions 1 Principle 1 5 reagents and reference materials, instruments and measuring instruments 1 Qualitative analysis Quantitative analysis 8 Results 5 Appendix A (informative) Related spectrum of active ingredients in opium 7

Foreword

This part is drafted in accordance with the rules given in GB/T 1.1-2009. Please note that some of the contents of this document may relate to patents and that the issuer of this document does not assume responsibility for the identification of these patents. GA/T 1008 "common drug gas chromatography, gas chromatography - mass spectrometry test method" is divided into 12 parts. - Part 1. Five elements in opium; - Part 2. morphine; - Part 3. Three ingredients in cannabis; - Part 4. Cocaine; - Part 5. Dimethylenediamine Amphetamine; - Part 6. methadone; - Part 7. Ammonone; - Part 8. Triazolam; - Part 9. estazolam; - Part 10. Diazepam; - Part 11. Bromepam; - Part 12. Chlorotiazole. This section is part 1 of GA/T 1008. This part of the National Criminal Technology Standardization Technical Committee of the Standardization Subcommittee on Poisons Analysis (SAC/TC179/SC1) Out of charge. This part of the drafting unit. the Ministry of Public Security evidence identification center. The main drafters of this part. Gao Lise, Zheng Hui, Zhang Chunshui, Qian Zhenhua, Xu Peng, Huang Xing, Wang Yi, Wang Weixin, Chang Ying, Liu Keling. Gas Chromatography, Gas Chromatography - Mass Spectrometry of Common Drugs Testing method Part 1. Five Ingredients in Opium

1 Scope

This section of GA/T 1008 specifies the gas chromatographic properties of opium in the active ingredient morphine, codeine, tibainine, papaverine, (GC-MS) qualitative analysis and morphine gas chromatography (GC) quantitative analysis. This part is applicable to the qualitative test of morphine, codeine, tibain, papaverine, and cacrine in solid samples. Quantitative inspection and identification.

2 normative reference documents

The following documents are indispensable for the application of this document. For dated references, only the dated edition applies to this article Pieces. For undated references, the latest edition (including all modifications) applies to this document. Glossary of Terminology for Poison Analysis Evaluation and Representation of Measurement Uncertainty JJF1059-1999

3 terms and definitions

The terms and definitions defined in GA/T 122 apply to this document.

4 principle

This method uses internal standard or external standard method for quality control, the suspected drug samples of solid morphine, codeine, babaine, poppy (GC-MS), and gas chromatography-hydrogen flame ionization (GC-MS) was carried out by gas chromatography-mass spectrometry (GC-MS) The detector (GC-FID) was used to quantitatively analyze morphine. 5 reagents and reference materials, instruments and measuring instruments 5.1 Reagents and standard substances The reagents used were of analytical grade. a) Methanol. b) chloroform. c) isopropanol. d) 0.5% glacial acetic acid aqueous solution. take 0.5mL glacial acetic acid in 100mL volumetric flask, add water to the volume, the preparation of 0.5% Glacial acetic acid aqueous solution. e) 0.1M aqueous sodium hydroxide solution. take 0.46g sodium hydroxide solid in a 100mL volumetric flask, add water to the volume, the preparation Into 0.1M aqueous sodium hydroxide solution. ......

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