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GB/T 5505-2008 English PDF

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GB/T 5505-2008: Inspection of grain and oils -- Determination of the ash content by incineration
Status: Obsolete

GB/T 5505: Historical versions

Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
GB/T 5505-2008239 Add to Cart 3 days Inspection of grain and oils -- Determination of the ash content by incineration Obsolete
GB/T 5505-1985199 Add to Cart 2 days Inspection of grain and oilseeds--Methods for determination of ash content Obsolete

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Basic data

Standard ID: GB/T 5505-2008 (GB/T5505-2008)
Description (Translated English): Inspection of grain and oils -- Determination of the ash content by incineration
Sector / Industry: National Standard (Recommended)
Classification of Chinese Standard: X04
Classification of International Standard: 67.050
Word Count Estimation: 6,630
Date of Issue: 2008-08-04
Date of Implementation: 2008-12-01
Older Standard (superseded by this standard): GB/T 5505-1985
Quoted Standard: GB/T 5497
Regulation (derived from): National Standard Approval Announcement 2008 No.14 (Total No.127)
Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary: This standard specifies the food, principle determination of ash in oil, reagents, instrument, analytical procedures and the results of calculations. This standard applies to food, determination of the ash content of the oil.

GB/T 5505-2008: Inspection of grain and oils -- Determination of the ash content by incineration

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Inspection of grain and oils. Determination of the ash content by incineration ICS 67.050 X04 National Standards of People's Republic of China Replacing GB/T 5505-1985 Inspection of grain - Determination of ash Posted 2008-08-04 2008-12-01 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released

Foreword

This standard is GB/T 5505-1985 "of grain and oilseeds - Determination of ash test" amendments. This standard and GB/T 5505-1985 main technical differences are as follows. --- The high temperature furnace burning temperature from 500 ℃ ~ 550 ℃ modified to 550 ℃ ± 10 ℃. Since the implementation of this standard, instead of the GB/T 5505-1985. The standard proposed by the National Food Authority. This standard by the National Standardization Technical Committee OILS. This standard was drafted. Beijing foodstuff and Inspection. The main drafters of this standard. Guo Qin, Shang Yane, Fan gull, Liu Jie. This standard replaces the standards previously issued as follows. --- GB/T 5505-1985. Inspection of grain - Determination of ash

1 Scope

This standard specifies the food, fuel ash in principle determined, reagents, instruments, analytical procedures, and the results of calculations. This standard applies to food, the determination of ash content in the oil.

2 Normative references

The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard. GB/T 5497 grain and oilseeds - Determination of water test 3 550 ℃ burning method 3.1 Principle The sample was 550 ℃ ± 10 ℃ ashing temperature to completely burning the volatile organic compounds after weighing the residues. 3.2 Reagents 3.2.1 Ferric chloride. AR. 3.2.2 ferric chloride solution (5g/L). Weigh 0.5g of ferric chloride dissolved in 100mL blue-black ink. 3.3 Instrument 3.3.1 muffle furnace. also known as Mao Fu furnace, Muffle furnace, high temperature furnace, capable of producing more than 550 ℃ high temperature, and temperature control. 3.3.2 Analytical Balance. a sense of the amount of 0.0001g. 3.3.3 porcelain crucible. a capacity of 18mL ~ 20mL. 3.3.4 dryers. built-effective color gel. 3.3.5 crucible tongs. long handle and short handle. 3.4 Analysis Steps 3.4.1 Moisture According to GB/T 5497 Determination of sample water (W). 3.4.2 Sample Preparation Samples were prepared according to GB/T in 5497 requirements. 3.4.3 crucible process Take a clean, dry porcelain crucible with a brush dipped in a solution of ferric chloride blue or black ink in the crucible ID number and then placed in a crucible 550 ℃ ± 10 ℃ muffle furnace burning 30min ~ 60min, to move the crucible furnace door, until red hot crucible disappear, transferred to a dryer The cooling to room temperature, taken out and weighed crucible mass, repeated burning, cooling, weighing, until the mass difference before and after no more than two 0.0002g, record crucible mass (m1 0). 3.4.4 Sample Determination Weigh and mix the sample (m1) 2g ~ 3g, accurate to 0.0002g, to deal with a good crucible, the crucible on the furnace, staggered crucible Cover, heating the sample until completely carbonized. Then, the crucible in a muffle furnace 550 ℃ ± 10 ℃, the first on the mouth for a moment, then moved Furnace, staggered crucible lid, close the door, at 550 ℃ ± 10 ℃ burning 2h ~ 3h. In the burning process, the crucible should swap positions 1 to 2 times, burning sample to black soot disappeared into a gray so far. Moving to the crucible furnace door, to be red hot crucible disappear After transfer to cool to room temperature in a desiccator, and weigh. Then burn 30min, cooling, weighing, until constant mass (m1). Last burning quality
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