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GB/T 35772-2017 English PDF

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GB/T 35772-2017: Rapid detection of phthalate esters in polyvinyl chloride products -- Infra-red spectrometric method
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
GB/T 35772-2017199 Add to Cart 3 days Rapid detection of phthalate esters in polyvinyl chloride products -- Infra-red spectrometric method Valid

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GB/T 36805.2   GB/T 36374.2   GB/T 36374.1   GB/T 18964.1   GB/T 12008.7   

Basic data

Standard ID: GB/T 35772-2017 (GB/T35772-2017)
Description (Translated English): Rapid detection of phthalate esters in polyvinyl chloride products -- Infra-red spectrometric method
Sector / Industry: National Standard (Recommended)
Classification of Chinese Standard: G31
Classification of International Standard: 83.040.30
Word Count Estimation: 10,143
Date of Issue: 2017-12-29
Date of Implementation: 2018-04-01
Regulation (derived from): National Standards Bulletin 2017 No. 32
Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China

GB/T 35772-2017: Rapid detection of phthalate esters in polyvinyl chloride products -- Infra-red spectrometric method


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Rapid detection of phthalate esters in polyvinyl chloride products - Infra-red spectrometric method ICS 83.040.30 G31 National Standards of People's Republic of China Polyvinyl chloride products in the phthalates Rapid detection methods infrared spectroscopy 2017-12-29 Posted 2018-04-01 implementation General Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China China National Standardization Administration released

Foreword

This standard was drafted in accordance with the rules given in GB/T 1.1-2009. This standard by the National Quality Supervision Key Products Testing Methods Standardization Technical Committee (SAC/TC374) and focal point. This standard was drafted unit. Guangzhou Quality Supervision, Inspection and Research Institute, the quality of Warner (Beijing) Technology Center Co., Ltd., the Federation of inspection (North Beijing) Quality Inspection Technology Institute Co., Ltd., Guangdong Yulan Group Co., Ltd., SGS Standard Technical Services Co., Ltd., Zhejiang Bond Pipe Co., Ltd., China National Nuclear Tuopu (Hubei) New Materials Co., Ltd., Zhejiang Tongzhengge Plastic Technology Co., Ltd., Tupperware Test Group Co., Ltd. Company, China Measurement and Certification Group Co., Ltd. test. The main drafters of this standard. Duan Xiaoxia, Shen Guanglai, Wang Yong, Yang Fengbo, Ma Weijuan, Wang Xiaoru, Sun Shizhen, Wan Qingtang, Zhang Xiaoqiong, He Xiaoyan, Zhao Chengfang, Han Zhongyuan, Tang Qingzhong, Song Wei, Yang Yang. Polyvinyl chloride products in the phthalates Rapid detection methods infrared spectroscopy

1 Scope

This standard specifies the principle of using infrared spectroscopy to quickly detect phthalate plasticizers in PVC products, reagents and materials, Equipment, qualitative screening, quantitative analysis and calculation of results This standard applies to the total content of phthalates not less than 1% of the qualitative and quantitative detection of PVC materials.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version applies to this article Pieces. For undated references, the latest edition (including all amendments) applies to this document. GB/T 6040-2002 General rules of infrared spectrometry

3 principle

Preparing a series of standard samples containing phthalate plasticizers, using infrared spectrometer to collect the infrared spectrum data of the standard, according to the standard red Partial Least Squares (PLS) stoichiometry model was established for the characteristic peaks of external spectra, and then the infrared spectra of unknown samples were scanned. 1580cm-1 and 1600cm-1 ring skeleton characteristic absorption peak qualitative analysis, and then using the stoichiometric model of unknown samples of o-benzene two Formate plasticizer total content.

4 Reagents and materials

4.1 Phthalate standards Purity ≥98%, see Appendix A. 4.2 Non-phthalate plasticizers Dioctyl terephthalate (DOTP) and trioctyl trimellitate (TOTM), purity ≥97%. 4.3 standard sample with polyvinyl chloride (PVC) resin. 4.4 Tetrahydrofuran (THF). Spectral purity.

5 equipment

5.1 Fourier transform infrared spectrometer in line with the provisions of GB/T 6040-2002 4.2.1. 5.2 Attenuated Total Reflection (ATR) Accessories. The test crystal is germanium (Ge) crystal. 5.3 Analytical balance. Accuracy of 0.01mg. 5.4 Drying oven temperature fluctuations ± 2 ℃.

6 qualitative screening

6.1 sample preparation Take a flat surface of the test sample, so that it can be close to the ATR attachment crystal surface.
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