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GB/T 32178-2015 English PDF

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GB/T 32178-2015: Determination of chromium (VI) in chrome refractories -- Spectrometric method
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
GB/T 32178-201578 Add to Cart 1 days Determination of chromium (VI) in chrome refractories -- Spectrometric method Valid

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Basic data

Standard ID: GB/T 32178-2015 (GB/T32178-2015)
Description (Translated English): Determination of chromium (VI) in chrome refractories -- Spectrometric method
Sector / Industry: National Standard (Recommended)
Classification of Chinese Standard: Q40
Classification of International Standard: 81.080
Word Count Estimation: 7,740
Date of Issue: 2015-12-10
Date of Implementation: 2017-01-01
Quoted Standard: GB/T 6682
Regulation (derived from): National Standard Announcement 2015 No.38
Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary: This standard specifies the method for the determination spectroscopy for chemical analysis of chromium-containing refractories of hexavalent chromium. This standard applies to the determination of hexavalent chromium range of less than 500 ��g/g.

GB/T 32178-2015: Determination of chromium (VI) in chrome refractories -- Spectrometric method

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of chromium (Ⅵ) in chrome refractories - Spectrometric method ICS 81.080 Q40 National Standards of People's Republic of China Hexavalent chromium-containing refractories Issued on. 2015-12-10 2017-01-01 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released

Table of Contents

Introduction Ⅲ 1 Scope 1 2 Normative references 1 3 Test principle 1 4 device 1 5 Reagent 1 6 Sample Preparation 2 7 Measurement 2 8 calculation results 2 9 allows poor 3 3 10 test reports Appendix A (normative) Acceptance value analysis program 4

Foreword

This standard was drafted in accordance with GB/T 1.1-2009 given rules. Please note that some of the content of this document may involve patents. Release mechanism of the present document does not assume responsibility for the identification of these patents. This standard by the National Standardization Technical Committee Refractories (SAC/TC193) and focal points. This standard is mainly drafted by. Sinosteel Luoyang Institute of Refractories Co., Ltd., Beijing Lier High Temperature Materials Co., Ltd. The main drafters of this standard. Caohai Jie, Zhao Ji increase, Zhangzhou Ming, Han Dan, Liu Li, Huang Fei, Wang Hui, Sunshou Qi. Hexavalent chromium-containing refractories Spectrophotometry

1 Scope

This standard specifies the method for the determination spectroscopy for chemical analysis of chromium-containing refractories of hexavalent chromium. This standard applies to the determination of hexavalent chromium range of less than 500μg/g. NOTE. If the dispensing amount is reduced to 10mL, the measure extended to 1250μg/g.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein Member. For undated references, the latest edition (including any amendments) applies to this document. Laboratory use specifications and test methods GB/T 6682 Analysis

3 Test principle

Sample hexavalent chromium hydroxide and sodium carbonate dissolved in a mixed solution of trivalent chromium is not dissolved in this alkaline solution, ammonia dissolved hexavalent chromium and diphenyl Urea generated purple color, absorbance was measured in a spectrophotometer at a wavelength of 540nm ~ 550nm.

4 Device

4.1 Analytical balance (the amount being 0.1mg). 4.2 Glass Container, A Class. 4.3 Spectrophotometer. 4.4 automatic temperature control oven. 4.5 heating magnetic stirrer.

5 Reagents

5.1 General Reagents were of analytical grade, water conductivity lower than 2μS/cm of water, or in compliance with GB/T 6682 requirements in third grade water. There are commercially available Permit the solution can also be used. 5.2 alkali solution Weigh 30g of sodium carbonate, 20g of sodium hydroxide dissolved in water, the volume 1000mL, and mix, using a formulation today. 5.3 Hexavalent chromium storage solution The benchmark potassium dichromate reagent at 110 ℃ ± 10 ℃ drying, weighed 0.3536g dissolved in 200mL of water, the volume 500mL, and mix. This solution is a chromium content of 250mg/L.
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