GB/T 29170-2012 English PDF

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GB/T 29170-2012: Petroleum and natural gas industries -- Drilling fluids -- Laboratory testing
Status: Valid

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Basic data

Standard ID: GB/T 29170-2012 (GB/T29170-2012)
Description (Translated English): Petroleum and natural gas industries -- Drilling fluids -- Laboratory testing
Sector / Industry: National Standard (Recommended)
Classification of Chinese Standard: E13
Classification of International Standard: 75.020
Word Count Estimation: 95,965
Quoted Standard: GB/T 261; GB/T 262; GB/T 1884; GB/T 3535; GB/T 5005-2010; GB/T 6682-2008; GB/T 16783.1; GB/T 16783.2; ISO 91-1-1992; ISO 3007; ISO 3104; ISO 3405-2011; ISO 3839; ASTM D1141; ASTM D4052; ASTM D5186; ASTM E100; IP 391
Adopted Standard: ISO 10416-2008, MOD
Regulation (derived from): National Standards Bulletin No. 41 of 2012
Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary: This standard specifies the water recycling system (hereinafter referred to as " water plant") classification, technology portfolio, general requirements, selection, testing and acceptance requirements. This standard applies to agricultural water, industr

GB/T 29170-2012: Petroleum and natural gas industries -- Drilling fluids -- Laboratory testing

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Petroleum and natural gas industries. Drilling fluids. Laboratory testing ICS 75.020 E13 National Standards of People's Republic of China Oil drilling and natural gas industries laboratory tests (ISO 10416.2008, MOD) Issued on. 2012-12-31 2013-07-01 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released

Table of Contents

Preface Ⅶ Introduction Ⅷ 1 Scope 1 2 Normative references 1 3 Terms and definitions 2 4 Symbols and abbreviations 2 4.1 Symbols 2 4.2 Abbreviations 4 The physical properties of barite powder 4 5 5.1 Overview 4 5.2 Reagents and Instruments 4 Sampling 5 5.3 5.4 Calculation of water 5 5.5 sieve residue analysis 6 5.6 Settlement of 6 6 barite powder rheological properties of the drilling fluid 10 6.1 Overview 10 6.2 Reagents and Instruments 11 6.3 based drilling fluid slurry preparation 11 6.4 Rheological test 12 6.5 Calculation 12 7 aggravate abrasive material 13 7.1 Overview 13 7.2 Reagents and Instruments 13 7.3 abrasive test 13 8 drilling barite powder mercury content 14 8.1 Overview 14 8.2 Reagents and Instruments 15 8.3 Preparation of standard solution of mercury 16 Sample digestion 16 8.4 8.5 recovery test mercury digestion period of 16 8.6 standard solution and sample analysis 16 8.7 Calculation 17 9 drilling barite powder, cadmium and lead content 17 9.1 Overview 17 9.2 Reagents and Instruments 17 Cd and Pb compound preparation 9.3 standard solution of 18 Sample digestion 18 9.4 9.5 standard solution and sample analysis 18 9.6 Calculation 19 10 drilling barite powder with arsenic content of 19 10.1 Overview 19 10.2 Reagents and Instruments 19 20 10.3 Preparation of standard solution 10.4 20 sample digestion 10.5 Analysis of the standard solution and the sample solution 21 21 10.6 Calculation 11 bridge plugging material 21 11.1 Overview 21 21 11.2 Instrument 11.3 Preparation of test drilling 22 11.4 Static test program slit 22 11.5 dynamic test procedure slit 22 11.6 Static test bed program 22 marbles 11.7 marbles dynamic test bed program 23 11.8 Static test program 23 balls bed 11.9 ball dynamic test bed program 23 12 fluid loss additive 23 12.1 Overview 23 12.2 Reagents and Instruments 23 12.3 Base paste formulated to claim 25 12.4 saturated brine drilling fluid 25 12.5 High hardness saturated brine drilling fluid 25 12.6 10% KCl drilling fluid 25 12.7 Pre-hydrated bentonite slurry 26 12.8 artificial seawater drilling fluid 26 12.9 Low concentration brine drilling fluid 26 12.10 27 drilling calcium treatment 12.11 low solids non-dispersed drilling fluid 27 12.12 Freshwater lignosulfonate drilling 27 12.13 Initial performance testing 28 After heat aging performance test 12.14 28 13 cuttings and commodity bentonite methylene blue test (MBT) 28 13.1 cuttings methylene blue capacity 28 13.2 Goods Bentonite methylene blue capacity 31 13.3 Solid content 32 Deflocculation diluent rating 32 14 14.1 Overview 32 14.2 Reagents and Instruments 33 14.3 Moisture measurement program 33 14.4 Calculation of water 34 14.5 Base paste formulated 34 34 14.6 Calculation 14.7 Determination of flow variability 35 14.8 diluent computing efficiency 36 15 test drilling 36 oil base 15.1 Overview 36 15.2 Reagents and Instruments 36 15.3 density, relative density (specific gravity), or API Gravity --- liquid density method (in line with the provisions of GB/T 1884's) 36 15.4 digital density meter measuring liquid density and relative density (in line with the provisions of ASTMD4052) 36 15.5 kinematic viscosity of transparent and opaque liquid petroleum --- calibration capillary method (ISO 3104 compliance) is 37 15.6 distillate (of compliance with ISO 3405) 37 15.7 aniline point and mixed aniline point (in line with GB/T 262-2010 requirements) 37 15.8 pour point (in line with GB/T 3535 provisions) 38 15.9 Pensky - Martens closed cup flash point test method (in line with GB/T 261 requirements) 38 15.10 aromatics content (in compliance with IP391 or ASTMD5186) 38 16 potassium ion content --- Ion Selective Electrode 39 16.1 Overview 39 16.2 Reagents and Instruments 39 16.3 Electrode Preparation 40 16.4 operating system to check the electrode 40 16.5 Concentration direct reading instrument measurement 41 16.6 millivolts digital or analog output measurement instrument 41 17 Calcium content --- Ion Selective Electrode 41 17.1 Overview 41 17.2 Reagents and Instruments 42 17.3 Electrode Preparation 42 17.4 operating system to check the electrode 43 17.5 Concentration direct reading instrument measurement 43 17.6 millivolts digital or analog output measurement instrument 43 18 Sodium content --- Ion Selective Electrode 44 18.1 Overview 44 18.2 Reagents and Instruments 44 Prepare and check the electrode system 45 18.3 18.4 Concentration direct reading instrument measurement 45 18.5 millivolts digital or analog output measurement instrument 46 The true density of solid density --- 19 46 Law 19.1 Overview 46 46 19.2 Instrument 19.3 Test Procedure Act 46 --- true density 19.4 --- calculate the true density of France 47 20 solid density --- air Pyknometer 47 20.1 Overview 47 47 20.2 Instrument 20.3 Test procedure --- air Pyknometer 48 20.4 Calculation --- air Pyknometer 48 Conservation of water-based drilling fluid 21 48 21.1 Overview 48 Conventional drilling operations 21.2 sample preparation, processing and testing 48 Sample preparation and maintenance of drilling fluid at room temperature 21.3 49 21.4 Drilling Fluid temperature [temperature to 65 ℃ (150 ℉)] Conservation 50 High temperature drilling fluid 21.5 [higher than 65 ℃ (150 ℉)] Conservation 51 21.6 high temperature curing tanks inert and chemical compatibility 53 21.7 Conservation drilling needed supplies and services 53 22 oil-based drilling fluids conservation 54 22.1 Overview 54 54 22.2 Instrument Conventional drilling operations 22.3 sample preparation, processing and testing 55 22.4 drilling fluid at room temperature curing 56 22.5 Drilling Fluid temperature [temperature to 65 ℃ (150 ℉)] Conservation 56 High temperature drilling fluid 22.6 [higher than 65 ℃ (150 ℉)] Conservation 57 22.7 high temperature curing tanks inert and chemical compatibility 58 22.8 Conservation drilling needed supplies and services 59 Scroll shale recovery test 23 59 23.1 Overview 59 23.2 Reagents and Instruments 59 23.3 Determination program 60 61 23.4 Calculation 24 drilling material --- high viscosity polyanionic cellulose (PAC-HV) (General) 61 24.1 Overview 61 24.2 Moisture 61 24.3 PAC-HV test fluid containing the test program 62 25 drilling materials --- low viscosity polyanionic cellulose (PAC-LV) 64 25.1 Overview 64 25.2 Moisture 64 25.3 PAC-LV containing the test fluid measurement program 65 26 invert emulsion drilling fluid formulation and evaluation 67 26.1 Overview 67 26.2 Reagents and Instruments 67 26.3 based slurry mixing procedure 68 26.4 Performance Test drilling fluid base mud 69 Sample preparation 26.5 pollution of the sea 69 Evaluation of soil contaminated samples preparation 26.6 69 26.7 composite brine sample preparation contamination 69 26.8 hot rolling conservation program 69 26.9 stationary conservation program 70 26.10 after curing test program 70 27 Determination of drilling HTHP filtration loss 70 screwed lid type permeability tester closure 27.1 Overview 70 27.2 Safety Precautions 70 27.3 Instrument --- screw lid closure type permeability tester 72 27.4 HTHP Filtration test program 73 76 27.5 end of the test and removal 27.6 Data Report 77 28 threaded lid sealing formula permeability measured drilling HTHP filtration loss 78 28.1 Overview 78 28.2 Safety Precautions 78 28.3 Instrument --- threaded lid closure type permeability tester 79 28.4 HTHP Filtration test program 81 83 28.5 end of the test and removal 28.6 Data Report 84 Appendix A (informative) This standard and ISO 10416.2008 technical differences and their reasons 85 References 86

Foreword

This standard was drafted in accordance with GB/T 1.1-2009 given rules. This standard uses redrafted Law Amendment uses ISO 10416.2008 "oil and gas industry drilling laboratory tests" (English Version). This standard and ISO 10416.2008 technical differences exist compared to the terms of these differences involved have been incorporated into the body and through the outer Vertical singlet side margin position (|) have been marked, the list given in Appendix A corresponding technical differences and their causes. This standard also made the following editorial changes. a) use the "standard" instead of "this International Standard"; '.' B) with a decimal point instead of a comma as the decimal point, ''; c) the text of the original text has been corrected the wrong place. 1) Original Table 2, 3.31 and 3.20 to be exchanged; 2) Original 8.2.16 in 8mm (3/16in) should be changed to 8mm (5/16in); 3) should be replaced by the original 9.5.5 228.8nm 283.3nm; 5) Original 14.2.7 and 26.2.6 in 10000r/min ± 100r/min should be changed to 1000r/min ± 100r/min; 6) should be replaced in its original 14.5.1 in 350g 360g; 7) Original 14.7.1 in 750r/min ± 50r/min should be changed to 7500r/min ± 500r/min; 8) should be replaced by the original 16.2.3 in 5mol 5mol/L; 9) the original formula (26) should be replaced in md m0; 10) Original 24 23.1.1 to 24.1.1; 11) Original 24.3.1.10 and 25.3.1.10 should be replaced in the 150 ℉ 140 ℉; 12) Original 25.2.1.1 in 25 ℃ ± 1 ℃ (77 ℉ ± 3 ℉) should be changed to 105 ℃ ± 3 ℃ (220 ℉ ± 5 ℉); 13) Original 26.4.1 in 50 ℃ (300 ℉) should be changed to 50 ℃ (120 ℉); 14) Original 27.4.1.3 and 28.4.1.3 in 6 ℃ (10 ℉) should be changed to 6 ℃ (43 ℉); 15) The original 28.2.6.1 6200kPa (460psi) should be changed to 6200kPa (900psi); 16) The original 28.3.1.4 9.87 × 10-16m2 ~ 9.87 × 10-11 m2 (100 mD ~ 100D) should be replaced 1.02 × 10-13m2 ~ 1.02 × 10-10m2 (100mD ~ 100D). This standard by the National Standardization Technical Committee of Oil and Gas (SAC/TC355) and focal points. This standard was drafted. China Research Institute of Petroleum and Chemical Corporation Zhongyuan Petroleum Exploration Bureau drilling engineering technology. The main drafters of this standard. Zhenjian Wu, Meng Lei Zu, WANG Xing-wu, Zhang Qilin, Mengli Yan, Song Shijun, ANS.

Introduction

Determination of drilling fluid materials used in this standard is referenced from APIRP13I seventh edition/ISO 10416.2002 [2]. This standard provides More and more rigorous testing methods to ensure the reproducibility and accuracy of test results. This standard applies to laboratory tests, if the site has More sophisticated equipment, through strict control of experimental conditions, can also be used for on-site drilling tests. This standard is used to test drilling site maintenance unconventional performance, and field testing standards GB/T 16783.1 and GB/T 16783.2 compared to test results or more accurately, or to provide on-site testing standard does not mention the performance test method. Users of this standard process can be made more or different requirements according to the special requirements of this standard is not intended to prevent vendors push Or a user acceptance test in favor of improvements in technology and innovative alternative products or engineering technology programs. When there are alternative products or technologies introduced , The supplier shall submit their differences with the technical specifications of this standard. If the test requires the use of hazardous chemicals, the user of this standard should have the appropriate knowledge and acceptance of the use and handling of these chemicals Training. Users should comply with local, regional and national labor laws and the HSE regulations. The standard example of a footnote apparatus, reagents and materials are examples of suitable commercially available products. This information is given for the convenience of the standard The user does not imply an endorsement of these products, if other equivalent product has the same effect, you can use these equivalent products. Oil drilling and natural gas industries laboratory tests

1 Scope

This standard specifies the method for laboratory testing of materials and drilling mud physical, chemical, rheological properties. This standard applies to water-based drilling fluids, oil-based drilling fluids and other fluid-based solutions or man made. This standard does not apply to control drilling fluid properties detailed manual. Since the test temperature and stirring conditions on drilling performance significantly The present standard gives the recommended test temperature and stirring conditions.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein Member. For undated references, the latest edition (including any amendments) applies to this document. GB/T 261 Flash Point by Pensky - Martens closed cup method (GB/T 261-2008, ISO 2719.2002, MOD) GB/T 262 Petroleum products and hydrocarbon solvents aniline point and mixed aniline point measurement method (GB/T 262-2010, ISO 2977.1997, MOD) GB/T 1884 crude oil and liquid petroleum products - Laboratory determination of density (density meter method) (GB/T 1884-2000, eqv ISO 3675.1998) GB/T 3535 Petroleum products - Determination of pour point (GB/T 3535-2006, ISO 3016.1994, MOD) GB/T 5005-2010 drilling material specification (ISO 13500.2008, MOD) GB/T 6682-2008 analytical laboratory use specifications and test methods (ISO 3696. 1987, MOD) GB/T 16783.1 Petroleum and natural gas industries - Field testing of drilling fluids - Part 1. Water-based drilling fluids GB/T 16783.2 Petroleum and natural gas industries - Field testing of drilling fluids - Part 2. Oil-based drilling fluids (GB/T 16783.2- 2012, ISO 10414-2.2002, MOD) ISO 91-1.1992 Petroleum Measurement Tables - Part 1. 60 ℉ to 15 ℃ and the temperature of the standard table (Petroleum measurementtables-Part 1. Tablesbasedonreferencetemperaturesof15 ℃ and60 ℉) ISO 3007 Petroleum products and crude oil measurement Reid vapor pressure (Reid) Act (Petroleumproductsandcrudepe- troleum-Determinationofvapourpressure-Reidmethod) Determination and calculation of dynamic viscosity ISO 3104 Petroleum products - Transparent and opaque liquids kinematic viscosity (Petroleum products-Transparentandopaqueliquids-Determinationofkinematicviscosityandcalculationof dynamicviscosity) Determination (Petroleumproducts-Determinationofdis- distillation characteristics of petroleum products under pressure 2011. ISO 3405 tilationcharacteristicsatatmosphericpressure) ISO 3839 Petroleum products distillates and aliphatic olefins - Determination of bromine number potentiometric titration (Petroleumproducts-Deter- minationofbrominenumberofdistilatesandaliphaticolefins-Electrometricmethod) ASTMD1141 seawater substitutes (Standardpracticeforpreparationofsubstituteoceanwater) ASTMD4052 digital density meter test method for determining the density and relative density of the liquid (Standardtestmethodforden- sityandrelativedensityofliquidsbydigitaldensitymeter) ASTMD5186 measured diesel and aviation turbine fuel aromatic content and polynuclear aromatics content by supercritical fluid chromatography Standard Test Method (Standardtestmethodfordeterminationofaromaticcontentandpolynucleararomatic ......

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