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GB/T 28732-2012 English PDF

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GB/T 28732-2012: Determination of total sulfur in solid biofuels
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
GB/T 28732-2012189 Add to Cart 3 days Determination of total sulfur in solid biofuels Valid

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Basic data

Standard ID: GB/T 28732-2012 (GB/T28732-2012)
Description (Translated English): Determination of total sulfur in solid biofuels
Sector / Industry: National Standard (Recommended)
Classification of Chinese Standard: D21
Classification of International Standard: 75.160.10
Word Count Estimation: 8,864
Quoted Standard: GB/T 212; GB/T 214; GB/T 21923
Regulation (derived from): National Standards Bulletin 2012 No. 28
Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary: This standard specifies the use Ai Shika France and Coulomb Titration solid biomass fuels Method summary of total sulfur, reagents and materials, equipment, testing procedures, results calculation and precision. Arbitration analysis, using Ai Shika method

GB/T 28732-2012: Determination of total sulfur in solid biofuels

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
ICS75.160.10 D21 National Standards of People's Republic of China Solid biomass fuels determination of total sulfur Issued on. 2013-06-01 2012-11-05 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released

Foreword

This standard rule according to GB/T 1.1-2009 given draft. The standard proposed by China Coal Industry Association. This standard coal by the National Standardization Technical Committee (SAC/TC42) centralized. This standard was drafted. CCRI coal analysis laboratory. The main drafters of this standard. leather Zhongyuan, Chen Baohua. Solid biomass fuels determination of total sulfur

1 Scope

This standard specifies the method used Ai Shika and Coulomb titration of solid biomass fuels in total sulfur in the feed method, reagents and materials, instruments Equipment, test procedures, the results of calculation and precision. Arbitration analysis used Ai Shika law. This standard applies to all kinds of solid biomass fuel.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated edition applies to this article Member. For undated references, the latest edition (including any amendments) applies to this document. GB/T 212 Coal Industry Analysis Determination of total sulfur in GB/T 214 coal GB/T 21923 solid biomass fuels General Inspection

3 Ai Shika law

3.1 Method summary The solid biomass fuels in general analysis sample and reagent mixing Ai Shika burning, all sulfur in the sample is converted to soluble sulfate, and then After allowing ions to form sulfuric acid, barium sulfate precipitation, calculate the total sulfur content of solid biomass fuels based on the quality of barium sulfate. 3.2 Reagents and materials Unless otherwise indicated in the analysis using only recognized as analytical reagent or distilled or deionized water or equivalent purity. 3.2.1 Ai Shika agent (hereinafter referred to as aldrin). 2 parts by mass of chemically pure light magnesium oxide (GB/T 9857) and 1 part by mass of Studies pure anhydrous sodium carbonate (GB/T 639) was mixed and finely ground to a particle size less than after 0.2mm, kept in a sealed container. 3.2.2 hydrochloric acid solution. (11), a volume of hydrochloric acid (GB/T 622) adding a volume of water and mix. 3.2.3 barium chloride solution. 100g/L, 10g of barium chloride (GB/T 652) were dissolved in 100mL water. 3.2.4 methyl orange solution. 2g/L, 0.2g of methyl orange was dissolved in 100mL of water. 3.2.5 silver nitrate solution. 10g/L, 1g silver nitrate (GB/T 670) was dissolved in 100mL of water, adding a few drops of nitric acid (GB/T 626), the reservoir In a dark bottle. 3.2.6 porcelain crucible. a capacity of 30mL and 10mL ~ 20mL two kinds. 3.2.7 filter. medium-speed qualitative filter paper and the dense ash quantitative filter paper (GB/T 1914). 3.3 Equipment 3.3.1 Analytical Balance. a sense of the amount of 0.1mg. 3.3.2 muffle furnace. with a temperature control device which can heat up to 900 ℃, adjustable temperature and ventilation. 3.4 Test procedure 3.4.1 in 30mL porcelain crucible weighed general analytical sample (1.00 ± 0.01) g (weighing accuracy of 0.0002g) and Aldrin (3.2.1)
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