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GB/T 19267.6-2008 English PDF

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GB/T 19267.6-2008: Physical and chemical examination of trace evidence in forensic sciences -- Part 6: Scanning electron microscope/X ray energy dispersive spectrometry
Status: Valid

GB/T 19267.6: Historical versions

Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
GB/T 19267.6-2008209 Add to Cart 3 days Physical and chemical examination of trace evidence in forensic sciences -- Part 6: Scanning electron microscope/X ray energy dispersive spectrometry Valid
GB/T 19267.6-2003319 Add to Cart 3 days Physical and chemical examination of trace evidence in forensic sciences -- Part 6: Scanning electron microscopy Obsolete

Similar standards

GB 16796   GA/T 1788.2   GA/T 424   GB/T 19267.13   GB/T 19267.7   GB/T 19267.1   

Basic data

Standard ID: GB/T 19267.6-2008 (GB/T19267.6-2008)
Description (Translated English): Physical and chemical examination of trace evidence in forensic sciences -- Part 6: Scanning electron microscope/X ray energy dispersive spectrometry
Sector / Industry: National Standard (Recommended)
Classification of Chinese Standard: A92
Classification of International Standard: 13.310
Word Count Estimation: 9,933
Date of Issue: 2008-08-14
Date of Implementation: 2009-03-01
Older Standard (superseded by this standard): GB/T 19267.6-2003
Regulation (derived from): Announcement of Newly Approved National Standards No. 14 of 2008 (total 127)
Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary: This standard specifies the scanning electron microscopy and energy dispersive X-ray inspection method is used in combination. This section applies to the field of criminal techniques and chemical examination of trace evidence, other areas may also refer to the use.

GB/T 19267.6-2008: Physical and chemical examination of trace evidence in forensic sciences -- Part 6: Scanning electron microscope/X ray energy dispersive spectrometry


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Physical and chemical examination of trace evidence in forensic sciences Part 6. Scanning electron microscope/X ray energy dispersive spectrometry ICS 13.310 A92 National Standards of People's Republic of China Replacing GB/T 19267.6-2003 Criminal and chemical examination of trace evidence Part 6. SEM/X-ray Spectroscopy Posted 2008-08-14 2009-03-01 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released

Foreword

GB/T 19267 "criminal and chemical examination of trace evidence" is divided into 12 parts. --- Part 1. Infrared absorption spectrometry; --- Part 2. UV - visible absorption spectroscopy; --- Part 3. Molecular Fluorescence Spectroscopy; --- Part 4. atomic emission spectrometry; --- Part 5. Atomic absorption spectrometry; --- Part 6. Scanning electron microscopy/X-ray spectroscopy; --- Part 7. Gas chromatography - mass spectrometry; --- Part 8. microscopic spectrophotometry; --- Part 9. thin layer chromatography; --- Part 10. gas chromatography; --- Part 11. High performance liquid chromatography; --- Part 12. Thermal Analysis. This section GB/T Part of 619,267. This Part replaces GB/T 19267.6-2003 "criminal and chemical examination of trace evidence in Part 6. Scanning Electron Microscopy Mirror method. " This portion of the GB/T 19267.6-2003 compared to the main changes are. --- Standard name a "scanning electron microscopy/X-ray spectroscopy"; --- Increasing the term of the environmental electron microscope (this section 3.2,3.18); --- Increasing the principle part of the environmental electron microscope (this section 4.1); --- Instrument composed of indicators made the necessary changes (this part of GB/T 19267.6-2003 and Chapter 5 of); --- Modify the content of the samples prepared (this section 6.4.1,6.4.2, GB/T 19267.6-2003 of 6.3, 6.4); --- Increased working distance describes the content (in this section 7.2.4); --- Modify the sample analysis of the content (in this section and GB/T 19267.6-2003 7.3). This section presents the People's Republic of China Ministry of Public Security. The criminal section of the National Standardization Technical Committee Physical Testing Standardization Technical Committee (SAC/TC179/SC4) Centralized. This section is drafted. Shanghai Public Security Bureau Evidence Identification Center. The main drafters of this section. Ding Minju, Shao Zhiyuan. This part of the standard replaces the previous editions are. --- GB/T 19267.6-2003. Criminal and chemical examination of trace evidence Part 6. SEM/X-ray Spectroscopy

1 Scope

GB/T 19267 provisions of this part of the scanning electron microscope and X-ray spectrometer combined with the test method. This section applies to the technical field of trace evidence in criminal physical and chemical testing, may also refer to other areas of use.

2 Normative references

The following documents contain provisions which, through reference GB/T 19267 in this section, constitute provisions of this part. For dated reference documents Member, all subsequent amendments (not including errata content) or revisions do not apply to this section, however, encouraged to reach under this section Parties to research agreement to use the latest versions of these documents. For undated reference documents, the latest versions apply to this section. GB/T 13966 Analytical Instruments terms

3 Terms and Definitions

GB/T 13966 and established in the following terms and definitions apply to this section. 3.1 Emitted by the electron gun and by electromagnetic lenses focus the electron beam in the magnetic field scanning coils, the sample surface by a certain time, empty In chronological order as the raster scan (also known as point by point scan), received by the detector samples the secondary electron excitation signal, etc., and then by the photoelectric conversion in significant To reflect the observed sample surface looks like an electronic representation of an upper display. 3.2 ESEM is a new scanning electron microscope developed in recent years. Conventional SEM sample chamber vacuum level must be better than 10-3Pa, non - Conductor and water samples need to be plated conductive layer, and ESEM sample chamber through the gas in low vacuum "environment" status (up pressure To 2600Pa), based on gas ionization and amplification principle, non-conductive and aqueous samples can be treated without the surface conduction can be observed directly. 3.3 Beam bombarding a sample with a substance having a certain energy and intensity, according to the particle energy and intensity of the excited sample substance, or a sample Reflective material particle energy and intensity of the relationship diagram (called spectrum) of the sample to achieve non-destructive elemental analysis, structural analysis and surface material Methods of Analysis. 3.4 (SEM/EDS) Micro-beam electron bombardment of the sample, the sample excitation of micro elements characteristic X-ray detection system displays the characteristics of each element microanalysis X Ray energy and intensity graph (called spectrum) and their distribution in the surface of the specimen.
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