GB/T 14455.7-2008 English PDFUS$229.00 ยท In stock
Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. GB/T 14455.7-2008: Fragrance/Flavor substances -- Determination of ester value after acetylation and evaluation of free alcohols and total alcohols content Status: Valid GB/T 14455.7: Historical versions
Basic dataStandard ID: GB/T 14455.7-2008 (GB/T14455.7-2008)Description (Translated English): Fragrance/Flavor substances -- Determination of ester value after acetylation and evaluation of free alcohols and total alcohols content Sector / Industry: National Standard (Recommended) Classification of Chinese Standard: Y41 Classification of International Standard: 71.100.60 Word Count Estimation: 10,186 Date of Issue: 2008-07-15 Date of Implementation: 2008-11-01 Older Standard (superseded by this standard): GB/T 14455.7-1993; GB/T 14455.8-1993; GB/T 14457.6-1993; GB/T 14457.8-1993 Quoted Standard: GB/T 14454.1; GB/T 14454.14; GB/T 14455.6 Adopted Standard: ISO 1241-1996, MOD; ISO 3794-1976, MOD Regulation (derived from): National Standard Approval Announcement 2008 No.12 (Total No.125) Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China Summary: This standard specifies the method of free alcohol and essential oils and determination of total alcohol content Isolate and synthetic fragrances alcohol content by measuring the presence of sodium acetate, acetic anhydride ester value after acetylation sample to evaluate. This method is not applicable to oils containing more tertiary alcohol (such as linalool and terpineol), tertiary alcohol, tertiary alcohol can be a result of fully acetylated, nor to contain more phenols, lactones, aldehydes ketone enolate easy oils. Because in addition to free alcohol, these components will be acetylated. GB/T 14455.7-2008: Fragrance/Flavor substances -- Determination of ester value after acetylation and evaluation of free alcohols and total alcohols content---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order. Fragrance/Flavor substances. Determination of ester value after acetylation and evaluation of free alcohols and total alcohols content ICS 71.100.60 Y41 National Standards of People's Republic of China Replacing GB/T 14455.7 ~ 14455.8-1993, GB/T 14457.6-1993, GB/T 14457.8-1993 Determination of free alcohols and ester value after acetylation spices and Assess the total alcohol content [ISO 1241.1996, Essentialoils-Determinationofestervalues, beforeandafter acetylation, andevaluationofthecontentsoffreeandtotalalcohols; ISO 3794. 1976, Essentialoils (containingtertiaryalcohols) -Estimationoffree alcoholscontentbydeterminationofestervalueafteracetylation, MOD] Posted 2008-11-01 2008-07-15 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released ForewordGB/T 14455 "spice general test method" consists of the following components. --- Part 1. Oil nomenclature; --- Part 3. spices dissolved in ethanol (mixed) to assess the degree; --- Part 5. Determination of acid value spices or acid content; --- Part 6. Determination of perfume ester value or ester containing an amount; --- Part 7. Determination of ester value assessment and the free alcohol and perfume total alcohol content after acetylation. This section GB/T 14455 Part 7. The partial modification of the use of ISO 1241.1996 "Determination of free alcohols and total alcohol content before and after the oil acetylated ester value assessment" and ISO 3794. 1976 "oils (containing tertiary alcohols) assessment of free alcohol content was measured after acetylation of ester value." This part of ISO 1241.1996 And ISO 3794. 1976 compared to the main technical differences are as follows. --- Remove the ISO 1241.1996 and ISO 3794. 1976 method of sampling; --- Increased the determination of the amount of alcohol and Appendix Isolate and synthetic fragrances containing A. This part is the "assessment ester value after acetylation oil Determination of free alcohols and total alcohol content" of GB/T 14455.7-1993, GB/T 14455.8-1993 "essential oils (containing tertiary alcohols) and free alcohol content was measured after acetylation ester value assessment", GB/T 14457.6- 1993 "Isolate and synthetic flavors, primary or secondary alcohols Determination acetylation method", GB/T 14457.8-1993 "Isolate and synthetic aroma Determination of material content of tertiary alcohols chloroacetyl - dimethyl aniline "consolidation and revision. This part of GB/T 14455.7 ~ 14455.8- 1993, GB/T 14457.6-1993, GB/T 14457.8-1993 compared, mainly to increase the content of the test report. Appendix A of this section is an informative annex. This part is proposed by the China National Light Industry Council. This part of the National Fragrance Flavor and Cosmetic Standardization Technical Committee. This section is responsible for drafting the Shanghai Institute of spices. The main drafters of this section. Dushi Xiang, Xu Yi, Cao Yi, Jinqi Zhang. This part of the standard replaces the previous editions are. --- GB/T 14455.7 ~ 14455.8-1993; --- GB/T 14457.6-1993; --- GB/T 14457.8-1993. Determination of free alcohols and ester value after acetylation spices and Assess the total alcohol content1 ScopeThe first part of the method of the present GB/T 14455 requirements by measuring the presence of sodium acetate, acetylated with acetic anhydride ester samples before and after Value assessment methodology oil free alcohol and determination of the total alcohol content Isolate and synthetic fragrances containing alcohol content. This method does not apply to oils containing more tertiary alcohols (such as linalool and terpineol), tertiary alcohols because tertiary alcohol can not be fully acetylated; nor Contains more suitable phenols, lactones, aldehydes, ketones and easy enolate oils, because in addition to the free alcohol, these components will also be acetylated. GB/T 14455 in the second part of the provisions of this law by measured at N, N- dimethylaniline, with acetyl chloride and acetic anhydride acetic Acylated ester value before and after the samples to assess the essential oil free alcohol content and method of determination Isolate and synthetic fragrances containing alcohol content. This method is applicable to oils contain significant amounts of tertiary alcohols (such as linalool and terpineol), tertiary alcohols, does not apply to contain significant amounts of phenols, anthranilic Benzoic acid esters, lactones, aldehydes, oils and primary alcohols, secondary alcohols.2 Normative referencesThe following documents contain provisions which, through reference GB/T 14455 in this section constitute provisions of this section. For dated reference documents Member, all subsequent amendments (not including errata content) or revisions do not apply to this section. However, under this part are encouraged to reach Parties to research agreement to use the latest versions of these documents. For undated reference documents, the latest versions apply to this section. GB/T 14454.1 perfume sample preparation (GB/T 14454.1-2008, ISO 356.1996, MOD) Preparation of GB/T 14454.14 spices standard solution, the test solution and the indicator solution GB/T 14455.6 perfume ester value or ester containing an amount of determination (GB/T 14455.6-2008, ISO 709.2001, MOD)3 Terms and DefinitionsThe following terms and definitions apply GB/T 14455 in this section. 3.1 Ester 1g and spices contained in the release of acid hydrolysis after the desired number of milligrams of potassium hydroxide. 3.2 The number of milligrams of potassium carbonate and 1g acetylated spices contained in the release of acid hydrolysis desired. The first method acetylation Principle 4 4.1 Determination of ester value according to GB/T 14455.6. 4.2 in the presence of sodium acetate, with acetic anhydride acetylation make perfume. After acetylation isolated and dried spices, according to GB/T 14455.6 Determination of ester value. 4.3 Calculation of free alcohol from the front acetylated ester value after acetylation and, combined with the total alcohol content of alcohol. ......Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of GB/T 14455.7-2008_English be delivered?Answer: Upon your order, we will start to translate GB/T 14455.7-2008_English as soon as possible, and keep you informed of the progress. The lead time is typically 1 ~ 3 working days. The lengthier the document the longer the lead time.Question 2: Can I share the purchased PDF of GB/T 14455.7-2008_English with my colleagues?Answer: Yes. The purchased PDF of GB/T 14455.7-2008_English will be deemed to be sold to your employer/organization who actually pays for it, including your colleagues and your employer's intranet.Question 3: Does the price include tax/VAT?Answer: Yes. 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