Home Cart Quotation About-Us
www.ChineseStandard.net
SEARCH

GB/T 10574.8-2017 English PDF

US$109.00 · In stock
Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email.
GB/T 10574.8-2017: Methods for chemical analysis of tin-lead solders -- Part 8: Determination of zinc content -- Flame atomic absorption spectrometric method
Status: Valid

GB/T 10574.8: Historical versions

Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
GB/T 10574.8-2017109 Add to Cart 3 days Methods for chemical analysis of tin-lead solders -- Part 8: Determination of zinc content -- Flame atomic absorption spectrometric method Valid
GB/T 10574.8-2003239 Add to Cart 3 days Methods for chemical analysis of tin-lead solders -- Determination of zine content Obsolete
GB/T 10574.8-1989199 Add to Cart 2 days Tin-lead solders--Determination of silver content--Flame atomic absorption spectrophotometric method Obsolete

Similar standards

GB/T 10574.11   GB/T 10119   GB/T 8647.8   GB/T 10574.13   GB/T 10574.14   GB/T 10574.12   

Basic data

Standard ID: GB/T 10574.8-2017 (GB/T10574.8-2017)
Description (Translated English): Methods for chemical analysis of tin-lead solders -- Part 8: Determination of zinc content -- Flame atomic absorption spectrometric method
Sector / Industry: National Standard (Recommended)
Classification of Chinese Standard: H13
Classification of International Standard: 77.120.60
Word Count Estimation: 5,532
Date of Issue: 2017-10-14
Date of Implementation: 2018-05-01
Older Standard (superseded by this standard): GB/T 10574.8-2003
Quoted Standard: GB/T 8012
Regulation (derived from): National Standard Announcement 2017 No. 26
Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary: This standard specifies the method for determining the amount of zinc in tin-lead solder. This standard applies to the determination of zinc in tin-lead solder. The measurement range is 0.00025% to 0.0050%. This standard is an arbitration analysis method.

GB/T 10574.8-2017: Methods for chemical analysis of tin-lead solders -- Part 8: Determination of zinc content -- Flame atomic absorption spectrometric method


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Methods for chemical analysis of tin-lead solders.Part 8. Determination of zinc content.Flame atomic absorption spectrometric method ICS 77.120.60 H13 National Standards of People's Republic of China Replacing GB/T 10574.8-2003 Tin-lead solder chemical analysis method Part 8. Determination of zinc content Flame Atomic Absorption Spectrometry Part 8. Determinationofzinccontent- Published on October 10,.2017 2018-05-01 Implementation General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China China National Standardization Administration released

Foreword

GB/T 10574 "Chemical analysis method for tin-lead solders" is divided into 14 parts. --- Part 1. Determination of tin content Potassium iodate titration; --- Part 2. Determination of barium content - Malachite green spectrophotometric method and potassium bromate titration method; --- Part 3. Determination of helium content by flame atomic absorption spectrometry; --- Part 4. Determination of iron content 1,10-Phenanthroline spectrophotometric method; Part 5 . Determination of arsenic content ; Arsenic molybdenum blue spectrophotometric method ; --- Part 6 . Determination of copper content Flame atomic absorption spectrometry ; --- Part 7. Determination of silver content Flame atomic absorption spectrometry and potassium thiocyanate potentiometric titration; --- Part 8. Determination of zinc content Flame atomic absorption spectrometric method; --- Part 9 . Determination of aluminium content by electrothermal atomic absorption spectrometry ; Part 10 . Determination of cadmium content Flame atomic absorption spectrometry and Na2EDTA titration ; Part 11 . Determination of phosphorus content Crystal violet - phosphorus vanadium molybdenum heteropolyacid spectrophotometric method ; --- Part 12. Determination of sulfur content - High-frequency combustion infrared absorption spectrometry; ---Part 13. Determination of the amounts of ruthenium, rhodium, iron, arsenic, copper, silver, zinc, aluminum, cadmium, phosphorus, and gold Inductively coupled plasma atomic emission Spectral method; ---Part 14. Determination of tin, lead, antimony, bismuth, silver, copper, zinc, cadmium, and arsenic - Photoelectric emission spectroscopy. This part is part 8 of GB/T 10574. This section was drafted in accordance with the rules given in GB/T 1.1-2009. This part is an amendment to GB/T 10574.8-2003 "Determination of zinc in chemical analysis methods for tin-lead solders." Compared with GB/T 10574.8-2003, the main technical changes are as follows. --- Increased reference standards; --- The lower limit of measurement was revised from 0.00003% to 0.00025%; --- Zinc standard storage solution and zinc standard solution modified to hydrobromic acid - hydrochloric acid medium, and increase the acidity; --- Removed the allowable error, increased repeatability and reproducibility content. This part is under the jurisdiction of the National Non-ferrous Metals Standardization Technical Committee (SAC/TC243). This section is responsible for drafting. Yunnan Tin Industry Co., Ltd. Participated in the drafting of this section. Yunnan Tin Industry Co., Ltd., Lianyungang Exit Inspection and Quarantine Bureau, Beijing Mining and Metallurgy Research Institute, Kunming Metallurgical Research Institute, China Nonferrous Metals Guilin Institute of Mineral Geology Co., Ltd., National Copper Lead and Zinc Quality Inspection Center. The main drafters of this section. Yang Zihua, Xia Xinyuan, Tan Feng, Shen Cui, Fan Lixin, Zhou Dian, Yang Haojin, Jin Xiaofeng, Li Min, Liu Yingbo, Li Rong and Sun Guojuan. The previous versions of the standards replaced in this section were. ---GB/T 10574.10-1989; --- GB/T 10574.8-2003. Tin-lead solder chemical analysis method Part 8. Determination of zinc content Flame Atomic Absorption Spectrometry

1 Scope

This part of GB/T 10574 specifies the method for the determination of zinc in tin-lead solders. This section applies to the determination of zinc in tin-lead solder. The measurement range is 0.00025% to 0.0050%. This section is an arbitration analysis method.

2 Normative references

The following documents are indispensable for the application of this document. For dated references, only dated versions apply to this article Pieces. For undated references, the latest version (including all amendments) applies to this document. GB/T 8012 cast tin-lead solder

3 Method summary

The sample was dissolved with hydrobromic acid, hydrochloric acid, and hydrogen peroxide. The hydrochloric acid-hydrobromic acid volatilized to remove tin and bismuth. In a dilute hydrochloric acid-hydrobromic acid medium, The absorbance of zinc was measured with an air-acetylene flame at an atomic absorption spectrometer wavelength of 213.9 nm.

4 Reagents

Unless otherwise stated, only reagents identified as superior grade and first grade water were used in the analysis. 4.1 Hydrobromic acid (ρ=1.48 g/mL). 4.2 Hydrochloric acid (ρ=1.19 g/mL). 4.3 Hydrochloric acid (5 95). 4.4 Hydrogen peroxide (1 2), analytically pure. 4.5 Zinc standard storage solution. Weigh 0.1250g of metal zinc (wZn≥99.99%) into a.200mL PTFE beaker. 8.0mL of hydrobromic acid (4.1), 12.0mL of hydrochloric acid (4.2), heated to complete dissolution at low temperature, cooled to room temperature, transferred to a 500mL volumetric flask, Dilute with water to the mark and mix. 1mL of this solution contains 250μg of zinc. 4.6 zinc standard solution. Pipette 5.00mL zinc standard stock solution (4.5) in 500mL volumetric flask, add 2.0mL hydrobromic acid (4.1), 4.0 mL of hydrochloric acid (4.2), dilute with water to the mark and mix. 1mL of this solution contains 2.5μg of zinc.

5 Instruments

Atomic absorption spectrometer with zinc hollow cathode lamp. Under the best working conditions of the instrument, anyone who can achieve the following indicators can be used. Sensitivity. The characteristic concentration of zinc should not be greater than 0.008 μg/mL.
......
Image     

Tips & Frequently Asked Questions:

Question 1: How long will the true-PDF of GB/T 10574.8-2017_English be delivered?

Answer: Upon your order, we will start to translate GB/T 10574.8-2017_English as soon as possible, and keep you informed of the progress. The lead time is typically 1 ~ 3 working days. The lengthier the document the longer the lead time.

Question 2: Can I share the purchased PDF of GB/T 10574.8-2017_English with my colleagues?

Answer: Yes. The purchased PDF of GB/T 10574.8-2017_English will be deemed to be sold to your employer/organization who actually pays for it, including your colleagues and your employer's intranet.

Question 3: Does the price include tax/VAT?

Answer: Yes. Our tax invoice, downloaded/delivered in 9 seconds, includes all tax/VAT and complies with 100+ countries' tax regulations (tax exempted in 100+ countries) -- See Avoidance of Double Taxation Agreements (DTAs): List of DTAs signed between Singapore and 100+ countries

Question 4: Do you accept my currency other than USD?

Answer: Yes. If you need your currency to be printed on the invoice, please write an email to Sales@ChineseStandard.net. In 2 working-hours, we will create a special link for you to pay in any currencies. Otherwise, follow the normal steps: Add to Cart -- Checkout -- Select your currency to pay.

Question 5: Should I purchase the latest version GB/T 10574.8-2017?

Answer: Yes. Unless special scenarios such as technical constraints or academic study, you should always prioritize to purchase the latest version GB/T 10574.8-2017 even if the enforcement date is in future. Complying with the latest version means that, by default, it also complies with all the earlier versions, technically.