GB/T 10513-2012 English PDFUS$149.00 · In stock
Delivery: <= 2 days. True-PDF full-copy in English will be manually translated and delivered via email. GB/T 10513-2012: Determination of free water for nitrophosphate -- Karl fischer method Status: Valid GB/T 10513: Historical versions
Basic dataStandard ID: GB/T 10513-2012 (GB/T10513-2012)Description (Translated English): Determination of free water for nitrophosphate -- Karl fischer method Sector / Industry: National Standard (Recommended) Classification of Chinese Standard: G20 Classification of International Standard: 65.080 Word Count Estimation: 5,591 Older Standard (superseded by this standard): GB/T 10513-1989 Quoted Standard: GB/T 6283; GB/T 10511-2008; HG/T 2843 Regulation (derived from): National Standards Bulletin 2012 No. 42 Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China Summary: This standard specifies the central air conditioning system energy saving control unit (hereinafter referred to as energy-saving control device) the technical requirements of the basic functions, test specifications and signs, packaging, transportation, s GB/T 10513-2012: Determination of free water for nitrophosphate -- Karl fischer method---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.ICS65.080 G20 National Standards of People's Republic of China Replacing GB/T 10513-1989 Nitrophosphate determination of free water content Karl Fischer Issued on. 2013-06-01 2012-12-31 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released ForewordThis standard rule according to GB/T 1.1-2009 given draft. This standard is one nitrate fertilizer, P and K series of standard test methods for nitrate, which are listed below national standards. --- GB/T 10511-2008 "After distillation of total nitrogen content for nitrophosphate titration method"; --- GB/T 10512-2008 "nitrate fertilizer phosphorus content - Quinoline phosphomolybdate gravimetric method"; --- GB/T 10514-2012 "nitrophosphate determination of water content - Oven method"; --- GB/T 10515-2012 "Determination of particle size Nitrophosphates"; --- GB/T 10516-2012 "nitrate fertilizer particles have an average crush strength of determination." This standard replaces GB/T 10513-1989 "nitrophosphate determination of water content Karl Fischer method." The main difference between this version and the previous version are. --- Reagent solution, such as a standard titration solution preparation and calibration methods are the implementation of HG/T2843 standard; --- Volume to absorb the test solution by 10.0mL 5.0mL; --- Increased content security warning. The standard proposed by China Petroleum and Chemical Industry Association. This standard by the National Standardization Technical Committee fertilizer and soil conditioner. This standard was drafted. Tianji Coal Chemical Industry Group Co., Ltd., National Fertilizer Quality Supervision and Inspection Center (Shanghai). The main drafters. Zhang Jiahong, Wang Yin, Li Yongping, Guo Lian Hong, Yang. This standard was first published in 1989. Nitrophosphate determination of free water content Karl Fischer1 ScopeThis standard specifies the determination of P and K fertilizer nitrate, the free water content by the Karl Fischer method. This standard applies to all kinds of technology, the nitrate fertilizer, measuring water content of phosphorus and potassium nitrate free.2 Normative referencesThe following documents for the application of this document is essential. For dated references, only the dated edition applies to this File. For undated references, the latest edition (including any amendments) applies to this document. GB/T 6283 Determination of chemical products, water content Karl Fischer method (General method) (GB/T 6283-2008, ISO 760. 1978, NEQ) GB/T 10511-2008 After distillation of total nitrogen content for nitrophosphate titration HG/T2843 fertilizer products commonly used standard titration solution, standard solution, reagent solution and indicator solution Chemical Analysis Principle 3 Free water sample with a known water titer of Karl Fischer reagent for quantitative reaction, reaction is as follows. H2O I2 SO2 3C5H5N = 2C5H5N · HI C5H5N · SO3 C5H5N · SO3 CH3OH = C5H5NH · OSO2OCH34 ReagentsReagents and solutions following the flammable and toxic and harmful to the human body, the operator should be careful! If splashed on the skin should be washed with water immediately Wash, if not meet the doctor immediately. This standard reagent solution and water, in the specifications and method of preparation is not specified, it shall comply with the provisions of HG/T2843's. 4.1 methanol. water content ≤0.05%, water content > 0.05%, 500mL of methanol was added to the 5A molecular sieve about 50g, stuffed with cork, To stand overnight, to learn to use the supernatant; 4.2 dioxane. dehydration treatment method with 4.1; 4.3 ethanol. dehydration treatment method with 4.1; 4.4 Karl Fischer reagent; NOTE. None of pyridine Karl Fischer reagent can also be used to improve, but at the time of arbitration, only the pyridine-containing reagents. 4.5 5A zeolite. 3mm ~ 5mm in diameter particles, is used as the desiccant before use calcined at 500 ℃ 2h and fresh interior points. Molecular sieve dryer cooled molecular sieve can be used with water washing, drying, calcination regeneration reserve.5 Instruments5.1 usually laboratory instruments; ......Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of GB/T 10513-2012_English be delivered?Answer: Upon your order, we will start to translate GB/T 10513-2012_English as soon as possible, and keep you informed of the progress. The lead time is typically 1 ~ 2 working days. The lengthier the document the longer the lead time.Question 2: Can I share the purchased PDF of GB/T 10513-2012_English with my colleagues?Answer: Yes. 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Unless special scenarios such as technical constraints or academic study, you should always prioritize to purchase the latest version GB/T 10513-2012 even if the enforcement date is in future. Complying with the latest version means that, by default, it also complies with all the earlier versions, technically. |