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YS/T 3005-2011 PDF English

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YS/T 3005-2011: Methods for sampling and sample preparation of flotation gold concentrates
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GB/T 3190   GB/T 8005.1   YS/T 3004   

YS/T 3005-2011: Methods for sampling and sample preparation of flotation gold concentrates

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GOLD INDUSTRY STANDARD OF THE PEOPLE’S REPUBLIC OF CHINA ICS 73.060.99 H 60 Methods for sampling and sample preparation of flotation gold concentrates Issued on. DECEMBER 20, 2011 Implemented on. JULY 01, 2012 Issued by. Ministry of Industry and Information Technology of PRC

Table of Contents

Foreword... 3 1 Scope... 4 2 Normative references... 4 3 Terms and definitions... 4 4 Basic requirements... 5 5 Sampling... 7 6 Sample preparation... 11 7 Storage of chemical composition specimen and identification of specimen 15 Appendix A (Normative) Method for determination of moisture of gold concentrates... 16 Appendix B (Normative) Gold concentrate - Test method for assessment of quality fluctuation... 19 Appendix C (Normative) Gold concentrate - Test method for calibrating sampling precision... 23

Foreword

YS/T 3005-2011 “Methods for sampling and sample preparation of flotation gold concentrates” was drafted in accordance with the rules given in GB/T 1.1-2009. Appendix A, Appendix B, Appendix C of this standard are normative appendixes. This standard was proposed by the China Gold Association. This standard shall be under the jurisdiction of the National Gold Standardization Technical Committee (SAC/TC 379). Responsible drafting organization of this standard. Changchun Gold Research Institute. Participated drafting organizations of this standard. Henan Zhongyuan Gold Smelter Co., Ltd., Zijin Mining Group Co., Ltd., Lingbao Gold Co., Ltd., Liaoning Tianli Gold Industry Co., Ltd., Zhaojin Mining Co., Ltd. Jinchiling Gold Mine, Shandong Hengbang Smelting Co., Ltd., Shandong Gold Group Co., Ltd. Drafters of this standard. Huang Rui, Xue Lixian, Ren Wensheng, Zou Laichang, Zhi Zifan, Liao Zhanpi, Liu Pengfei, Peng Guomin, Li Xueqiang, Han Xiaoguang, Zhu Yansheng, Pan Yuxi, Lan Meixiu, Dong Erxian, Liu Wenbo, Liao Zhongyi, Xu Zhongmin, Bi Hongtao. Methods for sampling and sample preparation of flotation gold concentrates

1 Scope

This standard specifies the methods for sampling and sample preparation of flotation gold concentrate, methods for determination of moisture, test methods for the quality fluctuation of gold concentrate assessment, test methods for the precision of calibration sampling. This standard is applicable to the sampling and preparation of samples for the chemical composition and moisture of bulk and bagged flotation gold concentrates as well as the determination of moisture.

2 Normative references

The following documents are essential to the application of this document. For the dated documents, only the versions with the dates indicated are applicable to this document; for the undated documents, only the latest version (including all the amendments) are applicable to this standard. GB/T 7739 Methods for chemical analysis of gold concentrates YS/T 3004 Gold concentrate

3 Terms and definitions

The following terms and definitions apply to this document. 3.1 Lot A lot of gold concentrates to be sampled for testing of quality characteristics. The mass of the gold concentrate that constitutes a lot is the lot mass. 3.2 Sub-lot If a lot is divided into several parts, each part is a sub-lot. The mass of the gold concentrate that constitutes a sub-lot is the sub-lot mass. 3.3 Increment A sample as taken from a lot or a sub-lot at a time by a sampling device. The mass of each increment is the increment mass. 3.4 Lot sample The sample which is mixed by the increment as taken from the lot and represents the lot. 3.5 Subsample The sample which is mixed by the increment as taken from the sub-lot and represents the sub-lot.

4 Basic requirements

4.1 The standard deviation (σw) of the mass fraction between the increments in a lot indicates the quality fluctuation of the gold concentrate. The quality fluctuations of gold concentrates are divided into three categories. high, medium, low (see Table 1). 4.3 If the quality fluctuation of the gold concentrate of the lot is σw ≥ 5.0 or otherwise it is mixed by foreign inclusions, it is negotiated between the supplier and the purchaser or otherwise no sample is taken. 4.4 The total precision for sampling of gold concentrate of a lot is 2% of the gold’s mass fraction. 4.5 For the first sampling of gold concentrate and the change of sampling and sample preparation method, it shall follow the requirements of Appendix C to carry out precision test of calibration sampling. 4.6 The sampling and sample preparation plan of gold concentrate shall be confirmed by the relevant parties. 4.7 Gold concentrates that do not meet the requirements of YS/T 3004 shall not be sampled or be negotiated between the supplier and the purchaser. 4.12 The operation of sampling and sample preparation shall comply with the relevant safety specifications.

5 Sampling

5.1 Sampling tools 5.1.1 Sampling brazing bar (see Figure 1), the specification size of which shall meet the requirements for the amount of sample taken. 5.2 Sampling procedure 5.2.1 Weigh the mass of the delivered gold concentrate. If the gold concentrate is mixed with rain or snow water or visible water, it shall be dewatered before weighing. 5.2.2 Develop a sampling plan, which shall include the following. 5.2.3 Check the sampling facility equipment and appliances. 5.2.4 According to the sampling plan, take sample and make record. Place the increment taken into a container with lid or plastic sample bag. 5.3 Increment mass The mass of the increment taken shall be not less than 300 g. The coefficient of mass variation (CV) shall be not more than 20%. 5.4 Combination of increments 5.5 Sampling method 5.5.1 Systematic sampling 5.5.1.1 In the course of movement of bulk gold concentrates during handling or weighing, take increment based on certain mass interval or time interval. 5.5.1.5 It shall select the sampling device of appropriate size to collect the full- width, full-thickness gold concentrate stream. 5.5.2 Truck sampling 5.5.2.1 From the motor vehicles, trains, bins which are loaded with gold concentrates, take the increment. 5.5.2.2 The material surface of the gold concentrate shall be flat. Based on the number of increments as specified in Table 1, calculate the uniform distribution points. 5.5.3 Sampling from stockyard 5.5.3.1 Unload a lot of gold concentrate in a stockyard that is spacious, clean, level, free from external contamination. 5.5.3.2 After mechanically or manually mix it evenly, flatten the pile to make its height be less than 1 m. 5.5.4 Sampling from bags 5.5.4.1 When handling the bagged gold concentrate, take the increment. Use the brazing bar to perpendicularly penetrate the packaging bag. 5.5.4.2 When the type of quality fluctuation is unknown, take at least one increment per bag.

6 Sample preparation

6.1 Sample preparation equipment and tools 6.1.1 Grinder or rod mill. 6.1.2 Constant-temperature drying oven. 6.1.3 Non-absorbent division plates, stainless-steel cross-split plates, baffles, rubber. 6.1.8 Sample container and component sample bag. 6.2 Sample preparation requirements 6.2.1 Sample preparation includes a series of operations such as mixing, drying, grinding, division. It shall prevent contamination and chemical composition changes of the sample. 6.3 Sample preparation procedure 6.3.1 Weigh and check the mass of the lot sample and subsample. 6.3.2 Establish the sample preparation plane, which shall include the following. 6.3.3 Check the cleaning facilities and equipment. 6.3.4 According to the plan, prepare specimen and make record. 6.4 Mixing method 6.4.1 Rolling method Place the sample on a clean sample-mixing rubber. Lift the opposite corners of the rubber to perform up-and-down movement, to allow the sample to roll over the centerline of the rubber. Use the same method to repeat operations for the other pair of opposite corners for at least 5 times, to mix the sample uniformly. 6.5 Division method 6.5.1 Quadruple Flatten the top of cone. Use the cross-split plate to divide the sample into four equal portions from top down. Discard half of the diagonal sample. Retain the other half of sample. Use the pile cone method to mix the retained sample uniformly. Repeat the above operation, to divide it to the required amount.

7 Storage of chemical composition specimen and identification of specimen

7.1 The shelf life of chemical composition specimen is three months. 7.2 The sample bag shall be clearly marked of the following. ......
Source: Above contents are excerpted from the full-copy PDF -- translated/reviewed by: www.ChineseStandard.net / Wayne Zheng et al.


      

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