YS/T 1075.7-2015 (YS/T1075.7-2015, YST 1075.7-2015, YST1075.7-2015) & related versions
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Methods for chemical analysis of vanadium-aluminium and molybdenum-aluminium master alloys. Part 7: Determination of oxygen content. Inert gas fusion-infrared method
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YS/T 1075.7-2015
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YST 1075.7-2015
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YS/T 1075.7-2015: PDF in English (YST 1075.7-2015)
YS/T 1075.7-2015
(Vanadium aluminum, molybdenum intermediate aluminum alloys - Part 7. Determination of oxygen inert gas fusion - infrared method)
ICS 77.120.99
H14
People's Republic of China Nonferrous Metals Industry Standard
Aluminum vanadium, molybdenum intermediate aluminum alloys -
Determination of the amount of oxygen. Part 7
Inert gas fusion - infrared method
Part 7. Determinationofoxygencontent-
Issued on. 2015-04-30
2015-10-01 implementation
Ministry of Industry and Information Technology of the People's Republic of China released
Foreword
YS/T 1075 "aluminum vanadium, molybdenum intermediate aluminum alloy chemical analysis method" including a total of 8 sections.
--- Part 1. Determination of iron content - 1,10-phenanthroline spectrophotometry;
--- Part 2. Determination of molybdenum content of lead molybdate gravimetric method;
--- Part 3. Determination of silicon content - Molybdenum blue spectrophotometric method;
--- Part 4. vanadium content - Inductively coupled plasma atomic emission spectrometry and ferrous ammonium sulfate titration;
--- Part 5. Determination of aluminum content EDTA titration;
--- Part 6. Determination of carbon content in the high-frequency combustion - infrared absorption method;
--- Part 7. Determination of the amount of oxygen in the inert gas fusion - infrared method;
--- Part 8. molybdenum, aluminum X- determining the amount of fluorescence spectroscopy.
This section YS/T 1075 Part 7.
This section drafted in accordance with GB/T 1.1-2009 given rules.
The non-ferrous metal part by the National Standardization Technical Committee (SAC/TC243) and focal points.
This section is drafted. big Chengde Vanadium Industry Co., Ltd., Northwest Nonferrous Metal Research Institute, Shangluo Amano Advanced Materials Co., Ltd.
Western Metal Materials Co., Ltd., Institute of Powder Metallurgy, Central South University, East Donggang hi-Metal Materials Co., Guangzhou colored
Metal Research Institute.
The main drafters of this section. Li Jianxin, Liu Jianfeng, Wang Kuan, Lin Xuemei, Liang Qinghua, Zhou Yonggui, Liu Yan, Zhao Fei, Liu Jianbin, Zheng Lingzhi,
Dong Feng Wen, Zhuang Yichun, Zou Deling.
Aluminum vanadium, molybdenum intermediate aluminum alloys -
Determination of the amount of oxygen. Part 7
Inert gas fusion - infrared method
1 Scope
YS/T 1075 This section provides the vanadium aluminum, aluminum master alloys determination of molybdenum in the amount of oxygen.
This section applies to vanadium aluminum, aluminum master alloys determination of molybdenum in the amount of oxygen. Measurement range. 0.010% to 0.30%.
2 Method summary
In an inert atmosphere, is heated to a molten sample pulses, i.e. pulses containing sample melted in the furnace graphite crucible. Samples of different forms
Oxygen at high temperatures to generate a large number of small amounts of CO and CO2 with the graphite crucible, which along with the heat carrier gas flow rare earth copper oxide, so that
Conversion of CO to CO2. Then, the mixed gas stream into the cell infrared detector, the oxygen content of the sample was measured.
3 Reagents
3.1 Carrier gas. argon or helium (volume fraction ≥99.99%).
3.2 Power gas. oil-free compressed air.
3.3 Nickel bag (thickness ≤0.05mm, wO≤0.001%).
3.4 sets graphite crucible.
3.5 standard sample.
4 Instrument
The inert gas fusion - thermal conductivity/IR detection system (including one electrode furnace, purification and analysis of a carrier gas stream conversion systems, carbon monoxide red
External infrared detectors and carbon dioxide detectors, computers and software control system).
Recommended Instruments working conditions are as follows.
Minimum analysis time. 40s; exhaust Power. 6000W; analysis of power. 5000W.
5 Sample
The specimen shall crush a particle size less than 500μm. If oil is required with an organic reagent acetone, dry before testing.
Step 6 Analysis
6.1 Sample
Weigh 0.040g ~ 0.070g sample (Chapter 5), accurate to 0.0001g.
......
| Standard ID | YS/T 1075.7-2015 (YS/T1075.7-2015) | | Description (Translated English) | Methods for chemical analysis of vanadium-aluminium and molybdenum-aluminium master alloys. Part 7: Determination of oxygen content. Inert gas fusion-infrared method | | Sector / Industry | Nonferrous Metallurgy Industry Standard (Recommended) | | Classification of Chinese Standard | H14 | | Classification of International Standard | 77.120.99 | | Word Count Estimation | 5,598 | | Date of Issue | 2015-04-30 | | Date of Implementation | 2015-10-01 | | Drafting Organization | Chengde Vanadium big industry limited liability company; Northwest Nonferrous Metal Research Institute; Advanced Materials Co., Ltd. Shangluo Amano; Western Metal Materials Co., Ltd; Powder Metallurgy Research Institute, Central South University; Donggang East high-tech Materials Co., Ltd. Metal; Guangzhou Research Institute of Nonferrous Metals | | Administrative Organization | National Standardization Technical Committee for Nonferrous Metals | | Regulation (derived from) | Ministry of Industry and Information Technology Announcement (2015 No. 28) | | Proposing organization | National Non-Ferrous Metals Standardization Technical Committee (SAC/TC 243) | | Issuing agency(ies) | Ministry of Industry and Information Technology of the People's Republic of China | | Summary | This Standard specifies the vanadium aluminum, aluminum master alloys determination of molybdenum in the amount of oxygen. This Standard applies to aluminum vanadium, molybdenum determination of aluminum alloy with oxygen. Measurement range: 0.010% to 0.30%. |
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