YS/T 1050.5-2015 (YS/T1050.5-2015, YST 1050.5-2015, YST1050.5-2015) & related versions
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Methods for chemical analysis of lead antimony concentrates. Part 5: Determination of sulfur content. Gravimetric method
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YS/T 1050.5-2015
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YST 1050.5-2015
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YS/T 1050.5-2015: PDF in English (YST 1050.5-2015)
YS/T 1050.5-2015
(Methods for chemical analysis of lead-antimony concentrates - Part 5. sulfur content - Gravimetric method)
ICS 73.060
D42
People's Republic of China Nonferrous Metals Industry Standard
Methods for chemical analysis of lead-antimony concentrate
Part 5. sulfur content - Gravimetric method
Part 5. Determinationofsulfurcontent-
Issued on. 2015-04-30
2015-10-01 implementation
Ministry of Industry and Information Technology of the People's Republic of China released
Foreword
YS/T 1050-2015 "Methods for chemical analysis of lead-antimony concentrate" is divided into the following nine sections.
--- Part 1. Determination of lead content Na2EDTA titration;
--- Part 2. Determination of antimony content cerium sulfate titration;
--- Part 3. Determination of arsenic content potassium bromate titration;
--- Part 4. Determination of zinc contents Na2EDTA titration;
--- Part 5. Determination of sulfur content - Gravimetric method;
--- Part 6. Determination of iron content cerium sulfate titration;
--- Part 7. Determination of the amount of bismuth and copper - Flame atomic absorption spectrometry amount;
--- Part 8. gold and silver content determination fire assay;
--- Part 9. Determination of the amount of silver by flame atomic absorption spectrometry.
This is Part 5.
This section drafted in accordance with GB/T 1.1-2009 given rules.
The non-ferrous metal part by the National Standardization Technical Committee (SAC/TC243) centralized.
This section is responsible for drafting unit. Guangxi Metallurgical Product Quality Supervision and Inspection Station.
This section drafted by. China Certification & Inspection Group Co., Ltd. Guangxi.
Participated in the drafting of this section. Nantong CIQ Comprehensive Technology Center, Beijing Research Institute of Mining and Metallurgy, Guangxi Zhuang Autonomous Region
Analysis and Testing Research Center.
The main drafters of this section. Zheng Xiangming, Weiya Juan, Douhuai Zhi, Huangzhao Min, Fu Li, Ma Li, Wei Gang, Huang Xusheng, Jiang Jing, Hou Jin, Yu Ye Boschniakia glabra,
Juan.
Methods for chemical analysis of lead-antimony concentrate
Part 5. sulfur content - Gravimetric method
1 Scope
This section YS/T 1050 specifies the method for determination of lead-antimony concentrate sulfur content.
This section applies to the determination of lead in antimony concentrate sulfur content measurement range (mass fraction) 15.00% - 30.00%.
2 Method summary
Sample at 750 ℃ by sodium carbonate - zinc oxide mixture after sintering, dissolved in water solubles, and precipitated barium sulfate solution.
The precipitate was filtered, burning, weighed, calculated according to the quality of barium sulfate sulfur content of the sample.
3 Reagents
Unless otherwise indicated, this part of the reagents were analytical reagent, the water for the two water.
3.1 zinc oxide.
3.2 anhydrous sodium carbonate.
3.3 hydrochloric acid (ρ = 1.19g/mL).
3.4 nitric acid (ρ = 1.42g/mL).
3.5 hydrochloride (11).
3.6 barium chloride solution (100g/L).
3.7 silver nitrate solution (10g/L). Per 100mL was added dropwise 3 to 4 drops of nitric acid (3.4).
3.8 sintering agent. anhydrous sodium carbonate (3.2) and zinc oxide (3.1) drying at 105 ℃ ± 5 ℃ 2h after mixing with 1 to 1 ratio, fine,
Mix well.
3.9 methyl orange indicator (1g/L).
4 Sample
4.1 Sample size should be less than 0.074mm.
4.2 specimen should be 100 ℃ ~ 105 ℃ drying 1h, placed in a desiccator to cool to room temperature.
Step 5 Analysis
5.1 Sample
Weigh 0.20g sample, accurate to 0.0001g.
5.2 Determination of the number of
Independently measured twice and averaged.
......
| Standard ID | YS/T 1050.5-2015 (YS/T1050.5-2015) | | Description (Translated English) | Methods for chemical analysis of lead antimony concentrates. Part 5: Determination of sulfur content. Gravimetric method | | Sector / Industry | Nonferrous Metallurgy Industry Standard (Recommended) | | Classification of Chinese Standard | D42 | | Classification of International Standard | 73.06 | | Word Count Estimation | 5,523 | | Date of Issue | 2015-04-30 | | Date of Implementation | 2015-10-01 | | Drafting Organization | Metallurgical Products Quality Supervision and Inspection Station of Guangxi Zhuang Autonomous Region | | Administrative Organization | National Standardization Technical Committee for Nonferrous Metals | | Regulation (derived from) | Ministry of Industry and Information Technology Announcement (2015 No. 28) | | Issuing agency(ies) | Ministry of Industry and Information Technology of the People's Republic of China | | Summary | This Standard specifies the method for determination of lead-antimony concentrate sulfur content. This Standard applies to the determination of lead-antimony concentrate sulfur content measurement range (mass fraction) was 15.00% ~ 30.00%. |
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