GB/T 20082-2006 (GB/T20082-2006, GBT 20082-2006, GBT20082-2006) & related versions
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Hydraulic fluid power -- Fluid contamination -- Determination of particulate contamination by the counting method using an optical microscope
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GB/T 20082-2006
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GBT 20082-2006
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GB/T 20082-2006: PDF in English (GBT 20082-2006)
GB/T 20082-2006
NATIONAL STANDARD OF THE
PEOPLE’S REPUBLIC OF CHINA
ICS 23.100.60
J 20
GB/T 20082-2006 / ISO 4407:2002
Hydraulic fluid power - Fluid contamination -
Determination of particulate contamination by the
counting method using an optical microscope
(ISO 4407:2002, IDT)
ISSUED ON: JANUARY 23, 2006
IMPLEMENTED ON: AUGUST 01, 2006
Issued by: General Administration of Quality Supervision, Inspection and
Quarantine of the PRC;
Standardization Administration of the PRC.
Table of Contents
Foreword ... 3
Introduction ... 4
1 Scope ... 5
2 Normative references ... 5
3 Terms and definitions ... 6
4 Counting principle ... 8
5 Apparatus ... 9
6 Reagents and chemicals ... 12
7 Glassware cleaning procedure ... 12
8 Calibration procedures ... 13
9 Membrane filter preparation ... 14
10 Particle sizing and counting procedure ... 18
11 Expression of results ... 21
12 Identification statement (Reference to this Standard) ... 21
Foreword
This Standard is identical to the international standard ISO 4407:2002
“Hydraulic fluid power - Fluid contamination - Determination of particulate
contamination by the counting method using an optical microscope” (English
edition).
For ease of use, this Standard makes the following modifications to ISO
4407:2002:
- ADD a view to Figure 1 and re-arrange the key;
- CHANGE Figure 3 to Table 2 and the “Note” of Figure 3 to the table note of
Table 2;
- For reference standards, replace international standards with
corresponding national standards.
This Standard was proposed by China Machinery Industry Federation.
This Standard shall be under the jurisdiction of National Technical Committee 3
on Hydraulic Pneumatics of Standardization Administration of China (SAC/TC
3).
Drafting organization of this Standard: China Aviation Industry Granularity
Measurement and Test Station.
Main drafters of this Standard: Lu Hong, Zhang Sufang, Guo Guixia, Wang Yan.
This Standard is first issued.
Hydraulic fluid power - Fluid contamination -
Determination of particulate contamination by the
counting method using an optical microscope
WARNING: The use of this Standard may involve hazardous materials,
operations and equipment. This Standard does not purport to address all
the safety problems associated with its use. It is the responsibility of the
user of this Standard to establish appropriate safety and health practices
and determine the applicability of regulative limitations prior to use.
1 Scope
This Standard specifies methods for determining the level of particulate
contamination in liquids used in hydraulic systems by counting the number of
particles deposited on the surface of a membrane filter using an optical
microscope. It includes particle counting by two manual methods and image
analysis, using either transmitted or incident lighting systems.
Particle sizes ≥ 2 μm can be sized and counted by this method, but the
resolution and accuracy of the results will depend upon the optical system used
and the capabilities of the operator.
All hydraulic fluids with a wide range of contamination levels can be analysed
according to this Standard. However, the counting uncertainty at the larger
particle sizes increases if the volume filtered is reduced to allow smaller sized
particles to be counted, where a fine precipitate or a high particle concentration
is present.
2 Normative references
The following documents contain provisions which, through reference in this
Standard, constitute provisions of this Standard. For the dated references, their
subsequent amendments (excluding corrections) or revisions do not apply to
this Standard. However, the parties who enter into agreement based on this
Standard are encouraged to investigate whether the latest editions of these
documents are applicable. For undated reference documents, the latest
editions apply to this Standard.
GB/T 12804 Laboratory glassware - Graduated measuring cylinders (GB/T
12804-1991, eqv ISO 4788:1980)
8.2.4 Unclamp, carefully remove the membrane filter from the base and
measure the diameter [effective filtration diameter (EFD)] of the stain in at least
two planes to within 0.1 mm. Average the at least two measurement results and
calculate the effective filtration area (EFA). Mark the funnel with a suitable code
and record the result in a suitable calibration recording system.
9 Membrane filter preparation
9.1 Sample preparation
9.1.1 After noting all sample identification details, remove any tied-up or loosely
attached labels ensuring that sample identity is retained. Thoroughly clean the
outside of the sample bottle, particularly around the cap, by washing with
filtered solvent.
9.1.2 If the sample has been standing for a period of time, particle settlement,
and hence agglomeration, will occur. It is essential that the agglomerates are
broken up, and the contaminant particles are re-dispersed evenly within the
contents of the sample before analysis.
9.1.3 Redistribute the contaminants within the contents of the bottle by either
hand shaking the sample vigorously for at least 1 min, or by using an acceptable
method of mixing such as a three-axis paint shaker for at least 5 min. The
method chosen should not alter the original distribution of the contaminant
9.1.4 If ultrasonic is used to break up any agglomerates, stand the sample
container so that the level of the liquid in the bath is either just below the fluid
level in the sample bottle, or 3/4 up the side of the container, whichever is least.
The period of immersion shall not exceed 1 min. Hand shake for 30 s afterwards.
9.2 Blank analysis
9.2.1 A blank analysis should be performed before each sample analysis,
unless it can be demonstrated that acceptable blanks can be consistently
obtained. If so, a blank analysis should be performed before starting a counting
programme and at least once during it.
9.2.2 Proceed as in 9.3, using solvent instead of sample liquid. Dispense a 100
mL volume of filtered solvent into the vacuum apparatus fitted with the selected
membrane filter, vacuum filter and aspirate to dryness.
9.2.3 Perform size analysis as specified in 10.3 at ≥ 5 μm. If the count at ≥ 5
μm exceeds the count levels given in the note below, this indicates insufficient
cleaning. Clean the apparatus again and repeat 9.2.2 to 9.2.3.
......
| Standard ID | GB/T 20082-2006 (GB/T20082-2006) | | Description (Translated English) | Hydralic fluid power. Fluid contamination. Determination of particulate contamination by the counting method using an optical microscope | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | J20 | | Classification of International Standard | 23.100.60 | | Word Count Estimation | 14,177 | | Date of Issue | 2006-01-23 | | Date of Implementation | 2006-08-01 | | Quoted Standard | GB/T 12804; GB/T 14039-2002; GB/T 17446; GB/T 17484; GB 50073-2001 | | Adopted Standard | ISO 4407-2002, IDT | | Drafting Organization | China Aviation Industry particle size measurement test station | | Administrative Organization | Hydraulic and pneumatic National Standardization Technical Committee | | Regulation (derived from) | China National Standard Approval Announcement 2006 No.2 (Total No.89) | | Proposing organization | China Machinery Industry Federation | | Issuing agency(ies) | Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China; Standardization Administration of China | | Summary | This standard specifies the use of optical microscopy collected through the membrane surface contaminant particle counting, determination of particulate contamination of the hydraulic fluid in the system, including the application of the transmission or the incident optical system, manually particle counting and image analysis of two way. �� 2��m particle size can be counted in this method, the resolution and accuracy of results and the capacity of the optical system and the operator using. All hydraulic system fluid contamination levels can be analyzed according to the standard. Has a fine precipitate or a high concentration of particles in a liquid sample, in order that the smaller the particle size can be reduced by counting the volume of the filter will increase the uncertainty of the large size of the particles counted. |
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