YY 0954-2015 PDF English
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YY 0954-2015 | English | 140 |
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Nonactive surgical implants - Type I collagen implants - Specific requirements
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YY/T 0954-2015 | English | 399 |
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Nonactive surgical implants--Type Ⅰ collagen implants--Specific requirements
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YY 0954-2015: Nonactive surgical implants - Type I collagen implants - Specific requirements---This is an excerpt. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.), auto-downloaded/delivered in 9 seconds, can be purchased online: https://www.ChineseStandard.net/PDF.aspx/YY0954-2015
YY
MEDICAL INDUSTRY STANDARD
ICS 11.040.40
C 45
Nonactive surgical implants - Type I collagen implants
- Specific requirements
Issued on. MARCH 02, 2015
Implemented on. JANUARY 01, 2017
Issued by. China Food and Drug Administration of China
Table of Contents
Foreword... 3
1 Scope... 4
2 Normative references... 4
3 Terms and definitions... 5
4 Expected performance... 7
5 Design properties... 7
6 Material... 7
APPENDIX A (Normative) Determination of collagen content... 17
APPENDIX B (Normative) Determination of total protein impurity content... 20
Appendix C (Normative) Trace element analysis... 24
Appendix D (Normative) Determination of melting point... 26
Appendix E (Normative) Tryptophan examination... 27
Foreword
This standard was drafted in accordance with the rules given in GB/T 1.1-2009.
Some of the contents of this standard may be related to patents. The issuer of
this document is not responsible for identifying such patents.
This standard was proposed by China Food and Drug Administration of China.
This standard shall be under the jurisdiction of the National Technical
Committee for Standardization of Surgical Implants and Orthopedic Devices
(SAC/TC 110).
The drafting organizations of this standard. China Food and Drug Research
Institute.
The main drafters of this standard. Ke Linnan, Fu Bufang, Wang Jian, Tang
Jinglong, Chen Dandan, Feng Xiaoming, Wang Chunren.
Nonactive surgical implants - Type I collagen
implants - Specific requirements
1 Scope
This standard specifies the specific requirements for injectable collagen
implants (abbreviated as implants) which are prepared from purified (non-
cross-linked) type I collagen as a starting material.
This standard specifies the implant technical requirements and testing methods.
It also specifies the expected performance, design properties, materials, design
evaluation, test methods, clinical evaluation, post-marketing surveillance,
manufacturing, packaging, and information provided by the manufacturer,
taking into account the safety factors of implant.
The implants as specified in this standard are suitable for use in dermal layers
and/or subcutaneous injections for clinical use, in order to eliminate or reduce
facial wrinkles and depressions caused by various reasons.
2 Normative references
The following documents are essential to the application of this document. For
the dated documents, only the versions with the dates indicated are applicable
to this document; for the undated documents, only the latest version (including
all the amendments) are applicable to this Standard.
GB/T 16886.1 Biological evaluation of medical devices - Part 1.Evaluation
and testing within a risk management process
GB/T 16886.3 Biological evaluation of medical devices Part 3.Test for
genotoxicity carcinogenicity and reproductive toxicity
GB/T 16886.4 Biological evaluation of medical devices - Part 4.Selection of
tests for interactions with blood
GB/T 16886.5 Biological evaluation of medical devices - Part 5.Test for vitro
cytotoxicity
GB/T 16886.6 Biological evaluation of medical devices - Part 6.Tests for
local effects after implantation
GB/T 16886.10 Biological evaluation of medical devices - Part 10.Tests for
irritation and delayed-type hypersensitivity
GB/T 16886.11 Biological evaluation of medical devices - Part 11.Tests for
systemic toxicity
GB/T 16886.12 Biological evaluation of medical devices - Part 12.Sample
preparation and reference materials
GB/T 16886.17 Biological evaluation of medical devices - Part 17.
Establishment of allowable limits for leachable substances
GB/T 16886.18 Biological evaluation of medical devices - Part 18.Chemical
characterization of materials
3 Terms and definitions
The following terms and definitions apply to this document.
3.1
Type I collagen
The most abundant collagen in mammalian tissues expressed by encoding
α chain COL1A1 gene and COL1A2 gene, which belongs to fibrin type
collagen.
3.2
Type I collagen implant
It refers to, under sterile conditions, the products produced by homogenously
dispersing the purified (non-cross-linked) type I collagen material into
phosphate buffer to prepare collagen suspensions of different concentrations
AND filling it in the prefilled syringes.
3.3
Protein impurity
It refers to other proteins other than type I collagen that remain after the
collagen purification process. It mainly includes (but not limited to) elastin,
improperly arranged collagen molecules, host cell contaminants, cell culture
contaminants, enzyme preparations, and the like. The type III collagen which
may be accompanied with type I collagen is not considered as protein
impurity.
4 Expected performance
The requirements in Chapter 4 of YY/T 0640-2008 are applicable.
5 Design properties
The requirements in Chapter 5 of YY/T 0640-2008 are applicable.
In order to achieve the desired performance requirements, the design
properties shall take into account the effects due to material degradation.
6 Material
6.1 The requirements in Chapter 6 of YY/T 0640-2008 are applicable.
6.2 The collagen material used shall comply with the requirements of ASTM F
2212-2009.Taking into account that the raw material comes from animals
and/or human body, it has the risk of carrying the virus, so it shall conduct
management in accordance with YY/T 0771.1, YY/T 0771.2, and YY/T 0771.3.
7 Design evaluation
7.1 General principles for design evaluation
7.1.1 The requirements in Chapter 7 of YY/T 0640-2008 are applicable.
7.1.2 In designing and manufacturing collagen implants, it shall pay attention to
the following.
7.2 Preclinical evaluation
7.2.1 General preclinical for preclinical evaluation
The preclinical evaluation of collagen implants shall comply with the
requirements in 7.2 of YY/T 0640-2008.
In accordance with the requirements of the experiment, all test samples shall
be the finally sterilized equipment or components.
The number of samples shall be chosen in accordance with the requirements
of this standard.
7.3 Chemical characteristics
7.3.1 Type I collagen identification
After the SDS-polyacrylamide gel electrophoresis analysis, COMPARE the
electrophoretic bands of the samples and the type I collagen reference product,
AND the electrophoretic bands shall be consistent.
7.3.2 Collagen content
It shall be 80% ~ 120% of the indicated amount.
7.3.6 Total heavy metals and trace elements
7.3.6.1 Total amount of heavy metals (calculated as Pb)
The total amount of heavy metal (calculated as lead Pb) in the implant shall not
exceed 10 μg/g (mass fraction).
7.3.6.2 Trace elements
The total amount of arsenic shall not exceed 1 μg/g; AND the total amount of
chromium, cadmium, copper, iron, mercury, nickel, lead and molybdenum shall
not be more than 50 μg/g (mass fraction).
7.3.7 Melting point
The melting point of the implant shall be within the indicated range.
7.4 Biological properties
7.4.1 Sterility
Type I collagen implants shall be sterile.
7.4.2 Biological evaluation
7.4.2.1 General principles of biological evaluation
It shall, in accordance with the requirements of ISO/IEC 6188 6.1, conduct
biological evaluation against the implants.
8 Test methods
8.1 Appearance
Vertically PLACE the type I collagen implant under the umbrella canopy light,
with the illumination of 1000 lx; arbitrarily ROTATE it and OBSERVE from the
horizontal direction, it shall comply with the provisions of 7.2.2.
8.2 Loading capacity
FOLLOW the provisions of Appendix X F of the Pharmacopoeia of the People's
Republic of China (volume II) (2010 version), AND it shall comply with the
provisions of 7.2.3.
8.3 Dynamic viscosity
8.5 Collagen content
FOLLOW the method of Appendix A, AND the results shall comply with the
provisions of 7.3.2.
8.6 Protein impurity analysis
FOLLOW the method of Appendix B, AND the results shall comply with the
provisions of 7.3.3.
8.9 Total heavy metals and trace elements
8.9.1 Total amount of heavy metals (calculated as Pb)
The residues left under the residues on ignition shall follow the 2nd method of
Appendix VIII H of the Pharmacopoeia of the People's Republic of China
(volume II) (2010 version), AND the results shall comply with the provisions of
7.3.6.1.
8.9.2 Trace elements
FOLLOW the methods as specified in Appendix C; AND the results shall comply
with the provisions of 7.3.6.2.
8.10 Melting point
FOLLOW the method as specified in Appendix D, AND the results shall comply
with the provisions of 7.3.7.
8.11 Acid hydrolyzate
FOLLOW the methods as specified in A.1 to prepare the sample acid
hydrolyzate test solution; USE the amino acid analyzer to determine the amino
acid composition of the acid hydrolyzate of the implants. The results shall
comply with the provisions of 7.3.8.
8.12 Tryptophan inspection
FOLLOW the method as specified in Appendix E, AND the results shall comply
with the provisions of 7.3.9.
9 Clinical evaluation
The requirements in 7.3 of YY/T 0640-2008 apply.
The requirements in ISO 14155-1 and ISO 14155-2 are applicable to clinical
studies.
...... Source: Above contents are excerpted from the full-copy PDF -- translated/reviewed by: www.ChineseStandard.net / Wayne Zheng et al.
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