|
US$339.00 · In stock
Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email.
YC/T 386-2011: Determination of organochlorine pesticide residues in soil. Gas chromatographic method
Status: Valid
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| YC/T 386-2011 | English | 339 |
Add to Cart
|
3 days [Need to translate]
|
Determination of organochlorine pesticide residues in soil. Gas chromatographic method
| Valid |
YC/T 386-2011
|
PDF similar to YC/T 386-2011
Basic data | Standard ID | YC/T 386-2011 (YC/T386-2011) | | Description (Translated English) | Determination of organochlorine pesticide residues in soil. Gas chromatographic method | | Sector / Industry | Tobacco Industry Standard (Recommended) | | Classification of Chinese Standard | X87 | | Classification of International Standard | 65.160 | | Word Count Estimation | 13,179 | | Date of Issue | 2011-03-25 | | Date of Implementation | 2011-04-01 | | Quoted Standard | GB/T 6682; NY/T 395 | | Adopted Standard | EPA 8081A-1996, reference | | Regulation (derived from) | National Tobacco Science (2011) 153 | | Issuing agency(ies) | State Tobacco Monopoly Administration | | Summary | This standard specifies the organochlorine pesticide residues in soil by Gas Chromatography. This standard applies to the soil for 21 organochlorine pesticides residues. The method of measuring soil for 21 organochlorine pesticide residues, the detection limit and the limit of quantification in Appendix A. | YC/T 386-2011: Determination of organochlorine pesticide residues in soil. Gas chromatographic method
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of organochlorine pesticide residues in soil.Gas chromatographic method
ICS 65.160
X87
Record Number. 31587-2011
People's Republic of China tobacco industry standards
Determination of pesticide residues in soil organic
Gas chromatography
Issued on. 2011-03-25
2011-04-01 implementation
State Tobacco Monopoly Bureau issued
Foreword
Accordance with the standards GB/T 1.1-2009. Drafting Rules "Standardization Guide Part 1 standard structure and preparation of" given.
The US Environmental Protection Agency standard reference EPA8081A.1996 "organochlorine pesticides gas chromatography" to develop.
Please note that some of the content of this document may involve patents. Release mechanism of the present document does not assume responsibility for the identification of these patents.
This standard was proposed by the State Tobacco Monopoly Bureau.
This standard by the National Standardization Technical Committee on Tobacco Cigarette Technical Committee (SAC/TC144/SC1) centralized.
This standard was drafted. Hubei Tobacco Research Institute (China Burley Tobacco Experimental Station), Huazhong University of Science and Technology, Tongji School of Pharmacy.
The main drafters of this standard. Lin Guoping, Zhou Qun, Wang Yi, Chengjun Qi, Zhao Yunfei, Chenjia Chun.
Determination of pesticide residues in soil organic
Gas chromatography
1 Scope
This standard specifies the organochlorine pesticide residues in soil by gas chromatography.
This standard applies to soil 21 organochlorine pesticide residues determination. The method for determining soil 21 organochlorine pesticide residues
The detection limit and the limit of quantification in Appendix A.
Note 1. For the soil in different regions, the process will not interfere with peak non-organic pesticide substances and the measurement result of the error. But this does not
This means that the method is applicable to all types of soil, areas, and therefore the measurement result of unknown causes significantly higher demand careful study, use quality
Spectral detector chromatogram confirmed the chemical structure of substances.
NOTE 2. ISO 1750 are listed in Appendix A of organochlorine pesticide chemical name and common name of the structural formula corresponding.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
Laboratory use specifications and test methods GB/T 6682 Analysis
NY/T 395 farmland soil environmental quality monitoring technical specifications
Principle 3
A mixture of organic solvent extraction of soil sample in a Soxhlet extractor, after Florisil SPE column with electron capture detection with
GC detection of organochlorine pesticides in the composition, the use of external calibration curve for quantitative analysis.
4 Reagents and materials
The reagents should apply to pesticide residue analysis, in accordance with the sample measurement (extraction and gas chromatography) The same procedure as blank test
To check its purity, should be achieved no significant effect on the determination of pesticide residues on the reagent blank peak chromatogram baseline. Water should reach GB/T 6682
Two water requirement.
4.1 hexane, pesticide grade or equivalent specifications.
4.2 acetone, pesticide grade or equivalent specifications.
4.3 anhydrous sodium sulfate, AR. Before use burning conditions at 450 ℃ 4h, and then stored in a desiccator, cooled standby.
4.4 hexane - acetone eluent
Take 100mL of acetone (4.2) in 1L flask, add 900mL of n-hexane (4.1) obtained by mixing hexane - acetone eluent.
4.5 0.1μg/mL solution of dieldrin
Pipette 100μg/mL standard solution 1mL dieldrin in 10mL volumetric flask, dilute to volume with n-hexane (4.1). Pipette 1mL
In 100mL flask with n-hexane (4.1) diluted to volume to obtain 0.1μg/mL solution of dieldrin.
4.6 Standards, Appendix A certified single standard solution listed substances in a concentration of 100μg/mL.
4.7 organochlorine pesticide standard solution at 0 ℃ ~ 4 ℃ dark storage conditions, valid for six months.
Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of YC/T 386-2011_English be delivered?Answer: Upon your order, we will start to translate YC/T 386-2011_English as soon as possible, and keep you informed of the progress. The lead time is typically 1 ~ 3 working days. The lengthier the document the longer the lead time. Question 2: Can I share the purchased PDF of YC/T 386-2011_English with my colleagues?Answer: Yes. The purchased PDF of YC/T 386-2011_English will be deemed to be sold to your employer/organization who actually pays for it, including your colleagues and your employer's intranet. Question 3: Does the price include tax/VAT?Answer: Yes. Our tax invoice, downloaded/delivered in 9 seconds, includes all tax/VAT and complies with 100+ countries' tax regulations (tax exempted in 100+ countries) -- See Avoidance of Double Taxation Agreements (DTAs): List of DTAs signed between Singapore and 100+ countriesQuestion 4: Do you accept my currency other than USD?Answer: Yes. If you need your currency to be printed on the invoice, please write an email to [email protected]. In 2 working-hours, we will create a special link for you to pay in any currencies. Otherwise, follow the normal steps: Add to Cart -- Checkout -- Select your currency to pay.
|