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SN/T 2290-2009 English PDF

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SN/T 2290-2009: Determination of acetylsalicylic acid in cosmetics for import and export
Status: Valid
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Basic data

Standard ID SN/T 2290-2009 (SN/T2290-2009)
Description (Translated English) Determination of acetylsalicylic acid in cosmetics for import and export
Sector / Industry Commodity Inspection Standard (Recommended)
Classification of Chinese Standard Y42
Classification of International Standard 71.100.70
Word Count Estimation 16,132
Date of Issue 2009-02-20
Date of Implementation 2009-09-01
Regulation (derived from) National Quality Inspection [2009] No. 67
Issuing agency(ies) General Administration of Customs
Summary This standard specifies the import and export of acetylsalicylic acid in cosmetics by high performance liquid chromatographic method and liquid chromatography mass spectrometry/mass spectrometry confirmatory method. This standard applies to whitening, moisturizing facial uses and other uses of ointments, creams and lotions cosmetics in the determination of acetylsalicylic acid and confirmation.

SN/T 2290-2009: Determination of acetylsalicylic acid in cosmetics for import and export

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of acetylsalicylic acid in cosmetics for import and export Exit inspection and quarantine industry standard book People's Republic of China Detection of acetyl salicylic acid in cosmetics Importers Posted 2009-02-20 2009-09-01 implementation People's Republic of China The State Administration of Quality Supervision, Inspection and Quarantine released

Foreword

The Standard Appendix A, Appendix B and Appendix C are informative appendices. This standard is proposed and managed by the National Certification and Accreditation Administration Committee. This standard was drafted. People's Republic of China Guangdong CIQ. The main drafters of this standard. Chen Jie, Xi Xinglin, Jiao Hong, Wu Ying, Li Xun?. This standard is the first release of the entry-exit inspection and quarantine industry standards. Detection of acetyl salicylic acid in cosmetics Importers

1 Scope

This standard specifies the import and export of acetylsalicylic acid in cosmetics by high performance liquid chromatographic method and LC - MS/MS confirmation methods. This standard applies to the determination and whitening, moisturizing facial and other uses of plaster used, creams and lotions Cosmetics acetyl salicylic acid Confirmed. Principle 2 Extracted with methanol cosmetics acetyl salicylic acid, and the extract after centrifugation, was measured by high performance liquid chromatography. External standard The amount of liquid chromatography - mass spectrometry/mass spectrometry confirmation.

3 Reagents and materials

Unless otherwise indicated, the secondary water is deionized water or redistilled. 3.1 Methanol. HPLC grade. Ammonium acetate 3.2. Analysis of alcohol. 3.3 ammonium acetate solution (0.02mol/L). Weigh accurately ammonium acetate 1.544g, dissolved in water and dilute to 1L. 3.4 acetylsalicylic acid standard substance. purity greater than or equal to 99%. 3.5 acetylsalicylic acid standard stock solution. accurately weighed amount of acetylsalicylic acid standard substance (accurate to 0.1mg), formulated as concentrated methanol Degree standard stock solution of 1000mg/L of. Diluted to concentrations applicable standard working solution as needed with methanol. 3.6 acetylsalicylic acid standard solution. draw a certain amount of standard stock solution was diluted to the appropriate concentration of standard working solution with methanol, temporary use When existing service.

4 instruments and equipment

4.1 High performance liquid chromatograph. equipped with a UV detector. 4.2 Liquid chromatography - mass spectrometry/mass spectrometer. 4.3 Analysis of balance. a sense of the amount of 0.1mg. 4.4 oscillator. 4.5 ultrasonic cleaner. 4.6 cryogenic centrifuge. 10000r/min. 4.7 Polypropylene plastic graduated centrifuge tube. 50mL, stoppered. 4.8 filter. 0.45μm, organic.

5 measuring step

5.1 Sample Processing Weigh about 1g cosmetic samples (accurate to 0.01g), a 50mL graduated centrifuge tube, and methanol was added to 10mL, in shaker The oscillation 1min, ultrasonic cleaner ultrasonic extraction 10min, 10min placed in an ice bath at 5 ℃, 10000r/min centrifugation 10min, supernatant membrane filtration for HPLC. 5.2 Determination 5.2.1 Chromatographic conditions a) UV detector. wavelength of 230nm;

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