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SN/T 2288-2009 English PDF

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SN/T 2288-2009: Determination of beryllium, cadmium, thallium, chromium, arsenic, tellurium, neodymium and lead in cosmetics for import and export. ICP-MS method
Status: Valid
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SN/T 2288-2009English169 Add to Cart 3 days [Need to translate] Determination of beryllium, cadmium, thallium, chromium, arsenic, tellurium, neodymium and lead in cosmetics for import and export. ICP-MS method Valid SN/T 2288-2009

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Basic data

Standard ID SN/T 2288-2009 (SN/T2288-2009)
Description (Translated English) Determination of beryllium, cadmium, thallium, chromium, arsenic, tellurium, neodymium and lead in cosmetics for import and export. ICP-MS method
Sector / Industry Commodity Inspection Standard (Recommended)
Classification of Chinese Standard Y42
Classification of International Standard 71.100.70
Word Count Estimation 6,694
Date of Issue 2009-02-20
Date of Implementation 2009-09-01
Regulation (derived from) National Quality Inspection [2009] No. 67
Issuing agency(ies) General Administration of Customs
Summary This standard specifies the cosmetics beryllium, cadmium, thallium, chromium, arsenic, tellurium, neodymium, lead and inductively coupled plasma mass spectrometry detection method. This standard applies to cosmetics beryllium, cadmium, thallium, chromium, arsenic, tellurium, neodymium, the determination of lead.

SN/T 2288-2009: Determination of beryllium, cadmium, thallium, chromium, arsenic, tellurium, neodymium and lead in cosmetics for import and export. ICP-MS method


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Determination of beryllium, cadmium, thallium, chromium, arsenic, tellurium, neodymium and lead in cosmetics for import and export.ICP-MS method Exit inspection and quarantine industry standard book People's Republic of China Importers and cosmetics Beryllium, cadmium, thallium, chromium, arsenic, tellurium, neodymium, lead Detection by Inductively Coupled Plasma Mass Spectrometry Posted 2009-02-20 2009-09-01 implementation People's Republic of China The State Administration of Quality Supervision, Inspection and Quarantine released

Foreword

Appendix A of this standard is an informative annex. This standard is proposed and managed by the National Certification and Accreditation Administration Committee. This standard was drafted. People's Republic of China Guangdong Entry-Exit Inspection and Quarantine Shanghai People's Republic of China Bureau, People's Republic of China Zhejiang Exit Inspection and Quarantine. The main drafters of this standard. Liujiang Hui, Jiao Hong, Yang Zhenyu, Chen Chun, Raymond, Xiexiang Na Chao. This standard is the first release of the entry-exit inspection and quarantine industry standards. Importers and cosmetics Beryllium, cadmium, thallium, chromium, arsenic, tellurium, neodymium, lead Detection by Inductively Coupled Plasma Mass Spectrometry

1 Scope

This standard specifies the cosmetics beryllium, cadmium, thallium, chromium, arsenic, tellurium, neodymium, lead detection method by inductively coupled plasma mass spectrometry. This standard applies to beryllium, cadmium, thallium, chromium, arsenic, tellurium, neodymium, the determination of lead in cosmetics.

2 Method summary

After the samples by acid digestion, into the inductively coupled plasma mass spectrometer, to a certain concentration range, ionic strength and the analyte content into Proportional, compared with standard series, internal standard.

3 Reagents and materials

Analysis of water deionized water (resistivity greater than 18.0MΩ · cm). 3.1 Nitric acid. pure class distinctions. 3.2 30% hydrogen peroxide. pure class distinctions. 3.3 1% nitric acid. Pipette 1mL, diluted with water to 100mL. 3.4 10μg/mL lithium, yttrium, indium, bismuth mixed internal standard solution. 3.5 10μg/mL beryllium, cadmium, thallium, chromium, arsenic, tellurium, neodymium, lead mixed standard solution. 3.6 1μg/mL beryllium, cadmium, thallium, chromium, arsenic, tellurium, Nd, Pb mixed standard solution. lessons 1mL mixed standard solution (3.5), with 1% nitric acid (3.3) and dilute to 10mL. 3.7 0.1μg/mL beryllium, cadmium, thallium, chromium, arsenic, tellurium, Nd, Pb mixed standard solution. lessons 1mL mixed standard solution (3.6), with 1% nitric acid (3.3) and dilute to 10mL.

4 instruments and equipment

4.1 inductively coupled plasma mass spectrometer. 4.2 Balance. a sense of the amount of 0.1mg. 4.3 microwave digestion. Than 4.4 colorimetric tube. 50mL. Step 5 Analysis 5.1 Microwave Digestion Weigh 0.3g ~ 1g sample (accurate to 0.01g), placed in a microwave digestion tank pressure tank, refer to Table A. 1 Add digestion reagent, Soak 30min. Refer to Table A. 2 digestion conditions, after digestion process is done, digestive moved 50mL colorimetric tube, a small amount of water and washed several times The inner tank washings were combined in colorimetric tube with water to volume, mix standby. 5.2 blank test But without addition of reagent addition, according to the above steps. 5.3 Preparation of the standard series Pipette each element mixed standard solution 0.1μg/mL (3.7) 0.50mL; 1μg/mL (3.6) 0.25mL, 0.50mL;

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