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QB/T 4791-2015 English PDF

QB/T 4791-2015 (QB/T4791-2015, QBT 4791-2015, QBT4791-2015)
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BASIC DATA
Standard ID QB/T 4791-2015 (QB/T4791-2015)
Description (Translated English) Creamer
Sector / Industry Light Industry Industry Standard (Recommended)
Classification of Chinese Standard X51
Classification of International Standard 67.160.20
Word Count Estimation 9,940
Date of Issue 2015-04-30
Date of Implementation 2015-10-01
Quoted Standard GB 2716; GB 2760; GB 4789.2; GB 4789.3; GB 5009.3; GB/T 5009.6-2003; GB/T 5009.37-2003; GB 7718; GB 14880; GB 17402; GB 28050
Drafting Organization China Beverage Industry Association Technical Committee; Beijing University of Science and Technology Development Co., Ltd. Matilda; Suzhou City Jiahe Food Industry Co; Ltd Wuxi Super Food Branch; Nestle (China) Co., Ltd.; Hubei Xiang Yuan Food Co., Ltd.; Fujian State collar food Ltd.; Shandong tree of Engineering Limited; Jiangxi Bougainville-food biological Ltd.
Administrative Organization National Beverage Standardization Technical Committee
Regulation (derived from) Ministry of Industry and Information Technology Announcement (2015 No. 28)
Issuing agency(ies) Ministry of Industry and Information Technology of the People's Republic of China
Summary This Standard specifies the terms and definitions creamer, requirements, test methods, inspection rules, marking, packaging, transportation and storage. This Standard applies to drinks from whitening, and other effects to improve the taste of dairy creamer.


QB/T 4791-2015 LIGHT INDUSTRY STANDARD OF THE PEOPLE’S REPUBLIC OF CHINA ICS 67.160.20 Classification No.: X 51 Record No.: 49705-2015 Creamer 植脂末 ISSUED ON: APRIL 30, 2015 IMPLEMENTED ON: OCTOBER 01, 2015 Issued by: Ministry of Industry and Information Technology of PRC Table of Contents Foreword ... 3 1 Scope ... 4 2 Normative References ... 4 3 Terms and Definitions ... 5 4 Requirements ... 5 5 Test Methods ... 6 6 Inspection Rules ... 8 7 Mark, Package, Transportation and Storage ... 9 Appendix A (Normative) Determination of Surface Oil-Fat-Content ... 10 Foreword This Standard was drafted as per the rules specified in GB/T 1.1-2009. This Standard was proposed by China Light Industry Council. This Standard shall be under the jurisdiction of National Technical Committee for Standardization of Beverage (SAC/TC 472). Drafting organizations of this Standard: Technical Working Committee of China Beverage Industry Association; Beijing Beida Mingde Technology Development Co., Ltd.; Suzhou Jiahe Foods Industry Co., Ltd.; Wuxi Super Food Technology Co., Ltd.; Nestle (China) Ltd.; Hubei Xiangyuan Food Co., Ltd.; Fujian Jumbo Grand Food Co., Ltd.; Shandong Dashu Biological Engineering Technology Co., Ltd.; and Jiangxi Weierbao Food Biology Co., Ltd. Chief drafting staffs of this Standard: Wang Qi, Kang Xiaobin, Zhang Dongbai, Liu Xinrong, Xiong Wenke, Jia Xiaolu, Li Sheng, Shen Fupeng, Xue Bing, and Xie Chuanhua. Creamer 1 Scope This Standard specifies the terms and definitions, requirements, test methods, inspection rules, mark, package, transportation and storage of creamer. This Standard is applicable to the creamers that play a role in whitening and improving the taste of beverages. 2 Normative References The following documents are essential to the application of this document. For the dated documents, only the versions with the dates indicated are applicable to this document; for the undated documents, only the latest version (including all the amendments) are applicable to this document. GB 2716 Hygienic Standard for Edible Vegetable Oil GB 2760 National Food Safety Standard - Standards for Uses of Food Additives GB 4789.2 National Food Safety Standard - Microbiological Examination of Food: Aerobic Plate Count GB 4789.3 National Food Safety Standard - Microbiological Examination of Food: Detection of Coliform Bacteria GB 5009.3 National Food Safety Standard – Determination of Moisture in Foods GB/T 5009.6-2003 Determination of Fat in Foods GB/T 5009.37-2003 Method for Analysis of Hygienic Standard of Edible Oils GB 7718 National Food Safety Standard - Standard for Nutrition Labelling of Prepackaged Foods GB 14880 National Food Safety Standard for the Use of Nutritional Fortification Substances in Foods GB 17402 Hygienic Standard for Edible Hydrogenated Oil GB 28050 National Food Safety Standard - Nutrition Label Standards of Pre- packaged Food 3 Terms and Definitions For the purpose of this document, the following terms and definitions apply. 3.1 Creamer The powdery or granular products taking sugar (including edible sugar or starch sugar) and/or syrup, edible oil and fat as the main raw materials; adding or not adding milk or dairy product, the like food ingredients and food additives; made by spraying, drying and other process technologies for whitening and improving the taste of beverage. 3.2 Scorch particles The dark yellow to black substance, formed by heating and carbonizing during the production of creamer, after screening, still mixed in the creamer. 4 Requirements 4.1 Ingredients 4.1.1 The edible vegetable oil shall conform to the provisions of GB 2716. 4.1.2 The edible hydrogenated oil shall conform to the provisions of GB 17402. 4.1.3 Other ingredients shall conform to the provisions of corresponding national and industry standards. 4.2 Sensory It shall conform to the provisions of Table 1. Table 1 – Sensory Requirements Items Requirements Color and luster White to milky white or milky yellow, or have the color and luster corresponding to the adding ingredients Taste and odor Have the taste and odor conforming to the ingredients, and odorless Structure state Powdery or particle state, loose, no block, no foreign matters 4.3 Physical chemical indicator It shall conform to the provisions of Table 2. Table 2 – Physical and Chemical Indicator Items Requirements Fat / (g/100g) ≥ 3.0 Proportion of surface oil-fat content in the fat / % ≤ 5.0 Peroxide value / (g/100g) ≤ 0.25 Moisture / (g/100g) ≤ 5.0 Scorch particles / (piece/100g) ≤ 5 4.4 Food safety 4.4.1 Food additive and food nutritive fortifier It shall conform to the provisions of GB 2760 and GB 14880. 4.4.2 Aerobic plate count and coliform bacteria It shall conform to the provisions of aerobic plate count and coliform bacteria specified by solid beverage. 4.4.3 Others It shall conform to the provisions of solid beverage specified in the relevant national food safety standard. 5 Test Methods 5.1 Sensory 5.1.1 Take 10g of sample onto the clean white vessel; place it in the bright position; observe its structure state, color and luster. 5.1.2 Take 5g~10g of sample; use 100mL of 80°C distilled water to dissolve; smell its odor, and taste it. 5.2 Physical and chemical indicator 5.2.1 Fat It shall be measured as per the “Method-II Acid Hydrolysis” specified in GB/T 5009.6- 2003. 5.2.2 Proportion of surface oil-fat-content in fat 5.2.2.1 The surface oil-fat-content shall be measured as per the method specified in Appendix A. 5.2.2.2 The proportion of surface oil-fat-content in fat shall be calculated as per the Formula (1): Y = × 100% …………………………………… (1) Where: Y – proportion of surface oil-fat-content in fat, in %; X – surface oil-fat-content of the creamer, in g/100g; M – fat content of the creamer, in g/100g. 5.2.3 Peroxide value 5.2.3.1 Mixed solvent: prepare as per the ratio between chloroform and methanol of 7:3. 5.2.3.2 Specimen: surface oil-fat specimen shall be obtained as per the operation procedures of A.4 in Appendix A. 5.2.3.3 Operation procedures: pipette 10mL of mixed solvent into the surface oil-fact specimen in 5.2.3.2; mix evenly till completely dissolve. Accurately pipette 1.0mL of such specimen solution into the 10mL dry colorimetric tube; then measure as per the “4.2.2 Method-II Colorimetry” in GB/T 5009.37-2003. 5.2.4 Moisture It shall be measured as per the method specified in GB 5009.3. 5.2.5 Scorch particles Take 100g of sample; horizontally pave on the clean white vessel; place in the bright position; then observe the quantities of scorch particles. 5.2.6 Aerobic plate count and coliform bacteria It shall be measured as per the method specified in GB 4789.2 and GB 4789.3. 5.2.7 Others The other food safety requirements shall be measured as per the methods specified in the relevant standards. 6 Inspection Rules 6.1 Batching and sampling 6.1.1 Batching The batch of the products shall be determined as per the corresponding rules specified by the quality management department of the manufacturer. 6.1.2 Sampling 6.1.2.1 Products directly provided to the consumers: randomly sampling at least 12 minimum independent packages (total mass shall be no less than 500g) from each batch of products; separately used for sensory, physical and chemical indicator, aerobic plate count, coliform bacterial inspection, and sample-reserving. 6.1.2.2 Products indirectly provided to the consumers: insert the sampling probe into 5/6 position of each minimum independent package; take no less than 100g of sample (the total mass of sample shall be no less than 1kg); separately used for sensory, physical and chemical indicator, aerobic plate count, coliform bacteria inspection, and sample-reserving. 6.2 Exit-factory inspection 6.2.1 The products can leave the factory only after the inspection department of the enterprise inspect them qualified according to this Standard. 6.2.2 Exit-factory inspection items: sensory, fat, moisture, aerobic plate count, coliform bacteria. 6.3 Type inspection 6.3.1 The type inspection items include all the contents in 4.2~4.4 of this Standard. 6.3.2 Generally, the type inspection shall be conducted once every 6 months. In one of the following cases, the type inspection shall be carried out: --- When there are significant changes on the raw materials, process, and equipment; --- When the production is restored after more than 6 months shutdown; --- When there is a big difference between the exit-factory inspection results and the normal production and inspection records. 6.4 Judgment rules 6.4.1 If all the inspection results are qualified, then the whole batch of products are judged to be qualified. If there are more than 3 items (including 3 items) do not conform to the provisions of this Standard, then the whole batch of products shall be judged to be unqualified directly. 6.4.2 If there are no more than 2 items (including 2 items) do not conform to the provisions of this Standard, double sampling can be taken from the same batch of products for re-inspection, the re-inspection results shall prevail. If there is still 1 item that does not conform to the provisions of this Standard in the re-inspection results, then the whole products shall be judged to be unqualified. 7 Mark, Package, Transportation and Storage 7.1 Mark 7.1.1 The pre-packaged products directly provided to the consumers shall conform to the relevant provisions of GB 7718 and GB 28050. 7.1.2 The pre-packaged products indirectly provided to the consumers shall, in addition to conforming to the GB 7718, be labelled nutrition as per the requirements of GB 28050, if they use hydrogenated and/or partial hydrogenated vegetable oils. 7.2 Package The package materials and containers of the products shall conform to the provisions of relevant national food safety standards. 7.3 Transportation and Storage The products shall be avoid exposing to the sun, rain, heavy pressure during the transportation process. The products shall be stored in a clean, dark, dry, ventilated, pest-and-rodent-free warehouse. The products shall not be transported or stored together with toxic, harmful, odorous, volatile, corrosive items. Appendix A (Normative) Determination of Surface Oil-Fat-Content A.1 Principle After using the petroleum ether solvent to fully extract the creamer sample, evaporate it. After removing the petroleum ether solvent, the remaining materials are the surface oil-fat of the creamer; then obtain the surface oil-fat-content through weighing and calculating. A.2 Reagents The reagents used for test include: a) Petroleum ether: boiling range of 30°C~60°C; b) Nitrogen: purity no less than 99.99%. A.3 Apparatus The apparatus used for test include: a) Electric heating and drying oven: temperature control accuracy of ±1°C; b) Analytical balance: sensitivity of 0.0001g; c) Round-bottomed flask: volume of 100mL; d) Conical flask; e) Rotary evaporator. A.4 Operation procedures Take 8g (accurate to 0.0001g) of sample into the conical flask; add 30mL of petroleum ether; fully shake for 5min; then use filter paper to filer it to the 100mL round-bottomed flask, which has been pre-dried in the 105°C electric heating and drying oven to the constant weight; the filtering slag shall be transferred into the original conical flask. Then use 30mL petroleum ether to shake and extract for twice, the filtrate shall be mixed into the 100mL round-bottomed flask. Place the round-bottomed flask in a rotary evaporator, reduce the pressure and evaporate at the water temperature of 35°C~40°C for 15min; use the filter paper to wipe the moisture outside the flask; blow dry with nitrogen for 30min to remove the solvent. After the solvent is removed completely, weigh the total mass of round-bottomed flask and surface oil-fat-content; then dry by nitrogen till the total mass of round-bottomed flask and surface oil-fat-content is constant. A.5 Result calculation Calculate surface oil-fat-content as per the Formula (A.1): Where: X – surface oil-fat-content of the sample, in g/100g; W1 – mass of round-bottomed flask, in g; W2 – total mass of round-bottomed flask and surface oil-fat, in g; G – Sample mass, in g. The calculation results shall retain one digit after the decimal point. A.6 Tolerance Each sample shall be made into two parallel samples; the result shall be expressed by the arithmetic mean. The absolute difference between two independent determination results obtained under the repeatability condition shall not exceed 5% of the arithmetic mean. __________ END __________ ......