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GB/T 42822-2023 English PDF

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GB/T 42822-2023: Determination of primary aromatic amines in art articles
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Basic data

Standard ID GB/T 42822-2023 (GB/T42822-2023)
Description (Translated English) Determination of primary aromatic amines in art articles
Sector / Industry National Standard (Recommended)
Classification of Chinese Standard Y50
Classification of International Standard 71.040.99
Word Count Estimation 14,158
Date of Issue 2023-08-06
Date of Implementation 2024-03-01
Issuing agency(ies) State Administration for Market Regulation, China National Standardization Administration

GB/T 42822-2023: Determination of primary aromatic amines in art articles

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
ICS 71.040.99 CCSY50 National Standards of People's Republic of China Determination of primary aromatic amines in art supplies Published on 2023-08-06 2024-03-01 Implementation State Administration for Market Regulation Released by the National Standardization Administration Committee

Foreword

This document complies with the provisions of GB/T 1.1-2020 "Standardization Work Guidelines Part 1.Structure and Drafting Rules of Standardization Documents" Drafting. Please note that some content in this document may be subject to patents. The publisher of this document assumes no responsibility for identifying patents. This document is proposed by China Light Industry Federation. This document is under the jurisdiction of the National Stationery and Sports Equipment Standardization Technical Committee (SAC/TC514). This document was drafted by. National Cultural and Educational Supplies Quality Supervision and Inspection Center, Ningbo Product and Food Quality Inspection Institute (Ningbo Fiber Inspection Institute), Ningbo Kangda Art Painting Materials Group Co., Ltd., Shanghai Chenguang Stationery Co., Ltd., Shenzhen Qixin Group Co., Ltd. Company, Guangbo Group Co., Ltd., and CTI Testing and Certification Group Co., Ltd. The main drafters of this document. Ma Ping, Yan Ji, Wang Quanlin, Sun Jianqiang, Zhu Qing, Yao Hongjun, Kang Hongbing, Qiu Guangjin, and Liu Wenqiu. Determination of primary aromatic amines in art supplies

1 Scope

This document describes a liquid chromatography-tandem mass spectrometry method for the determination of primary aromatic amines in art supplies. This document applies to primary aromatic amines in art supplies (including crayons, oil pastels, gouache paints, oil paints, acrylic paints) Determination.

2 Normative reference documents

The contents of the following documents constitute essential provisions of this document through normative references in the text. Among them, the dated quotations For undated referenced documents, only the version corresponding to that date applies to this document; for undated referenced documents, the latest version (including all amendments) applies to this document. GB/T 6682 Specifications and test methods for water used in analytical laboratories GB/T 35600-2017 Stationery terminology and classification

3 Terms and definitions

The terms and definitions defined in GB/T 35600-2017 and the following apply to this document. 3.1 art suppliesartarticles Art stationery Stationery for painting study and creation.

4 Principles

The sample was extracted with acetonitrile, purified and concentrated, then measured with a liquid chromatography-tandem mass spectrometer and quantified by the isotope internal standard method.

5 reagents or materials

Unless otherwise specified, use only analytically pure reagents. 5.1 Water. Class 1 water specified in GB/T 6682. 5.2 Acetonitrile. chromatographically pure. 5.3 Methanol. chromatographically pure. 5.4 Formic acid. chromatographically pure. 5.5 n-hexane. chromatographically pure. 5.6 0.07% formic acid methanol solution. Transfer 70 μL formic acid (5.4) into 100 mL methanol (5.3). 5.7 Fixed volume solution. methanol water = 10 90 (V1 V2). 5.8 Acetonitrile saturated n-hexane. Add acetonitrile to n-hexane to separate layers. 5.9 Hydrochloric acid solution (1mol/L).

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